Crystallography Open Database

Information card for entry 4340695

Preview

Coordinates	4340695.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	jb3_4
Chemical name	jb3_4
Formula	C27 H51 Co K N4 O9
Calculated formula	C27 H51 Co K N4 O9
Title of publication	Synthesis and reactivity of tripodal complexes containing pendant bases.
Authors of publication	Blacquiere, Johanna M.; Pegis, Michael L.; Raugei, Simone; Kaminsky, Werner; Forget, Amélie; Cook, Sarah A.; Taguchi, Taketo; Mayer, James M.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	17
Pages of publication	9242 - 9253
a	8.9332 ± 0.0005 Å
b	21.4229 ± 0.0012 Å
c	16.8751 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	3229.5 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0471
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.071
Weighted residual factors for all reflections included in the refinement	0.0782
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179509 (current)	2016-03-23	cif/4/34/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/34/06.	4340695.cif
122943	2014-09-06	cif/ Updating files of 4340692, 4340693, 4340694, 4340695 Original log message: Adding full bibliography for 4340692--4340695.cif.	4340695.cif
122008	2014-08-18	cif/ Adding structures of 4340692, 4340693, 4340694, 4340695 via cif-deposit CGI script.	4340695.cif