Crystallography Open Database

Information card for entry 4346784

Preview

Coordinates	4346784.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H62 B F4 N O2 Os P2
Calculated formula	C35 H62 B F4 N O2 Os P2
Title of publication	2-Azetidinones as Precursors of Pincer Ligands: Preparation, Structure, and Spectroscopic Properties of CC'N-Osmium Complexes.
Authors of publication	Casarrubios, Luis; Esteruelas, Miguel A.; Larramona, Carmen; Muntaner, Jaime G.; Oñate, Enrique; Sierra, Miguel A.
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	22
Pages of publication	10998 - 11006
a	8.6959 ± 0.0012 Å
b	12.9629 ± 0.0017 Å
c	17.039 ± 0.002 Å
α	90°
β	104.647 ± 0.002°
γ	90°
Cell volume	1858.3 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0366
Residual factor for significantly intense reflections	0.0312
Weighted residual factors for significantly intense reflections	0.0738
Weighted residual factors for all reflections included in the refinement	0.0763
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
231980 (current)	2019-11-23	cif/ Adding structures of 4346782, 4346783, 4346784 via cif-deposit CGI script.	4346784.cif