Crystallography Open Database

Information card for entry 4339522

Preview

Coordinates	4339522.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C114 H261 Cl4 N7 O74 Si2 W20 Zr2
Calculated formula	C114 Cl4 N7 O74 Si2 W20 Zr2
Title of publication	Synthesis and structural characterization of a gamma-Keggin-type dimeric silicotungstate with a bis(mu-hydroxo) dizirconium core [(gamma-SiW10O36)2Zr2(mu-OH)2]10-.
Authors of publication	Yamaguchi, Syuhei; Kikukawa, Yuji; Tsuchida, Kazutaka; Nakagawa, Yoshinao; Uehara, Kazuhiro; Yamaguchi, Kazuya; Mizuno, Noritaka
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	21
Pages of publication	8502 - 8504
a	29.4764 ± 0.0007 Å
b	35.6269 ± 0.0008 Å
c	19.0523 ± 0.0003 Å
α	90°
β	108.747 ± 0.0008°
γ	90°
Cell volume	18946.4 ± 0.7 Å³
Cell temperature	153.1 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.068
Weighted residual factors for all reflections included in the refinement	0.202
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4339522.cif
117362	2014-06-14	cif/ Adding structures of 4339522 via cif-deposit CGI script.	4339522.cif