Crystallography Open Database

Information card for entry 4341316

Preview

Coordinates	4341316.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H142 Na16 O183 P4 Pd4 W30
Calculated formula	Na9 O143.76 P4 Pd4.02 W30
Title of publication	Tetrapalladium-Containing Polyoxotungstate [Pd(II)4(α-P2W15O56)2](16-): A Comparative Study.
Authors of publication	Izarova, Natalya V.; Maksimovskaya, Raisa I.; Willbold, Sabine; Kögerler, Paul
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	21
Pages of publication	11778 - 11784
a	14.0333 ± 0.0003 Å
b	14.0985 ± 0.0003 Å
c	25.2703 ± 0.0005 Å
α	83.9425 ± 0.0017°
β	76.516 ± 0.0019°
γ	60.514 ± 0.002°
Cell volume	4231.89 ± 0.18 Å³
Cell temperature	120 ± 0.14 K
Ambient diffraction temperature	120 ± 0.14 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0781
Residual factor for significantly intense reflections	0.0722
Weighted residual factors for significantly intense reflections	0.1829
Weighted residual factors for all reflections included in the refinement	0.1874
Goodness-of-fit parameter for all reflections included in the refinement	1.109
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179516 (current)	2016-03-23	cif/4/34/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/34/13.	4341316.cif
126958	2014-11-12	cif/ Updating files of 4341316 Original log message: Adding full bibliography for 4341316.cif.	4341316.cif
125544	2014-10-18	cif/ Adding structures of 4341316 via cif-deposit CGI script.	4341316.cif