Crystallography Open Database

Information card for entry 4346041

Preview

Coordinates	4346041.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C67 H92 Ge3 N6 O9 Ru3
Calculated formula	C67 H92 Ge3 N6 O9 Ru3
Title of publication	Amidinatogermylene derivatives of ruthenium carbonyl: new insights into the reactivity of [Ru3(CO)12] with two-electron-donor reagents of high basicity.
Authors of publication	Álvarez-Rodríguez, Lucía; Cabeza, Javier A.; García-Álvarez, Pablo; Pérez-Carreño, Enrique; Polo, Diego
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	6
Pages of publication	2983 - 2994
a	15.6511 ± 0.0002 Å
b	17.8306 ± 0.0002 Å
c	26.7297 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	7459.42 ± 0.17 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0329
Residual factor for significantly intense reflections	0.0287
Weighted residual factors for significantly intense reflections	0.0655
Weighted residual factors for all reflections included in the refinement	0.0685
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
231590 (current)	2019-11-22	cif/ Adding structures of 4346039, 4346040, 4346041, 4346042 via cif-deposit CGI script.	4346041.cif