Crystallography Open Database

Information card for entry 4342304

Preview

Coordinates	4342304.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H59 Al Ge
Calculated formula	C51 H59 Al Ge
Title of publication	Reaction of a germylene, stannylene, or plumbylene with trimethylaluminum and trimethylgallium: insertion into Al-C or ga-C bonds, a reversible metal-carbon insertion equilibrium, and a new route to diplumbenes.
Authors of publication	Erickson, Jeremy D.; Fettinger, James C.; Power, Philip P.
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	4
Pages of publication	1940 - 1948
a	10.0578 ± 0.0003 Å
b	41.8918 ± 0.0012 Å
c	10.6748 ± 0.0003 Å
α	90°
β	112.046 ± 0.0011°
γ	90°
Cell volume	4168.9 ± 0.2 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0297
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0674
Weighted residual factors for all reflections included in the refinement	0.069
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179526 (current)	2016-03-24	cif/4/34/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/34/23.	4342304.cif
132835	2015-03-04	cif/ Updating files of 4342304, 4342305, 4342306, 4342307, 4342308, 4342309, 4342310 Original log message: Adding full bibliography for 4342304--4342310.cif.	4342304.cif
130512	2015-02-04	cif/ Adding structures of 4342304, 4342305, 4342306, 4342307, 4342308, 4342309, 4342310 via cif-deposit CGI script.	4342304.cif