Crystallography Open Database

Information card for entry 4339396

Preview

Coordinates	4339396.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H83 Cl Li2 O12 Si4 Y
Calculated formula	C72 H83 Cl Li2 O12 Si4 Y
Title of publication	Structural varieties in heterobimetallic lanthanide disiloxanediolates: "inorganic metallocenes" versus in-plane metallacrowns.
Authors of publication	Giessmann, Stephan; Blaurock, Steffen; Lorenz, Volker; Edelmann, Frank T.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	24
Pages of publication	10383 - 10389
a	13.0818 ± 0.0006 Å
b	17.1151 ± 0.0008 Å
c	17.1817 ± 0.0008 Å
α	90°
β	92.599 ± 0.001°
γ	90°
Cell volume	3843 ± 0.3 Å³
Cell temperature	210 ± 2 K
Ambient diffraction temperature	210 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0743
Residual factor for significantly intense reflections	0.0584
Weighted residual factors for significantly intense reflections	0.1802
Weighted residual factors for all reflections included in the refinement	0.1877
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179496 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/93.	4339396.cif
117306	2014-06-14	cif/ Adding structures of 4339396 via cif-deposit CGI script.	4339396.cif