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Information card for entry 4339160
Preview
| Coordinates | 4339160.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C63 H51 Cl2 N5 Os P2 |
|---|---|
| Calculated formula | C63 H51 Cl2 N5 Os P2 |
| Title of publication | cis-Dicyanoosmium(II) diimine complexes bearing phosphine or sulfoxide ligands: spectroscopic and luminescent studies. |
| Authors of publication | Lai, Siu-Wai; Chan, Queenie K.-W.; Zhu, Nianyong; Che, Chi-Ming |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2007 |
| Journal volume | 46 |
| Journal issue | 26 |
| Pages of publication | 11003 - 11016 |
| a | 12.015 ± 0.002 Å |
| b | 13.223 ± 0.003 Å |
| c | 17.861 ± 0.004 Å |
| α | 83.28 ± 0.03° |
| β | 87.84 ± 0.03° |
| γ | 75.57 ± 0.03° |
| Cell volume | 2729.1 ± 1.1 Å3 |
| Cell temperature | 301 ± 2 K |
| Ambient diffraction temperature | 301 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0355 |
| Residual factor for significantly intense reflections | 0.0315 |
| Weighted residual factors for significantly intense reflections | 0.0856 |
| Weighted residual factors for all reflections included in the refinement | 0.0866 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211151 (current) | 2018-09-25 | cif/4/33/91/ Marking attached hydrogen atoms in entries 4339160-4339163, 4339165. |
4339160.cif |
| 211150 | 2018-09-25 | cif/4/33/91/ Marking atoms 'N5', 'C62', 'C63' and 'N5'', 'C62'', 'C63'' in entry 4339160 as belonging to disorder groups around special positions '-1' and '-2' respectively. |
4339160.cif |
| 179494 | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/91. |
4339160.cif |
| 117171 | 2014-06-14 | cif/ Adding structures of 4339157, 4339158, 4339159, 4339160, 4339161, 4339162, 4339163, 4339164, 4339165 via cif-deposit CGI script. |
4339160.cif |
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Users of the data should acknowledge the original authors of the
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