#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:59:06 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179498 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/95/4339528.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4339528
loop_
_publ_author_name
'Tobash, Paul H.'
'DiFilippo, Gary'
'Bobev, Svilen'
'Hur, Namjung'
'Thompson, Joe D.'
'Sarrao, John L.'
_publ_section_title
;
 Structure and properties of Gd3Ge4: the orthorhombic RE3Ge4 structures
 revisited (RE = Y, Tb-Tm).
;
_journal_issue                   21
_journal_name_full               'Inorganic chemistry'
_journal_page_first              8690
_journal_page_last               8697
_journal_paper_doi               10.1021/ic7009034
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         4(Ge),3(Dy)
_chemical_formula_sum            'Dy3 Ge4'
_chemical_formula_weight         777.86
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2007-04-11 # Formatted by publCIF
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   4.0401(11)
_cell_length_b                   10.604(3)
_cell_length_c                   14.159(4)
_cell_measurement_reflns_used    368
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      26.35
_cell_measurement_theta_min      2.88
_cell_volume                     606.6(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0446
_diffrn_reflns_av_sigmaI/netI    0.0290
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            2257
_diffrn_reflns_theta_full        26.35
_diffrn_reflns_theta_max         26.35
_diffrn_reflns_theta_min         2.88
_exptl_absorpt_coefficient_mu    55.863
_exptl_absorpt_correction_T_max  0.112
_exptl_absorpt_correction_T_min  0.082
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
SADABS (Sheldrick, 2003)
;
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    8.517
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1304
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.428
_refine_diff_density_min         -2.002
_refine_diff_density_rms         0.453
_refine_ls_extinction_coef       0.00086(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.120
_refine_ls_matrix_type           full
_refine_ls_number_parameters     28
_refine_ls_number_reflns         368
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.120
_refine_ls_R_factor_all          0.0316
_refine_ls_R_factor_gt           0.0265
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0272P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0542
_refine_ls_wR_factor_ref         0.0559
_reflns_number_gt                324
_reflns_number_total             368
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic7009034-file003.cif
_cod_data_source_block           Dy3Ge4
_cod_database_code               4339528
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy2 Dy 0.0000 0.04465(8) 0.2500 0.0082(3) Uani 1 4 d S
Dy1 Dy 0.0000 0.33044(6) 0.09712(4) 0.0084(2) Uani 1 2 d S
Ge1 Ge 0.0000 0.0170(6) 0.0143(4) 0.0089(11) Uani 0.50 2 d SP
Ge3 Ge 0.0000 0.77286(19) 0.2500 0.0091(4) Uani 1 4 d S
Ge2 Ge 0.0000 0.61992(14) 0.10872(9) 0.0099(4) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge3 Dy2 Ge2 105.68(3) 1_545 5_445
Ge3 Dy2 Ge2 105.68(3) 1_545 5_545
Ge2 Dy2 Ge2 86.33(4) 5_445 5_545
Ge3 Dy2 Ge2 105.68(3) 1_545 14_546
Ge2 Dy2 Ge2 148.63(6) 5_445 14_546
Ge2 Dy2 Ge2 85.29(5) 5_545 14_546
Ge3 Dy2 Ge2 105.68(3) 1_545 14_446
Ge2 Dy2 Ge2 85.29(5) 5_445 14_446
Ge2 Dy2 Ge2 148.63(6) 5_545 14_446
Ge2 Dy2 Ge2 86.33(4) 14_546 14_446
Ge3 Dy2 Ge3 140.15(3) 1_545 5_545
Ge2 Dy2 Ge3 103.35(4) 5_445 5_545
Ge2 Dy2 Ge3 49.77(3) 5_545 5_545
Ge2 Dy2 Ge3 49.77(3) 14_546 5_545
Ge2 Dy2 Ge3 103.35(4) 14_446 5_545
Ge3 Dy2 Ge3 140.15(3) 1_545 5_445
Ge2 Dy2 Ge3 49.77(3) 5_445 5_445
Ge2 Dy2 Ge3 103.35(4) 5_545 5_445
Ge2 Dy2 Ge3 103.35(4) 14_546 5_445
Ge2 Dy2 Ge3 49.77(3) 14_446 5_445
Ge3 Dy2 Ge3 79.71(6) 5_545 5_445
Ge3 Dy2 Ge1 84.98(12) 1_545 .
Ge2 Dy2 Ge1 49.37(6) 5_445 .
Ge2 Dy2 Ge1 49.37(6) 5_545 .
Ge2 Dy2 Ge1 134.31(4) 14_546 .
Ge2 Dy2 Ge1 134.31(4) 14_446 .
Ge3 Dy2 Ge1 93.85(9) 5_545 .
Ge3 Dy2 Ge1 93.85(9) 5_445 .
Ge3 Dy2 Ge1 84.99(12) 1_545 10_556
Ge2 Dy2 Ge1 134.31(4) 5_445 10_556
Ge2 Dy2 Ge1 134.31(4) 5_545 10_556
Ge2 Dy2 Ge1 49.37(6) 14_546 10_556
Ge2 Dy2 Ge1 49.37(6) 14_446 10_556
Ge3 Dy2 Ge1 93.85(9) 5_545 10_556
Ge3 Dy2 Ge1 93.85(9) 5_445 10_556
Ge1 Dy2 Ge1 170.0(2) . 10_556
Ge3 Dy2 Dy1 144.464(17) 1_545 10_556
Ge2 Dy2 Dy1 100.01(4) 5_445 10_556
Ge2 Dy2 Dy1 100.01(4) 5_545 10_556
Ge2 Dy2 Dy1 52.14(3) 14_546 10_556
Ge2 Dy2 Dy1 52.14(3) 14_446 10_556
Ge3 Dy2 Dy1 51.34(2) 5_545 10_556
Ge3 Dy2 Dy1 51.34(2) 5_445 10_556
Ge1 Dy2 Dy1 130.55(12) . 10_556
Ge1 Dy2 Dy1 59.48(12) 10_556 10_556
Ge3 Dy2 Dy1 144.462(17) 1_545 .
Ge2 Dy2 Dy1 52.14(3) 5_445 .
Ge2 Dy2 Dy1 52.14(3) 5_545 .
Ge2 Dy2 Dy1 100.01(4) 14_546 .
Ge2 Dy2 Dy1 100.01(4) 14_446 .
Ge3 Dy2 Dy1 51.34(2) 5_545 .
Ge3 Dy2 Dy1 51.34(2) 5_445 .
Ge1 Dy2 Dy1 59.48(12) . .
Ge1 Dy2 Dy1 130.55(12) 10_556 .
Dy1 Dy2 Dy1 71.07(3) 10_556 .
Ge3 Dy2 Dy1 52.504(17) 1_545 14_446
Ge2 Dy2 Dy1 100.79(3) 5_445 14_446
Ge2 Dy2 Dy1 158.09(4) 5_545 14_446
Ge2 Dy2 Dy1 98.16(3) 14_546 14_446
Ge2 Dy2 Dy1 53.22(3) 14_446 14_446
Ge3 Dy2 Dy1 144.508(14) 5_545 14_446
Ge3 Dy2 Dy1 96.92(3) 5_445 14_446
Ge1 Dy2 Dy1 121.64(10) . 14_446
Ge1 Dy2 Dy1 50.87(9) 10_556 14_446
Dy1 Dy2 Dy1 99.10(2) 10_556 14_446
Dy1 Dy2 Dy1 146.354(15) . 14_446
Ge2 Dy1 Ge2 100.67(3) 9_565 5_445
Ge2 Dy1 Ge2 100.67(3) 9_565 5_545
Ge2 Dy1 Ge2 84.13(5) 5_445 5_545
Ge2 Dy1 Ge3 137.776(14) 9_565 5_545
Ge2 Dy1 Ge3 105.02(5) 5_445 5_545
Ge2 Dy1 Ge3 50.49(4) 5_545 5_545
Ge2 Dy1 Ge3 137.776(14) 9_565 5_445
Ge2 Dy1 Ge3 50.49(4) 5_445 5_445
Ge2 Dy1 Ge3 105.02(5) 5_545 5_445
Ge3 Dy1 Ge3 83.86(3) 5_545 5_445
Ge2 Dy1 Ge1 52.62(8) 9_565 13
Ge2 Dy1 Ge1 150.46(7) 5_445 13
Ge2 Dy1 Ge1 88.68(10) 5_545 13
Ge3 Dy1 Ge1 92.01(10) 5_545 13
Ge3 Dy1 Ge1 157.80(8) 5_445 13
Ge2 Dy1 Ge1 52.62(8) 9_565 13_455
Ge2 Dy1 Ge1 88.68(10) 5_445 13_455
Ge2 Dy1 Ge1 150.46(7) 5_545 13_455
Ge3 Dy1 Ge1 157.80(8) 5_545 13_455
Ge3 Dy1 Ge1 92.01(10) 5_445 13_455
Ge1 Dy1 Ge1 83.6(2) 13 13_455
Ge2 Dy1 Ge1 60.53(9) 9_565 5
Ge2 Dy1 Ge1 160.31(8) 5_445 5
Ge2 Dy1 Ge1 93.29(10) 5_545 5
Ge3 Dy1 Ge1 87.93(11) 5_545 5
Ge3 Dy1 Ge1 147.76(7) 5_445 5
Ge1 Dy1 Ge1 10.20(12) 13 5
Ge1 Dy1 Ge1 84.00(3) 13_455 5
Ge2 Dy1 Ge1 60.53(9) 9_565 5_455
Ge2 Dy1 Ge1 93.29(10) 5_445 5_455
Ge2 Dy1 Ge1 160.31(8) 5_545 5_455
Ge3 Dy1 Ge1 147.76(7) 5_545 5_455
Ge3 Dy1 Ge1 87.93(11) 5_445 5_455
Ge1 Dy1 Ge1 84.00(3) 13 5_455
Ge1 Dy1 Ge1 10.20(12) 13_455 5_455
Ge1 Dy1 Ge1 82.6(2) 5 5_455
Ge2 Dy1 Ge2 82.82(4) 9_565 .
Ge2 Dy1 Ge2 137.43(2) 5_445 .
Ge2 Dy1 Ge2 137.43(2) 5_545 .
Ge3 Dy1 Ge2 99.41(4) 5_545 .
Ge3 Dy1 Ge2 99.41(4) 5_445 .
Ge1 Dy1 Ge2 59.66(9) 13 .
Ge1 Dy1 Ge2 59.66(9) 13_455 .
Ge1 Dy1 Ge2 51.32(7) 5 .
Ge1 Dy1 Ge2 51.32(7) 5_455 .
Ge2 Dy1 Dy2 135.77(4) 9_565 .
Ge2 Dy1 Dy2 50.64(3) 5_445 .
Ge2 Dy1 Dy2 50.64(3) 5_545 .
Ge3 Dy1 Dy2 54.51(4) 5_545 .
Ge3 Dy1 Dy2 54.51(4) 5_445 .
Ge1 Dy1 Dy2 137.46(11) 13 .
Ge1 Dy1 Dy2 137.46(11) 13_455 .
Ge1 Dy1 Dy2 138.48(10) 5 .
Ge1 Dy1 Dy2 138.48(10) 5_455 .
Ge2 Dy1 Dy2 141.40(4) . .
Ge2 Dy1 Dy2 117.56(3) 9_565 5
Ge2 Dy1 Dy2 141.42(3) 5_445 5
Ge2 Dy1 Dy2 93.23(3) 5_545 5
Ge3 Dy1 Dy2 49.15(4) 5_545 5
Ge3 Dy1 Dy2 93.97(3) 5_445 5
Ge1 Dy1 Dy2 67.43(7) 13 5
Ge1 Dy1 Dy2 109.75(8) 13_455 5
Ge1 Dy1 Dy2 58.10(8) 5 5
Ge1 Dy1 Dy2 100.72(7) 5_455 5
Ge2 Dy1 Dy2 50.30(2) . 5
Dy2 Dy1 Dy2 99.10(2) . 5
Ge1 Ge1 Ge2 130.46(10) 9 5_545
Ge1 Ge1 Ge2 130.46(10) 9 5_445
Ge2 Ge1 Ge2 98.98(12) 5_545 5_445
Ge1 Ge1 Dy1 88.1(13) 9 13
Ge2 Ge1 Dy1 62.36(10) 5_545 13
Ge2 Ge1 Dy1 123.3(2) 5_445 13
Ge1 Ge1 Dy1 88.1(13) 9 13_455
Ge2 Ge1 Dy1 123.3(2) 5_545 13_455
Ge2 Ge1 Dy1 62.36(10) 5_445 13_455
Dy1 Ge1 Dy1 83.6(2) 13 13_455
Ge1 Ge1 Dy1 81.7(13) 9 5_445
Ge2 Ge1 Dy1 125.1(3) 5_545 5_445
Ge2 Ge1 Dy1 64.59(10) 5_445 5_445
Dy1 Ge1 Dy1 169.80(12) 13 5_445
Dy1 Ge1 Dy1 96.00(3) 13_455 5_445
Ge1 Ge1 Dy1 81.7(13) 9 5_545
Ge2 Ge1 Dy1 64.59(10) 5_545 5_545
Ge2 Ge1 Dy1 125.1(3) 5_445 5_545
Dy1 Ge1 Dy1 96.00(3) 13 5_545
Dy1 Ge1 Dy1 169.80(12) 13_455 5_545
Dy1 Ge1 Dy1 82.6(2) 5_445 5_545
Ge1 Ge1 Dy2 143.2(19) 9 .
Ge2 Ge1 Dy2 57.50(9) 5_545 .
Ge2 Ge1 Dy2 57.50(9) 5_445 .
Dy1 Ge1 Dy2 118.16(9) 13 .
Dy1 Ge1 Dy2 118.16(9) 13_455 .
Dy1 Ge1 Dy2 71.02(14) 5_445 .
Dy1 Ge1 Dy2 71.02(14) 5_545 .
Ge2 Ge3 Ge2 101.93(10) 10_556 .
Ge2 Ge3 Dy2 129.03(5) 10_556 1_565
Ge2 Ge3 Dy2 129.03(5) . 1_565
Ge2 Ge3 Dy1 64.60(3) 10_556 14_556
Ge2 Ge3 Dy1 133.11(4) . 14_556
Dy2 Ge3 Dy1 78.35(4) 1_565 14_556
Ge2 Ge3 Dy1 64.60(3) 10_556 14_456
Ge2 Ge3 Dy1 133.11(4) . 14_456
Dy2 Ge3 Dy1 78.35(4) 1_565 14_456
Dy1 Ge3 Dy1 83.86(3) 14_556 14_456
Ge2 Ge3 Dy1 133.11(4) 10_556 5_455
Ge2 Ge3 Dy1 64.59(3) . 5_455
Dy2 Ge3 Dy1 78.35(4) 1_565 5_455
Dy1 Ge3 Dy1 156.70(8) 14_556 5_455
Dy1 Ge3 Dy1 91.46(3) 14_456 5_455
Ge2 Ge3 Dy1 133.11(4) 10_556 5
Ge2 Ge3 Dy1 64.59(3) . 5
Dy2 Ge3 Dy1 78.35(4) 1_565 5
Dy1 Ge3 Dy1 91.46(3) 14_556 5
Dy1 Ge3 Dy1 156.70(8) 14_456 5
Dy1 Ge3 Dy1 83.86(3) 5_455 5
Ge2 Ge3 Dy2 61.09(4) 10_556 5_455
Ge2 Ge3 Dy2 61.09(4) . 5_455
Dy2 Ge3 Dy2 140.15(3) 1_565 5_455
Dy1 Ge3 Dy2 125.68(4) 14_556 5_455
Dy1 Ge3 Dy2 74.15(3) 14_456 5_455
Dy1 Ge3 Dy2 74.15(3) 5_455 5_455
Dy1 Ge3 Dy2 125.68(4) 5 5_455
Ge2 Ge3 Dy2 61.09(4) 10_556 5
Ge2 Ge3 Dy2 61.09(4) . 5
Dy2 Ge3 Dy2 140.15(3) 1_565 5
Dy1 Ge3 Dy2 74.15(3) 14_556 5
Dy1 Ge3 Dy2 125.68(4) 14_456 5
Dy1 Ge3 Dy2 125.68(4) 5_455 5
Dy1 Ge3 Dy2 74.15(3) 5 5
Dy2 Ge3 Dy2 79.70(6) 5_455 5
Ge3 Ge2 Ge1 130.51(6) . 5_455
Ge3 Ge2 Ge1 130.51(6) . 5
Ge1 Ge2 Ge1 98.98(12) 5_455 5
Ge3 Ge2 Dy2 69.15(4) . 5
Ge1 Ge2 Dy2 138.60(18) 5_455 5
Ge1 Ge2 Dy2 73.13(13) 5 5
Ge3 Ge2 Dy2 69.15(4) . 5_455
Ge1 Ge2 Dy2 73.13(13) 5_455 5_455
Ge1 Ge2 Dy2 138.60(18) 5 5_455
Dy2 Ge2 Dy2 86.33(4) 5 5_455
Ge3 Ge2 Dy1 130.73(7) . 9_565
Ge1 Ge2 Dy1 65.02(15) 5_455 9_565
Ge1 Ge2 Dy1 65.02(15) 5 9_565
Dy2 Ge2 Dy1 135.62(2) 5 9_565
Dy2 Ge2 Dy1 135.62(2) 5_455 9_565
Ge3 Ge2 Dy1 64.92(4) . 5
Ge1 Ge2 Dy1 141.81(18) 5_455 5
Ge1 Ge2 Dy1 76.54(12) 5 5
Dy2 Ge2 Dy1 77.22(3) 5 5
Dy2 Ge2 Dy1 134.06(5) 5_455 5
Dy1 Ge2 Dy1 79.33(3) 9_565 5
Ge3 Ge2 Dy1 64.92(4) . 5_455
Ge1 Ge2 Dy1 76.54(12) 5_455 5_455
Ge1 Ge2 Dy1 141.81(18) 5 5_455
Dy2 Ge2 Dy1 134.06(5) 5 5_455
Dy2 Ge2 Dy1 77.22(3) 5_455 5_455
Dy1 Ge2 Dy1 79.33(3) 9_565 5_455
Dy1 Ge2 Dy1 84.13(5) 5 5_455
Ge3 Ge2 Dy1 132.10(6) . .
Ge1 Ge2 Dy1 64.09(15) 5_455 .
Ge1 Ge2 Dy1 64.09(15) 5 .
Dy2 Ge2 Dy1 76.48(4) 5 .
Dy2 Ge2 Dy1 76.48(4) 5_455 .
Dy1 Ge2 Dy1 97.18(4) 9_565 .
Dy1 Ge2 Dy1 137.43(2) 5 .
Dy1 Ge2 Dy1 137.43(2) 5_455 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy2 Ge3 2.882(2) 1_545
Dy2 Ge2 2.9528(12) 5_445
Dy2 Ge2 2.9528(12) 5_545
Dy2 Ge2 2.9529(12) 14_546
Dy2 Ge2 2.9529(12) 14_446
Dy2 Ge3 3.1523(18) 5_545
Dy2 Ge3 3.1523(18) 5_445
Dy2 Ge1 3.350(5) .
Dy2 Ge1 3.350(5) 10_556
Dy2 Dy1 3.7242(12) 10_556
Dy2 Dy1 3.7243(12) .
Dy2 Dy1 3.7318(10) 14_446
Dy1 Ge2 2.9618(17) 9_565
Dy1 Ge2 3.0152(13) 5_445
Dy1 Ge2 3.0152(13) 5_545
Dy1 Ge3 3.0231(8) 5_545
Dy1 Ge3 3.0231(8) 5_445
Dy1 Ge1 3.031(6) 13
Dy1 Ge1 3.031(6) 13_455
Dy1 Ge1 3.061(6) 5
Dy1 Ge1 3.061(6) 5_455
Dy1 Ge2 3.0742(18) .
Dy1 Dy2 3.7318(10) 5
Ge1 Ge1 0.542(7) 9
Ge1 Ge2 2.657(2) 5_545
Ge1 Ge2 2.657(2) 5_445
Ge1 Dy1 3.031(6) 13
Ge1 Dy1 3.031(6) 13_455
Ge1 Dy1 3.061(6) 5_445
Ge1 Dy1 3.061(6) 5_545
Ge3 Ge2 2.575(2) 10_556
Ge3 Ge2 2.575(2) .
Ge3 Dy2 2.882(2) 1_565
Ge3 Dy1 3.0231(8) 14_556
Ge3 Dy1 3.0231(8) 14_456
Ge3 Dy1 3.0231(8) 5_455
Ge3 Dy1 3.0231(8) 5
Ge3 Dy2 3.1523(18) 5_455
Ge3 Dy2 3.1523(18) 5
Ge2 Ge1 2.657(2) 5_455
Ge2 Ge1 2.657(2) 5
Ge2 Dy2 2.9528(12) 5
Ge2 Dy2 2.9528(12) 5_455
Ge2 Dy1 2.9618(17) 9_565
Ge2 Dy1 3.0152(13) 5
Ge2 Dy1 3.0152(13) 5_455
