Crystallography Open Database

Information card for entry 4339741

Preview

Coordinates	4339741.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H30 Dy2 N4 O18
Calculated formula	C52 H30 Dy2 N4 O18
Title of publication	Porphyrin framework solids. Synthesis and structure of hybrid coordination polymers of tetra(carboxyphenyl)porphyrins and lanthanide-bridging ions.
Authors of publication	Muniappan, Sankar; Lipstman, Sophia; George, Sumod; Goldberg, Israel
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5544 - 5554
a	18.6144 ± 0.0004 Å
b	27.9022 ± 0.0009 Å
c	11.7735 ± 0.0008 Å
α	90°
β	100.085 ± 0.0013°
γ	90°
Cell volume	6020.5 ± 0.5 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1241
Residual factor for significantly intense reflections	0.0693
Weighted residual factors for significantly intense reflections	0.1725
Weighted residual factors for all reflections included in the refinement	0.1913
Goodness-of-fit parameter for all reflections included in the refinement	0.91
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339741.cif
117510	2014-06-15	cif/ Adding structures of 4339737, 4339738, 4339739, 4339740, 4339741, 4339742, 4339743 via cif-deposit CGI script.	4339741.cif