Crystallography Open Database

Information card for entry 4339653

Preview

Coordinates	4339653.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(Me4N)2(Mo(CN)6).H2O
Formula	C14 H26 Mo N8 O
Calculated formula	C13.92 H34.14 Mo N8 O
Title of publication	Missing link in the ligand-field photolysis of [Mo(CN)8]4-: synthesis, X-ray crystal structure, and physicochemical properties of [Mo(CN)6]2-.
Authors of publication	Szklarzewicz, Janusz; Matoga, Dariusz; Niezgoda, Agnieszka; Yoshioka, Daisuke; Mikuriya, Masahiro
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	23
Pages of publication	9531 - 9533
a	12.59 ± 0.0013 Å
b	12.59 ± 0.0013 Å
c	12.59 ± 0.0013 Å
α	90°
β	90°
γ	90°
Cell volume	1995.6 ± 0.4 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	225
Hermann-Mauguin space group symbol	F m -3 m
Hall space group symbol	-F 4 2 3
Residual factor for all reflections	0.0712
Residual factor for significantly intense reflections	0.067
Weighted residual factors for significantly intense reflections	0.1666
Weighted residual factors for all reflections included in the refinement	0.1729
Goodness-of-fit parameter for all reflections included in the refinement	1.202
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179499 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/96.	4339653.cif
117450	2014-06-15	cif/ Adding structures of 4339653 via cif-deposit CGI script.	4339653.cif