Crystallography Open Database

Information card for entry 4347335

Preview

Coordinates	4347335.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H59 Ge2 N4 O0.5 Si4 Te2
Calculated formula	C40 H59 Ge2 N4 O0.5 Si4 Te2
Title of publication	Reactivity Study of a Pyridyl-1-azaallylgermanium(I) Dimer: Synthesis of Heavier Ether and Ester Analogues of Germanium.
Authors of publication	Leung, Wing-Por; Chan, Yuk-Chi; So, Cheuk-Wai; Mak, Thomas C. W.
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	7
Pages of publication	3553 - 3557
a	11.4954 ± 0.0003 Å
b	12.3514 ± 0.0004 Å
c	18.835 ± 0.0005 Å
α	84.4139 ± 0.0017°
β	73.568 ± 0.0015°
γ	70.8713 ± 0.0016°
Cell volume	2423.39 ± 0.12 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.053
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for significantly intense reflections	0.0704
Weighted residual factors for all reflections included in the refinement	0.0777
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
232271 (current)	2019-11-23	cif/ Adding structures of 4347332, 4347333, 4347334, 4347335 via cif-deposit CGI script.	4347335.cif