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Information card for entry 4341288
Preview
| Coordinates | 4341288.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29 H32 Mo2 O7 P2 W |
|---|---|
| Calculated formula | C29 H32 Mo2 O7 P2 W |
| Title of publication | Mild P-P Bond Cleavage in the Methyldiphosphenyl Complex [Mo2Cp2(μ-PCy2)(μ-κ(2):κ(2)-P2Me)(CO)2] To Give Novel Phosphide-Bridged Trinuclear Derivatives. |
| Authors of publication | Alvarez, M. Angeles; García, M Esther; García-Vivó, Daniel; Lozano, Raquel; Ramos, Alberto; Ruiz, Miguel A. |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2014 |
| Journal volume | 53 |
| Journal issue | 20 |
| Pages of publication | 11261 - 11273 |
| a | 10.4478 ± 0.0008 Å |
| b | 11.2943 ± 0.0012 Å |
| c | 14.2992 ± 0.0017 Å |
| α | 71.451 ± 0.011° |
| β | 88.166 ± 0.008° |
| γ | 83.909 ± 0.008° |
| Cell volume | 1590.6 ± 0.3 Å3 |
| Cell temperature | 123 ± 0.14 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1221 |
| Residual factor for significantly intense reflections | 0.0695 |
| Weighted residual factors for significantly intense reflections | 0.1673 |
| Weighted residual factors for all reflections included in the refinement | 0.2121 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.954 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179515 (current) | 2016-03-23 | cif/4/34/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/34/12. |
4341288.cif |
| 126926 | 2014-11-12 | cif/ Updating files of 4341286, 4341287, 4341288, 4341289 Original log message: Adding full bibliography for 4341286--4341289.cif. |
4341288.cif |
| 125293 | 2014-10-12 | cif/ Adding structures of 4341286, 4341287, 4341288, 4341289 via cif-deposit CGI script. |
4341288.cif |
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Users of the data should acknowledge the original authors of the
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