Crystallography Open Database

Information card for entry 4339124

Preview

Coordinates	4339124.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C7 H134 Fe13 N7 O200 P8 W36
Calculated formula	C7 H35 Fe13 N7 O200 P8 W36
Title of publication	Combination of lacunary polyoxometalates and high-nuclear transition-metal clusters under hydrothermal conditions. 5. A novel tetrameric cluster of [{Fe(II)Fe(III)(12)(mu(3)-OH)(12)(mu(4)-PO(4))(4)}(B-alpha-PW(9)O(34))(4)](22)(-).
Authors of publication	Zhao, Jun-Wei; Zhang, Jie; Zheng, Shou-Tian; Yang, Guo-Yu
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	26
Pages of publication	10944 - 10946
a	36.666 ± 0.007 Å
b	25.887 ± 0.005 Å
c	21.682 ± 0.004 Å
α	90°
β	94.891 ± 0.003°
γ	90°
Cell volume	20505 ± 7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0598
Residual factor for significantly intense reflections	0.0526
Weighted residual factors for significantly intense reflections	0.1327
Weighted residual factors for all reflections included in the refinement	0.1378
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179494 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/91.	4339124.cif
117155	2014-06-14	cif/ Adding structures of 4339124 via cif-deposit CGI script.	4339124.cif