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Information card for entry 4345341
Preview
| Coordinates | 4345341.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C46 H69 B2 N13 O U |
|---|---|
| Calculated formula | C46 H69 B2 N13 O U |
| Title of publication | [2π+2π] Cycloaddition of Isocyanates to Uranium(IV) Imido Complexes for the Synthesis of U(IV) κ(2)-Ureato Compounds. |
| Authors of publication | Tatebe, Caleb J.; Zeller, Matthias; Bart, Suzanne C. |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2017 |
| Journal volume | 56 |
| Journal issue | 4 |
| Pages of publication | 1956 - 1965 |
| a | 16.0622 ± 0.0004 Å |
| b | 20.1994 ± 0.0012 Å |
| c | 17.3817 ± 0.0009 Å |
| α | 90° |
| β | 115.484 ± 0.003° |
| γ | 90° |
| Cell volume | 5090.8 ± 0.4 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0904 |
| Residual factor for significantly intense reflections | 0.0518 |
| Weighted residual factors for significantly intense reflections | 0.1061 |
| Weighted residual factors for all reflections included in the refinement | 0.139 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.101 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 192896 (current) | 2017-03-04 | cif/ Adding structures of 4345341 via cif-deposit CGI script. |
4345341.cif |
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Users of the data should acknowledge the original authors of the
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