Crystallography Open Database

Information card for entry 4341019

Preview

Coordinates	4341019.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Cl7 O P U
Calculated formula	Cl7 O P U
Title of publication	The synthesis and characterization of four new uranium(IV) chlorophosphates: UCl₄(POCl₃), [U₂Cl₉][PCl₄], UCl₃(PO₂Cl₂), and U₂Cl₈(POCl₃).
Authors of publication	Ward, Matthew D.; Chan, Ian Y.; Lebègue, Sébastien; Ibers, James A.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	18
Pages of publication	9969 - 9975
a	8.9155 ± 0.0002 Å
b	8.4329 ± 0.0002 Å
c	17.1934 ± 0.0004 Å
α	90°
β	120.52 ± 0.0012°
γ	90°
Cell volume	1113.56 ± 0.05 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0428
Residual factor for significantly intense reflections	0.0297
Weighted residual factors for significantly intense reflections	0.0594
Weighted residual factors for all reflections included in the refinement	0.0637
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179513 (current)	2016-03-23	cif/4/34/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/34/10.	4341019.cif
126881	2014-11-11	cif/ Updating files of 4341019, 4341020, 4341021, 4341022 Original log message: Adding full bibliography for 4341019--4341022.cif.	4341019.cif
122658	2014-08-31	cif/ Adding structures of 4341019, 4341020, 4341021, 4341022 via cif-deposit CGI script.	4341019.cif