Crystallography Open Database

Information card for entry 4344448

Preview

Coordinates	4344448.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C173 H284 P8 Pt4 Si4
Calculated formula	C173 H284 P8 Pt4 Si4
Title of publication	Understanding the Solution and Solid-State Structures of Pd and Pt PSiP Pincer-Supported Hydrides.
Authors of publication	Suh, Hee-Won; Balcells, David; Edwards, Alison J.; Guard, Louise M.; Hazari, Nilay; Mader, Elizabeth A.; Mercado, Brandon Q.; Repisky, Michal
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	23
Pages of publication	11411 - 11422
a	29.5946 ± 0.0005 Å
b	17.3883 ± 0.0003 Å
c	33.97 ± 0.002 Å
α	90°
β	99.69 ± 0.007°
γ	90°
Cell volume	17231.6 ± 1.2 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0284
Residual factor for significantly intense reflections	0.0272
Weighted residual factors for significantly intense reflections	0.0671
Weighted residual factors for all reflections included in the refinement	0.0678
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	1.54187 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
173573 (current)	2016-01-06	cif/ Updating files of 4344446, 4344447, 4344448, 4344449, 4344450, 4344451 Original log message: Adding full bibliography for 4344446--4344451.cif.	4344448.cif
170419	2015-11-20	cif/ Adding structures of 4344446, 4344447, 4344448, 4344449, 4344450, 4344451 via cif-deposit CGI script.	4344448.cif