#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:59:06 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179498 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/95/4339529.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4339529
loop_
_publ_author_name
'Tobash, Paul H.'
'DiFilippo, Gary'
'Bobev, Svilen'
'Hur, Namjung'
'Thompson, Joe D.'
'Sarrao, John L.'
_publ_section_title
;
 Structure and properties of Gd3Ge4: the orthorhombic RE3Ge4 structures
 revisited (RE = Y, Tb-Tm).
;
_journal_issue                   21
_journal_name_full               'Inorganic chemistry'
_journal_page_first              8690
_journal_page_last               8697
_journal_paper_doi               10.1021/ic7009034
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         4(Ge),3(Ho)
_chemical_formula_sum            'Ge4 Ho3'
_chemical_formula_weight         785.15
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2007-04-11 # Formatted by publCIF
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   4.0305(17)
_cell_length_b                   10.582(4)
_cell_length_c                   14.138(6)
_cell_measurement_reflns_used    365
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      26.36
_cell_measurement_theta_min      2.88
_cell_volume                     603.0(4)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0447
_diffrn_reflns_av_sigmaI/netI    0.0244
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            3088
_diffrn_reflns_theta_full        26.36
_diffrn_reflns_theta_max         26.36
_diffrn_reflns_theta_min         2.88
_exptl_absorpt_coefficient_mu    58.387
_exptl_absorpt_correction_T_max  0.0538
_exptl_absorpt_correction_T_min  0.0433
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
SADABS (Sheldrick, 2003)
;
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    8.648
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1316
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.372
_refine_diff_density_min         -1.946
_refine_diff_density_rms         0.408
_refine_ls_extinction_coef       0.00163(10)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.183
_refine_ls_matrix_type           full
_refine_ls_number_parameters     28
_refine_ls_number_reflns         365
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.183
_refine_ls_R_factor_all          0.0257
_refine_ls_R_factor_gt           0.0217
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0212P)²+1.7769P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0447
_refine_ls_wR_factor_ref         0.0458
_reflns_number_gt                331
_reflns_number_total             365
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic7009034-file003.cif
_cod_data_source_block           Ho3Ge4
_cod_database_code               4339529
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ho2 Ho 0.0000 0.04521(6) 0.2500 0.0081(2) Uani 1 4 d S
Ho1 Ho 0.0000 0.33034(4) 0.09719(3) 0.0083(2) Uani 1 2 d S
Ge1 Ge 0.0000 0.0159(9) 0.0099(8) 0.0118(13) Uani 0.50 2 d SP
Ge3 Ge 0.0000 0.77394(14) 0.2500 0.0090(3) Uani 1 4 d S
Ge2 Ge 0.0000 0.61985(10) 0.10854(7) 0.0099(3) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ho Ho -0.2175 4.6783 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge3 Ho2 Ge2 105.55(2) 1_545 14_546
Ge3 Ho2 Ge2 105.55(2) 1_545 5_445
Ge2 Ho2 Ge2 148.91(5) 14_546 5_445
Ge3 Ho2 Ge2 105.55(2) 1_545 14_446
Ge2 Ho2 Ge2 86.28(4) 14_546 14_446
Ge2 Ho2 Ge2 85.48(5) 5_445 14_446
Ge3 Ho2 Ge2 105.55(2) 1_545 5_545
Ge2 Ho2 Ge2 85.48(4) 14_546 5_545
Ge2 Ho2 Ge2 86.28(4) 5_445 5_545
Ge2 Ho2 Ge2 148.91(5) 14_446 5_545
Ge3 Ho2 Ge3 140.22(2) 1_545 5_545
Ge2 Ho2 Ge3 49.95(3) 14_546 5_545
Ge2 Ho2 Ge3 103.39(3) 5_445 5_545
Ge2 Ho2 Ge3 103.39(3) 14_446 5_545
Ge2 Ho2 Ge3 49.95(3) 5_545 5_545
Ge3 Ho2 Ge3 140.22(2) 1_545 5_445
Ge2 Ho2 Ge3 103.39(3) 14_546 5_445
Ge2 Ho2 Ge3 49.95(3) 5_445 5_445
Ge2 Ho2 Ge3 49.95(3) 14_446 5_445
Ge2 Ho2 Ge3 103.39(3) 5_545 5_445
Ge3 Ho2 Ge3 79.56(5) 5_545 5_445
Ge3 Ho2 Ge1 84.79(16) 1_545 .
Ge2 Ho2 Ge1 134.44(5) 14_546 .
Ge2 Ho2 Ge1 49.35(7) 5_445 .
Ge2 Ho2 Ge1 134.44(5) 14_446 .
Ge2 Ho2 Ge1 49.35(8) 5_545 .
Ge3 Ho2 Ge1 94.01(13) 5_545 .
Ge3 Ho2 Ge1 94.01(13) 5_445 .
Ge3 Ho2 Ge1 84.79(16) 1_545 10_556
Ge2 Ho2 Ge1 49.35(7) 14_546 10_556
Ge2 Ho2 Ge1 134.44(5) 5_445 10_556
Ge2 Ho2 Ge1 49.35(7) 14_446 10_556
Ge2 Ho2 Ge1 134.44(5) 5_545 10_556
Ge3 Ho2 Ge1 94.01(13) 5_545 10_556
Ge3 Ho2 Ge1 94.01(13) 5_445 10_556
Ge1 Ho2 Ge1 169.6(3) . 10_556
Ge3 Ho2 Ho1 144.398(18) 1_545 .
Ge2 Ho2 Ho1 100.20(3) 14_546 .
Ge2 Ho2 Ho1 52.19(2) 5_445 .
Ge2 Ho2 Ho1 100.20(3) 14_446 .
Ge2 Ho2 Ho1 52.19(2) 5_545 .
Ge3 Ho2 Ho1 51.33(2) 5_545 .
Ge3 Ho2 Ho1 51.33(2) 5_445 .
Ge1 Ho2 Ho1 59.61(17) . .
Ge1 Ho2 Ho1 130.82(17) 10_556 .
Ge3 Ho2 Ho1 144.397(18) 1_545 10_556
Ge2 Ho2 Ho1 52.19(2) 14_546 10_556
Ge2 Ho2 Ho1 100.20(3) 5_445 10_556
Ge2 Ho2 Ho1 52.19(2) 14_446 10_556
Ge2 Ho2 Ho1 100.20(3) 5_545 10_556
Ge3 Ho2 Ho1 51.33(2) 5_545 10_556
Ge3 Ho2 Ho1 51.33(2) 5_445 10_556
Ge1 Ho2 Ho1 130.82(17) . 10_556
Ge1 Ho2 Ho1 59.61(17) 10_556 10_556
Ho1 Ho2 Ho1 71.21(4) . 10_556
Ge3 Ho2 Ho1 52.418(17) 1_545 5_445
Ge2 Ho2 Ho1 157.88(3) 14_546 5_445
Ge2 Ho2 Ho1 53.17(3) 5_445 5_445
Ge2 Ho2 Ho1 100.78(3) 14_446 5_445
Ge2 Ho2 Ho1 98.04(3) 5_545 5_445
Ge3 Ho2 Ho1 144.546(16) 5_545 5_445
Ge3 Ho2 Ho1 97.06(3) 5_445 5_445
Ge1 Ho2 Ho1 50.76(12) . 5_445
Ge1 Ho2 Ho1 121.44(13) 10_556 5_445
Ho1 Ho2 Ho1 99.12(3) . 5_445
Ho1 Ho2 Ho1 146.435(16) 10_556 5_445
Ge2 Ho1 Ge1 53.60(18) 9_565 13
Ge2 Ho1 Ge1 53.60(18) 9_565 13_455
Ge1 Ho1 Ge1 84.4(3) 13 13_455
Ge2 Ho1 Ge2 100.63(3) 9_565 5_445
Ge1 Ho1 Ge2 151.45(14) 13 5_445
Ge1 Ho1 Ge2 88.76(14) 13_455 5_445
Ge2 Ho1 Ge2 100.63(3) 9_565 5_545
Ge1 Ho1 Ge2 88.76(14) 13 5_545
Ge1 Ho1 Ge2 151.45(14) 13_455 5_545
Ge2 Ho1 Ge2 84.13(5) 5_445 5_545
Ge2 Ho1 Ge3 137.781(17) 9_565 5_545
Ge1 Ho1 Ge3 91.15(19) 13 5_545
Ge1 Ho1 Ge3 156.68(12) 13_455 5_545
Ge2 Ho1 Ge3 105.25(4) 5_445 5_545
Ge2 Ho1 Ge3 50.74(3) 5_545 5_545
Ge2 Ho1 Ge3 137.781(17) 9_565 5_445
Ge1 Ho1 Ge3 156.68(12) 13 5_445
Ge1 Ho1 Ge3 91.15(19) 13_455 5_445
Ge2 Ho1 Ge3 50.74(3) 5_445 5_445
Ge2 Ho1 Ge3 105.25(4) 5_545 5_445
Ge3 Ho1 Ge3 83.92(4) 5_545 5_445
Ge2 Ho1 Ge2 82.72(3) 9_565 .
Ge1 Ho1 Ge2 59.00(11) 13 .
Ge1 Ho1 Ge2 59.00(11) 13_455 .
Ge2 Ho1 Ge2 137.45(2) 5_445 .
Ge2 Ho1 Ge2 137.45(2) 5_545 .
Ge3 Ho1 Ge2 99.22(3) 5_545 .
Ge3 Ho1 Ge2 99.22(3) 5_445 .
Ge2 Ho1 Ge1 59.40(18) 9_565 5
Ge1 Ho1 Ge1 8.2(2) 13 5
Ge1 Ho1 Ge1 83.76(4) 13_455 5
Ge2 Ho1 Ge1 159.09(16) 5_445 5
Ge2 Ho1 Ge1 93.17(13) 5_545 5
Ge3 Ho1 Ge1 88.62(19) 5_545 5
Ge3 Ho1 Ge1 148.53(12) 5_445 5
Ge2 Ho1 Ge1 51.88(10) . 5
Ge2 Ho1 Ge1 59.40(18) 9_565 5_455
Ge1 Ho1 Ge1 83.76(4) 13 5_455
Ge1 Ho1 Ge1 8.2(2) 13_455 5_455
Ge2 Ho1 Ge1 93.17(13) 5_445 5_455
Ge2 Ho1 Ge1 159.09(16) 5_545 5_455
Ge3 Ho1 Ge1 148.53(12) 5_545 5_455
Ge3 Ho1 Ge1 88.62(19) 5_445 5_455
Ge2 Ho1 Ge1 51.88(10) . 5_455
Ge1 Ho1 Ge1 82.0(3) 5 5_455
Ge2 Ho1 Ho2 135.87(3) 9_565 .
Ge1 Ho1 Ho2 137.28(16) 13 .
Ge1 Ho1 Ho2 137.28(16) 13_455 .
Ge2 Ho1 Ho2 50.72(3) 5_445 .
Ge2 Ho1 Ho2 50.72(3) 5_545 .
Ge3 Ho1 Ho2 54.67(3) 5_545 .
Ge3 Ho1 Ho2 54.67(3) 5_445 .
Ge2 Ho1 Ho2 141.40(3) . .
Ge1 Ho1 Ho2 138.89(17) 5 .
Ge1 Ho1 Ho2 138.89(17) 5_455 .
Ge2 Ho1 Ho2 117.48(3) 9_565 5
Ge1 Ho1 Ho2 66.34(16) 13 5
Ge1 Ho1 Ho2 108.96(11) 13_455 5
Ge2 Ho1 Ho2 141.53(3) 5_445 5
Ge2 Ho1 Ho2 93.36(3) 5_545 5
Ge3 Ho1 Ho2 49.00(4) 5_545 5
Ge3 Ho1 Ho2 93.83(3) 5_445 5
Ge2 Ho1 Ho2 50.26(2) . 5
Ge1 Ho1 Ho2 59.22(17) 5 5
Ge1 Ho1 Ho2 101.38(10) 5_455 5
Ho2 Ho1 Ho2 99.12(3) . 5
Ge2 Ge1 Ge2 97.2(2) 5_545 5_445
Ge2 Ge1 Ho1 62.36(13) 5_545 13
Ge2 Ge1 Ho1 123.0(3) 5_445 13
Ge2 Ge1 Ho1 123.0(3) 5_545 13_455
Ge2 Ge1 Ho1 62.36(13) 5_445 13_455
Ho1 Ge1 Ho1 84.4(3) 13 13_455
Ge2 Ge1 Ho1 123.1(5) 5_545 5_445
Ge2 Ge1 Ho1 63.97(17) 5_445 5_445
Ho1 Ge1 Ho1 171.8(2) 13 5_445
Ho1 Ge1 Ho1 96.24(4) 13_455 5_445
Ge2 Ge1 Ho1 63.97(17) 5_545 5_545
Ge2 Ge1 Ho1 123.1(5) 5_445 5_545
Ho1 Ge1 Ho1 96.24(4) 13 5_545
Ho1 Ge1 Ho1 171.8(2) 13_455 5_545
Ho1 Ge1 Ho1 82.0(3) 5_445 5_545
Ge2 Ge1 Ho2 56.35(19) 5_545 .
Ge2 Ge1 Ho2 56.35(19) 5_445 .
Ho1 Ge1 Ho2 116.96(14) 13 .
Ho1 Ge1 Ho2 116.96(14) 13_455 .
Ho1 Ge1 Ho2 70.0(3) 5_445 .
Ho1 Ge1 Ho2 70.0(3) 5_545 .
Ge2 Ge3 Ge2 101.62(8) 10_556 .
Ge2 Ge3 Ho2 129.19(4) 10_556 1_565
Ge2 Ge3 Ho2 129.19(4) . 1_565
Ge2 Ge3 Ho1 64.51(3) 10_556 14_556
Ge2 Ge3 Ho1 132.90(4) . 14_556
Ho2 Ge3 Ho1 78.58(3) 1_565 14_556
Ge2 Ge3 Ho1 132.90(4) 10_556 5_455
Ge2 Ge3 Ho1 64.51(3) . 5_455
Ho2 Ge3 Ho1 78.58(3) 1_565 5_455
Ho1 Ge3 Ho1 157.16(6) 14_556 5_455
Ge2 Ge3 Ho1 64.51(3) 10_556 14_456
Ge2 Ge3 Ho1 132.90(4) . 14_456
Ho2 Ge3 Ho1 78.58(3) 1_565 14_456
Ho1 Ge3 Ho1 83.92(4) 14_556 14_456
Ho1 Ge3 Ho1 91.58(4) 5_455 14_456
Ge2 Ge3 Ho1 132.90(4) 10_556 5
Ge2 Ge3 Ho1 64.51(3) . 5
Ho2 Ge3 Ho1 78.58(3) 1_565 5
Ho1 Ge3 Ho1 91.58(4) 14_556 5
Ho1 Ge3 Ho1 83.92(4) 5_455 5
Ho1 Ge3 Ho1 157.16(6) 14_456 5
Ge2 Ge3 Ho2 60.95(4) 10_556 5_455
Ge2 Ge3 Ho2 60.95(4) . 5_455
Ho2 Ge3 Ho2 140.22(2) 1_565 5_455
Ho1 Ge3 Ho2 125.45(4) 14_556 5_455
Ho1 Ge3 Ho2 74.00(3) 5_455 5_455
Ho1 Ge3 Ho2 74.00(3) 14_456 5_455
Ho1 Ge3 Ho2 125.45(4) 5 5_455
Ge2 Ge3 Ho2 60.95(3) 10_556 5
Ge2 Ge3 Ho2 60.95(3) . 5
Ho2 Ge3 Ho2 140.22(3) 1_565 5
Ho1 Ge3 Ho2 74.00(3) 14_556 5
Ho1 Ge3 Ho2 125.45(4) 5_455 5
Ho1 Ge3 Ho2 125.45(4) 14_456 5
Ho1 Ge3 Ho2 74.00(3) 5 5
Ho2 Ge3 Ho2 79.56(5) 5_455 5
Ge3 Ge2 Ge1 131.38(11) . 5_455
Ge3 Ge2 Ge1 131.38(11) . 5
Ge1 Ge2 Ge1 97.2(2) 5_455 5
Ge3 Ge2 Ho2 69.11(4) . 5
Ge1 Ge2 Ho2 139.1(3) 5_455 5
Ge1 Ge2 Ho2 74.3(2) 5 5
Ge3 Ge2 Ho2 69.11(4) . 5_455
Ge1 Ge2 Ho2 74.3(2) 5_455 5_455
Ge1 Ge2 Ho2 139.1(3) 5 5_455
Ho2 Ge2 Ho2 86.28(4) 5 5_455
Ge3 Ge2 Ho1 130.54(5) . 9_565
Ge1 Ge2 Ho1 64.0(3) 5_455 9_565
Ge1 Ge2 Ho1 64.0(3) 5 9_565
Ho2 Ge2 Ho1 135.69(2) 5 9_565
Ho2 Ge2 Ho1 135.69(2) 5_455 9_565
Ge3 Ge2 Ho1 64.75(3) . 5
Ge1 Ge2 Ho1 141.1(3) 5_455 5
Ge1 Ge2 Ho1 76.87(16) 5 5
Ho2 Ge2 Ho1 77.09(3) 5 5
Ho2 Ge2 Ho1 133.85(4) 5_455 5
Ho1 Ge2 Ho1 79.37(3) 9_565 5
Ge3 Ge2 Ho1 64.75(3) . 5_455
Ge1 Ge2 Ho1 76.87(16) 5_455 5_455
Ge1 Ge2 Ho1 141.1(3) 5 5_455
Ho2 Ge2 Ho1 133.85(4) 5 5_455
Ho2 Ge2 Ho1 77.09(3) 5_455 5_455
Ho1 Ge2 Ho1 79.37(3) 9_565 5_455
Ho1 Ge2 Ho1 84.13(5) 5 5_455
Ge3 Ge2 Ho1 132.19(5) . .
Ge1 Ge2 Ho1 64.2(2) 5_455 .
Ge1 Ge2 Ho1 64.2(2) 5 .
Ho2 Ge2 Ho1 76.57(3) 5 .
Ho2 Ge2 Ho1 76.57(3) 5_455 .
Ho1 Ge2 Ho1 97.28(3) 9_565 .
Ho1 Ge2 Ho1 137.45(2) 5 .
Ho1 Ge2 Ho1 137.45(2) 5_455 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ho2 Ge3 2.871(2) 1_545
Ho2 Ge2 2.9471(11) 14_546
Ho2 Ge2 2.9471(11) 5_445
Ho2 Ge2 2.9471(11) 14_446
Ho2 Ge2 2.9471(11) 5_545
Ho2 Ge3 3.1496(16) 5_545
Ho2 Ge3 3.1496(15) 5_445
Ho2 Ge1 3.408(11) .
Ho2 Ge1 3.408(11) 10_556
Ho2 Ho1 3.7110(13) .
Ho2 Ho1 3.7110(13) 10_556
Ho2 Ho1 3.7281(11) 5_445
Ho1 Ge2 2.9560(17) 9_565
Ho1 Ge1 3.000(10) 13
Ho1 Ge1 3.000(10) 13_455
Ho1 Ge2 3.0080(13) 5_445
Ho1 Ge2 3.0080(13) 5_545
Ho1 Ge3 3.0141(10) 5_545
Ho1 Ge3 3.0141(10) 5_445
Ho1 Ge2 3.0679(18) .
Ho1 Ge1 3.073(10) 5
Ho1 Ge1 3.073(10) 5_455
Ho1 Ho2 3.7281(11) 5
Ge1 Ge2 2.686(5) 5_545
Ge1 Ge2 2.686(5) 5_445
Ge1 Ho1 3.000(10) 13
Ge1 Ho1 3.000(10) 13_455
Ge1 Ho1 3.073(10) 5_445
Ge1 Ho1 3.073(10) 5_545
Ge3 Ge2 2.5804(16) 10_556
Ge3 Ge2 2.5804(16) .
Ge3 Ho2 2.871(2) 1_565
Ge3 Ho1 3.0141(10) 14_556
Ge3 Ho1 3.0141(10) 5_455
Ge3 Ho1 3.0141(10) 14_456
Ge3 Ho1 3.0141(10) 5
Ge3 Ho2 3.1496(16) 5_455
Ge3 Ho2 3.1496(15) 5
Ge2 Ge1 2.686(5) 5_455
Ge2 Ge1 2.686(5) 5
Ge2 Ho2 2.9471(11) 5
Ge2 Ho2 2.9471(11) 5_455
Ge2 Ho1 2.9559(17) 9_565
Ge2 Ho1 3.0081(13) 5
Ge2 Ho1 3.0081(13) 5_455
