Crystallography Open Database

Information card for entry 4339150

Preview

Coordinates	4339150.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H81 Ag4 F9 N24 O15.5 S3
Calculated formula	C72 H81 Ag4 F9 N24 O15.5 S3
Title of publication	Structural comparisons of silver(I) complexes of third-generation ligands built from tridentate (o-C(6)H(4)[CH(2)OCH(2)C(pz)(3)](2)) versus bidentate poly(1-pyrazolyl)methane units (o-C(6)H(4)[CH(2)OCH(2)CH(pz)(2)](2)) (pz = pyrazolyl ring).
Authors of publication	Reger, Daniel L.; Foley, Elizabeth A.; Semeniuc, Radu F.; Smith, Mark D.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	26
Pages of publication	11345 - 11355
a	13.5708 ± 0.0006 Å
b	28.5556 ± 0.0012 Å
c	25.5868 ± 0.0011 Å
α	90°
β	101.854 ± 0.001°
γ	90°
Cell volume	9704 ± 0.7 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0985
Residual factor for significantly intense reflections	0.0818
Weighted residual factors for significantly intense reflections	0.2071
Weighted residual factors for all reflections included in the refinement	0.2175
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4339150.cif
117161	2014-06-14	cif/ Adding structures of 4339147, 4339148, 4339149, 4339150 via cif-deposit CGI script.	4339150.cif