Crystallography Open Database

Information card for entry 4339706

Preview

Coordinates	4339706.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C81 H104 Al3 N7
Calculated formula	C81 H104 Al3 N7
Title of publication	Alumazene adducts with pyridines: synthesis, structure, and stability studies.
Authors of publication	Löbl, Jiri; Timoshkin, Alexey Y.; Cong, Trinh; Necas, Marek; Roesky, Herbert W.; Pinkas, Jiri
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5678 - 5685
a	46.001 ± 0.009 Å
b	16.707 ± 0.003 Å
c	19.466 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	14960 ± 5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.1644
Residual factor for significantly intense reflections	0.083
Weighted residual factors for significantly intense reflections	0.1917
Weighted residual factors for all reflections included in the refinement	0.2312
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339706.cif
117491	2014-06-15	cif/ Adding structures of 4339706 via cif-deposit CGI script.	4339706.cif