Crystallography Open Database

Information card for entry 4343090

Preview

Coordinates	4343090.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C99 H126 O2 Sn2
Calculated formula	C99 H126 O2 Sn2
Title of publication	Reversibility in Reactions of Linker-Bridged Distannenes with Terminal Alkynes at Ambient Temperature.
Authors of publication	Schneider, Julia; Henning, Jens; Edrich, Jessica; Schubert, Hartmut; Wesemann, Lars
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	12
Pages of publication	6020 - 6027
a	14.0725 ± 0.0004 Å
b	31.2528 ± 0.0009 Å
c	20.4685 ± 0.0006 Å
α	90°
β	107.206 ± 0.002°
γ	90°
Cell volume	8599.3 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0437
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.098
Goodness-of-fit parameter for all reflections included in the refinement	1.185
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4343090.cif
154606	2015-09-06	cif/ Updating files of 4343090, 4343091, 4343092, 4343093, 4343094, 4343095 Original log message: Adding full bibliography for 4343090--4343095.cif.	4343090.cif
137706	2015-06-04	cif/ Adding structures of 4343090 via cif-deposit CGI script.	4343090.cif