Crystallography Open Database

Information card for entry 4345173

Preview

Coordinates	4345173.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C104 H490 Cl21 Eu37 O378
Calculated formula	C104 H175 Cl14 Eu37 O250
Title of publication	Three Giant Lanthanide Clusters Ln37 (Ln = Gd, Tb, and Eu) Featuring A Double-Cage Structure.
Authors of publication	Zhou, Yang; Zheng, Xiu-Ying; Cai, Jing; Hong, Zi-Feng; Yan, Zhi-Hao; Kong, Xiang-Jian; Ren, Yan-Ping; Long, La-Sheng; Zheng, Lan-Sun
Journal of publication	Inorganic chemistry
Year of publication	2017
Journal volume	56
Journal issue	4
Pages of publication	2037 - 2041
a	49.948 ± 0.01 Å
b	27.552 ± 0.006 Å
c	29.639 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	40788 ± 15 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.0585
Residual factor for significantly intense reflections	0.0555
Weighted residual factors for significantly intense reflections	0.143
Weighted residual factors for all reflections included in the refinement	0.1448
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	synchrotronMonochr
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
193410 (current)	2017-03-04	cif/ Updating files of 4345172, 4345173 Original log message: Adding full bibliography for 4345172--4345173.cif.	4345173.cif
191834	2017-02-07	cif/ Adding structures of 4345173 via cif-deposit CGI script.	4345173.cif