#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:59:06 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179498 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/95/4339526.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4339526
loop_
_publ_author_name
'Tobash, Paul H.'
'DiFilippo, Gary'
'Bobev, Svilen'
'Hur, Namjung'
'Thompson, Joe D.'
'Sarrao, John L.'
_publ_section_title
;
 Structure and properties of Gd3Ge4: the orthorhombic RE3Ge4 structures
 revisited (RE = Y, Tb-Tm).
;
_journal_issue                   21
_journal_name_full               'Inorganic chemistry'
_journal_page_first              8690
_journal_page_last               8697
_journal_paper_doi               10.1021/ic7009034
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         '4(Ge), 3(Gd)'
_chemical_formula_sum            'Gd3 Ge4'
_chemical_formula_weight         762.11
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2007-04-11 # Formatted by publCIF
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   4.0953(11)
_cell_length_b                   10.735(3)
_cell_length_c                   14.335(4)
_cell_measurement_reflns_used    376
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      26.36
_cell_measurement_theta_min      2.84
_cell_volume                     630.2(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0260
_diffrn_reflns_av_sigmaI/netI    0.0205
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            1900
_diffrn_reflns_theta_full        26.36
_diffrn_reflns_theta_max         26.36
_diffrn_reflns_theta_min         2.84
_exptl_absorpt_coefficient_mu    49.772
_exptl_absorpt_correction_T_max  0.1353
_exptl_absorpt_correction_T_min  0.0751
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
SADABS (Sheldrick, 2003) 
;
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    8.032
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1280
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.04
_refine_diff_density_max         0.919
_refine_diff_density_min         -1.647
_refine_diff_density_rms         0.299
_refine_ls_extinction_coef       0.00040(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.149
_refine_ls_matrix_type           full
_refine_ls_number_parameters     28
_refine_ls_number_reflns         376
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.149
_refine_ls_R_factor_all          0.0238
_refine_ls_R_factor_gt           0.0217
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0250P)²+6.4020P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0492
_refine_ls_wR_factor_ref         0.0501
_reflns_number_gt                358
_reflns_number_total             376
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic7009034-file003.cif
_cod_data_source_block           Gd3Ge4
_cod_database_code               4339526
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Gd2 Gd 0.0000 0.04422(7) 0.2500 0.0086(2) Uani 1 4 d S
Gd1 Gd 0.0000 0.33128(5) 0.09670(3) 0.0088(2) Uani 1 2 d S
Ge1 Ge 0.0000 0.0237(2) 0.01938(16) 0.0123(6) Uani 0.50 2 d SP
Ge3 Ge 0.0000 0.77079(15) 0.2500 0.0102(3) Uani 1 4 d S
Ge2 Ge 0.0000 0.62019(11) 0.10931(7) 0.0106(3) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Gd Gd -0.1653 3.9035 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge3 Gd2 Ge2 105.84(3) 1_545 5_445
Ge3 Gd2 Ge2 105.84(3) 1_545 5_545
Ge2 Gd2 Ge2 86.53(3) 5_445 5_545
Ge3 Gd2 Ge2 105.84(3) 1_545 14_546
Ge2 Gd2 Ge2 148.32(5) 5_445 14_546
Ge2 Gd2 Ge2 84.92(4) 5_545 14_546
Ge3 Gd2 Ge2 105.84(3) 1_545 14_446
Ge2 Gd2 Ge2 84.92(4) 5_445 14_446
Ge2 Gd2 Ge2 148.32(5) 5_545 14_446
Ge2 Gd2 Ge2 86.53(3) 14_546 14_446
Ge3 Gd2 Ge3 139.91(2) 1_545 5_545
Ge2 Gd2 Ge3 103.45(3) 5_445 5_545
Ge2 Gd2 Ge3 49.44(2) 5_545 5_545
Ge2 Gd2 Ge3 49.44(2) 14_546 5_545
Ge2 Gd2 Ge3 103.45(3) 14_446 5_545
Ge3 Gd2 Ge3 139.91(2) 1_545 5_445
Ge2 Gd2 Ge3 49.44(2) 5_445 5_445
Ge2 Gd2 Ge3 103.45(3) 5_545 5_445
Ge2 Gd2 Ge3 103.45(3) 14_546 5_445
Ge2 Gd2 Ge3 49.44(2) 14_446 5_445
Ge3 Gd2 Ge3 80.18(5) 5_545 5_445
Ge3 Gd2 Ge1 86.18(4) 1_545 .
Ge2 Gd2 Ge1 49.05(3) 5_445 .
Ge2 Gd2 Ge1 49.05(3) 5_545 .
Ge2 Gd2 Ge1 133.77(2) 14_546 .
Ge2 Gd2 Ge1 133.77(2) 14_446 .
Ge3 Gd2 Ge1 92.92(3) 5_545 .
Ge3 Gd2 Ge1 92.92(3) 5_445 .
Ge3 Gd2 Ge1 86.18(4) 1_545 10_556
Ge2 Gd2 Ge1 133.77(2) 5_445 10_556
Ge2 Gd2 Ge1 133.77(2) 5_545 10_556
Ge2 Gd2 Ge1 49.05(3) 14_546 10_556
Ge2 Gd2 Ge1 49.05(3) 14_446 10_556
Ge3 Gd2 Ge1 92.92(3) 5_545 10_556
Ge3 Gd2 Ge1 92.92(3) 5_445 10_556
Ge1 Gd2 Ge1 172.36(9) . 10_556
Ge3 Gd2 Gd1 52.726(15) 1_545 5_445
Ge2 Gd2 Gd1 53.17(3) 5_445 5_445
Ge2 Gd2 Gd1 98.29(3) 5_545 5_445
Ge2 Gd2 Gd1 158.46(3) 14_546 5_445
Ge2 Gd2 Gd1 100.75(2) 14_446 5_445
Ge3 Gd2 Gd1 144.357(12) 5_545 5_445
Ge3 Gd2 Gd1 96.54(2) 5_445 5_445
Ge1 Gd2 Gd1 51.60(3) . 5_445
Ge1 Gd2 Gd1 122.72(4) 10_556 5_445
Ge3 Gd2 Gd1 52.726(15) 1_545 5_545
Ge2 Gd2 Gd1 98.29(3) 5_445 5_545
Ge2 Gd2 Gd1 53.17(3) 5_545 5_545
Ge2 Gd2 Gd1 100.75(2) 14_546 5_545
Ge2 Gd2 Gd1 158.46(3) 14_446 5_545
Ge3 Gd2 Gd1 96.54(2) 5_545 5_545
Ge3 Gd2 Gd1 144.357(12) 5_445 5_545
Ge1 Gd2 Gd1 51.60(3) . 5_545
Ge1 Gd2 Gd1 122.72(4) 10_556 5_545
Gd1 Gd2 Gd1 65.71(2) 5_445 5_545
Ge3 Gd2 Gd1 52.727(15) 1_545 14_446
Ge2 Gd2 Gd1 100.75(2) 5_445 14_446
Ge2 Gd2 Gd1 158.46(3) 5_545 14_446
Ge2 Gd2 Gd1 98.29(3) 14_546 14_446
Ge2 Gd2 Gd1 53.17(3) 14_446 14_446
Ge3 Gd2 Gd1 144.359(13) 5_545 14_446
Ge3 Gd2 Gd1 96.54(2) 5_445 14_446
Ge1 Gd2 Gd1 122.72(4) . 14_446
Ge1 Gd2 Gd1 51.60(3) 10_556 14_446
Gd1 Gd2 Gd1 71.21(2) 5_445 14_446
Gd1 Gd2 Gd1 105.45(3) 5_545 14_446
Ge2 Gd1 Ge2 100.77(3) 9_565 5_445
Ge2 Gd1 Ge2 100.77(3) 9_565 5_545
Ge2 Gd1 Ge2 84.02(4) 5_445 5_545
Ge2 Gd1 Ge1 51.45(4) 9_565 13_455
Ge2 Gd1 Ge1 87.78(4) 5_445 13_455
Ge2 Gd1 Ge1 148.85(4) 5_545 13_455
Ge2 Gd1 Ge1 51.45(4) 9_565 13
Ge2 Gd1 Ge1 148.85(4) 5_445 13
Ge2 Gd1 Ge1 87.78(4) 5_545 13
Ge1 Gd1 Ge1 83.88(7) 13_455 13
Ge2 Gd1 Ge3 137.810(12) 9_565 5_545
Ge2 Gd1 Ge3 104.31(3) 5_445 5_545
Ge2 Gd1 Ge3 49.86(3) 5_545 5_545
Ge1 Gd1 Ge3 160.24(5) 13_455 5_545
Ge1 Gd1 Ge3 92.89(4) 13 5_545
Ge2 Gd1 Ge3 137.810(12) 9_565 5_445
Ge2 Gd1 Ge3 49.86(3) 5_445 5_445
Ge2 Gd1 Ge3 104.31(3) 5_545 5_445
Ge1 Gd1 Ge3 92.89(4) 13_455 5_445
Ge1 Gd1 Ge3 160.24(5) 13 5_445
Ge3 Gd1 Ge3 83.57(3) 5_545 5_445
Ge2 Gd1 Ge2 83.33(3) 9_565 .
Ge2 Gd1 Ge2 137.39(2) 5_445 .
Ge2 Gd1 Ge2 137.39(2) 5_545 .
Ge1 Gd1 Ge2 61.59(4) 13_455 .
Ge1 Gd1 Ge2 61.59(4) 13 .
Ge3 Gd1 Ge2 99.75(3) 5_545 .
Ge3 Gd1 Ge2 99.75(3) 5_445 .
Ge2 Gd1 Ge1 62.22(4) 9_565 5
Ge2 Gd1 Ge1 162.33(5) 5_445 5
Ge2 Gd1 Ge1 94.14(4) 5_545 5
Ge1 Gd1 Ge1 84.78(2) 13_455 5
Ge1 Gd1 Ge1 13.98(7) 13 5
Ge3 Gd1 Ge1 87.51(4) 5_545 5
Ge3 Gd1 Ge1 146.44(5) 5_445 5
Ge2 Gd1 Ge1 50.08(4) . 5
Ge2 Gd1 Ge1 62.22(4) 9_565 5_455
Ge2 Gd1 Ge1 94.14(4) 5_445 5_455
Ge2 Gd1 Ge1 162.33(5) 5_545 5_455
Ge1 Gd1 Ge1 13.98(7) 13_455 5_455
Ge1 Gd1 Ge1 84.78(2) 13 5_455
Ge3 Gd1 Ge1 146.44(5) 5_545 5_455
Ge3 Gd1 Ge1 87.51(4) 5_445 5_455
Ge2 Gd1 Ge1 50.08(4) . 5_455
Ge1 Gd1 Ge1 82.28(7) 5 5_455
Ge2 Gd1 Ge1 81.45(5) 9_565 .
Ge2 Gd1 Ge1 46.89(3) 5_445 .
Ge2 Gd1 Ge1 46.89(3) 5_545 .
Ge1 Gd1 Ge1 108.00(5) 13_455 .
Ge1 Gd1 Ge1 108.00(5) 13 .
Ge3 Gd1 Ge1 91.56(5) 5_545 .
Ge3 Gd1 Ge1 91.56(5) 5_445 .
Ge2 Gd1 Ge1 164.78(5) . .
Ge1 Gd1 Ge1 121.05(5) 5 .
Ge1 Gd1 Ge1 121.05(5) 5_455 .
Ge2 Gd1 Gd2 117.91(2) 9_565 5
Ge2 Gd1 Gd2 141.01(3) 5_445 5
Ge2 Gd1 Gd2 92.93(3) 5_545 5
Ge1 Gd1 Gd2 111.77(4) 13_455 5
Ge1 Gd1 Gd2 69.26(4) 13 5
Ge3 Gd1 Gd2 49.47(3) 5_545 5
Ge3 Gd1 Gd2 94.19(3) 5_445 5
Ge2 Gd1 Gd2 50.323(19) . 5
Ge1 Gd1 Gd2 56.53(4) 5 5
Ge1 Gd1 Gd2 99.34(4) 5_455 5
Ge1 Gd1 Gd2 139.41(3) . 5
Ge1 Ge1 Ge2 128.84(5) 9 5_545
Ge1 Ge1 Ge2 128.83(5) 9 5_445
Ge2 Ge1 Ge2 102.14(8) 5_545 5_445
Ge1 Ge1 Gd1 86.7(3) 9 13_455
Ge2 Ge1 Gd1 125.86(9) 5_545 13_455
Ge2 Ge1 Gd1 63.00(4) 5_445 13_455
Ge1 Ge1 Gd1 86.7(3) 9 13
Ge2 Ge1 Gd1 63.00(4) 5_545 13
Ge2 Ge1 Gd1 125.86(9) 5_445 13
Gd1 Ge1 Gd1 83.88(7) 13_455 13
Ge1 Ge1 Gd1 79.3(3) 9 5_445
Ge2 Ge1 Gd1 126.77(10) 5_545 5_445
Ge2 Ge1 Gd1 64.85(4) 5_445 5_445
Gd1 Ge1 Gd1 95.22(2) 13_455 5_445
Gd1 Ge1 Gd1 166.02(7) 13 5_445
Ge1 Ge1 Gd1 79.3(3) 9 5_545
Ge2 Ge1 Gd1 64.85(4) 5_545 5_545
Ge2 Ge1 Gd1 126.77(10) 5_445 5_545
Gd1 Ge1 Gd1 166.02(7) 13_455 5_545
Gd1 Ge1 Gd1 95.22(2) 13 5_545
Gd1 Ge1 Gd1 82.28(7) 5_445 5_545
Ge1 Ge1 Gd2 141.4(5) 9 .
Ge2 Ge1 Gd2 59.01(5) 5_545 .
Ge2 Ge1 Gd2 59.01(5) 5_445 .
Gd1 Ge1 Gd2 120.54(5) 13_455 .
Gd1 Ge1 Gd2 120.54(5) 13 .
Gd1 Ge1 Gd2 71.87(5) 5_445 .
Gd1 Ge1 Gd2 71.87(5) 5_545 .
Ge1 Ge1 Gd1 151.0(5) 9 .
Ge2 Ge1 Gd1 58.06(5) 5_545 .
Ge2 Ge1 Gd1 58.06(5) 5_445 .
Gd1 Ge1 Gd1 72.00(5) 13_455 .
Gd1 Ge1 Gd1 72.00(5) 13 .
Gd1 Ge1 Gd1 121.05(5) 5_445 .
Gd1 Ge1 Gd1 121.05(5) 5_545 .
Gd2 Ge1 Gd1 67.63(4) . .
Ge2 Ge3 Ge2 102.56(8) 10_556 .
Ge2 Ge3 Gd2 128.72(4) 10_556 1_565
Ge2 Ge3 Gd2 128.72(4) . 1_565
Ge2 Ge3 Gd1 133.64(3) 10_556 5_455
Ge2 Ge3 Gd1 64.80(2) . 5_455
Gd2 Ge3 Gd1 77.80(3) 1_565 5_455
Ge2 Ge3 Gd1 133.64(3) 10_556 5
Ge2 Ge3 Gd1 64.80(2) . 5
Gd2 Ge3 Gd1 77.80(3) 1_565 5
Gd1 Ge3 Gd1 83.57(3) 5_455 5
Ge2 Ge3 Gd1 64.80(2) 10_556 14_556
Ge2 Ge3 Gd1 133.64(3) . 14_556
Gd2 Ge3 Gd1 77.80(3) 1_565 14_556
Gd1 Ge3 Gd1 155.60(6) 5_455 14_556
Gd1 Ge3 Gd1 91.30(3) 5 14_556
Ge2 Ge3 Gd1 64.80(2) 10_556 14_456
Ge2 Ge3 Gd1 133.64(3) . 14_456
Gd2 Ge3 Gd1 77.80(3) 1_565 14_456
Gd1 Ge3 Gd1 91.30(3) 5_455 14_456
Gd1 Ge3 Gd1 155.60(6) 5 14_456
Gd1 Ge3 Gd1 83.57(3) 14_556 14_456
Ge2 Ge3 Gd2 61.41(3) 10_556 5_455
Ge2 Ge3 Gd2 61.41(3) . 5_455
Gd2 Ge3 Gd2 139.91(2) 1_565 5_455
Gd1 Ge3 Gd2 74.48(2) 5_455 5_455
Gd1 Ge3 Gd2 126.21(3) 5 5_455
Gd1 Ge3 Gd2 126.21(3) 14_556 5_455
Gd1 Ge3 Gd2 74.49(2) 14_456 5_455
Ge2 Ge3 Gd2 61.41(3) 10_556 5
Ge2 Ge3 Gd2 61.41(3) . 5
Gd2 Ge3 Gd2 139.91(2) 1_565 5
Gd1 Ge3 Gd2 126.21(3) 5_455 5
Gd1 Ge3 Gd2 74.48(2) 5 5
Gd1 Ge3 Gd2 74.49(2) 14_556 5
Gd1 Ge3 Gd2 126.21(3) 14_456 5
Gd2 Ge3 Gd2 80.18(5) 5_455 5
Ge3 Ge2 Ge1 128.93(4) . 5_455
Ge3 Ge2 Ge1 128.93(4) . 5
Ge1 Ge2 Ge1 102.14(8) 5_455 5
Ge3 Ge2 Gd2 69.15(3) . 5
Ge1 Ge2 Gd2 139.14(7) 5_455 5
Ge1 Ge2 Gd2 71.94(5) 5 5
Ge3 Ge2 Gd2 69.15(3) . 5_455
Ge1 Ge2 Gd2 71.94(5) 5_455 5_455
Ge1 Ge2 Gd2 139.14(7) 5 5_455
Gd2 Ge2 Gd2 86.53(3) 5 5_455
Ge3 Ge2 Gd1 131.28(5) . 9_565
Ge1 Ge2 Gd1 65.55(6) 5_455 9_565
Ge1 Ge2 Gd1 65.55(6) 5 9_565
Gd2 Ge2 Gd1 135.417(18) 5 9_565
Gd2 Ge2 Gd1 135.417(19) 5_455 9_565
Ge3 Ge2 Gd1 65.34(3) . 5
Ge1 Ge2 Gd1 141.56(7) 5_455 5
Ge1 Ge2 Gd1 75.05(5) 5 5
Gd2 Ge2 Gd1 77.49(2) 5 5
Gd2 Ge2 Gd1 134.49(4) 5_455 5
Gd1 Ge2 Gd1 79.23(3) 9_565 5
Ge3 Ge2 Gd1 65.34(3) . 5_455
Ge1 Ge2 Gd1 75.05(5) 5_455 5_455
Ge1 Ge2 Gd1 141.56(7) 5 5_455
Gd2 Ge2 Gd1 134.49(4) 5 5_455
Gd2 Ge2 Gd1 77.49(2) 5_455 5_455
Gd1 Ge2 Gd1 79.23(3) 9_565 5_455
Gd1 Ge2 Gd1 84.02(4) 5 5_455
Ge3 Ge2 Gd1 132.05(5) . .
Ge1 Ge2 Gd1 65.07(6) 5_455 .
Ge1 Ge2 Gd1 65.07(6) 5 .
Gd2 Ge2 Gd1 76.51(3) 5 .
Gd2 Ge2 Gd1 76.51(3) 5_455 .
Gd1 Ge2 Gd1 96.67(3) 9_565 .
Gd1 Ge2 Gd1 137.39(2) 5 .
Gd1 Ge2 Gd1 137.39(2) 5_455 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Gd2 Ge3 2.9353(19) 1_545
Gd2 Ge2 2.9876(9) 5_445
Gd2 Ge2 2.9876(9) 5_545
Gd2 Ge2 2.9876(9) 14_546
Gd2 Ge2 2.9876(9) 14_446
Gd2 Ge3 3.1795(15) 5_545
Gd2 Ge3 3.1795(15) 5_445
Gd2 Ge1 3.313(2) .
Gd2 Ge1 3.313(2) 10_556
Gd2 Gd1 3.7746(8) 5_445
Gd2 Gd1 3.7746(8) 5_545
Gd2 Gd1 3.7746(8) 14_446
Gd1 Ge2 2.9989(13) 9_565
Gd1 Ge2 3.0596(11) 5_445
Gd1 Ge2 3.0596(11) 5_545
Gd1 Ge1 3.064(2) 13_455
Gd1 Ge1 3.064(2) 13
Gd1 Ge3 3.0730(7) 5_545
Gd1 Ge3 3.0730(7) 5_445
Gd1 Ge2 3.1068(15) .
Gd1 Ge1 3.112(2) 5
Gd1 Ge1 3.112(2) 5_455
Gd1 Ge1 3.483(2) .
Gd1 Gd2 3.7746(8) 5
Ge1 Ge1 0.753(4) 9
Ge1 Ge2 2.6322(15) 5_545
Ge1 Ge2 2.6322(15) 5_445
Ge1 Gd1 3.064(2) 13_455
Ge1 Gd1 3.064(2) 13
Ge1 Gd1 3.112(2) 5_445
Ge1 Gd1 3.112(2) 5_545
Ge3 Ge2 2.5849(15) 10_556
Ge3 Ge2 2.5849(15) .
Ge3 Gd2 2.9353(19) 1_565
Ge3 Gd1 3.0730(7) 5_455
Ge3 Gd1 3.0730(7) 5
Ge3 Gd1 3.0730(7) 14_556
Ge3 Gd1 3.0730(7) 14_456
Ge3 Gd2 3.1795(15) 5_455
Ge3 Gd2 3.1795(15) 5
Ge2 Ge1 2.6322(15) 5_455
Ge2 Ge1 2.6322(15) 5
Ge2 Gd2 2.9875(9) 5
Ge2 Gd2 2.9875(9) 5_455
Ge2 Gd1 2.9989(13) 9_565
Ge2 Gd1 3.0596(11) 5
Ge2 Gd1 3.0595(11) 5_455
