Crystallography Open Database

Information card for entry 4347801

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Coordinates	4347801.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Ni(tren)(1,2-dap)]2[Sn2S6]*2H2O
Chemical name	'[Ni(C6H18N4)(C3H10N2)]2[Sn2S6]*2H2O'
Formula	C18 H60 N12 Ni2 O2 S6 Sn2
Calculated formula	C18 H60 N12 Ni2 O2 S6 Sn2
Title of publication	Room-Temperature Synthesis of Thiostannates from {[Ni(tren)]2[Sn2S6]}n.
Authors of publication	Hilbert, Jessica; Näther, Christian; Weihrich, Richard; Bensch, Wolfgang
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	16
Pages of publication	7859 - 7865
a	12.9264 ± 0.0003 Å
b	10.1627 ± 0.0003 Å
c	15.6585 ± 0.0004 Å
α	90°
β	113.263 ± 0.002°
γ	90°
Cell volume	1889.78 ± 0.09 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0288
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for significantly intense reflections	0.0575
Weighted residual factors for all reflections included in the refinement	0.0589
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
232508 (current)	2019-11-23	cif/ Adding structures of 4347801 via cif-deposit CGI script.	4347801.cif