Crystallography Open Database

Information card for entry 4343093

Preview

Coordinates	4343093.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C77 H73 Sn2
Calculated formula	C77 H73 Sn2
Title of publication	Reversibility in Reactions of Linker-Bridged Distannenes with Terminal Alkynes at Ambient Temperature.
Authors of publication	Schneider, Julia; Henning, Jens; Edrich, Jessica; Schubert, Hartmut; Wesemann, Lars
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	12
Pages of publication	6020 - 6027
a	11.607 ± 0.0004 Å
b	13.7772 ± 0.0005 Å
c	21.0867 ± 0.0008 Å
α	83.638 ± 0.002°
β	76.096 ± 0.001°
γ	67.05 ± 0.001°
Cell volume	3013.57 ± 0.19 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0231
Residual factor for significantly intense reflections	0.0201
Weighted residual factors for significantly intense reflections	0.0502
Weighted residual factors for all reflections included in the refinement	0.0524
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
154606 (current)	2015-09-06	cif/ Updating files of 4343090, 4343091, 4343092, 4343093, 4343094, 4343095 Original log message: Adding full bibliography for 4343090--4343095.cif.	4343093.cif
137709	2015-06-04	cif/ Adding structures of 4343093 via cif-deposit CGI script.	4343093.cif