Crystallography Open Database

Information card for entry 4348208

Preview

Coordinates	4348208.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H58 N12 Ni2 O17
Calculated formula	C54 H58 N12 Ni2 O17
Title of publication	Syntheses, X-ray structures, catalytic activity and magnetic properties of two new coordination polymers of Co(ii) and Ni(ii) based on benzenedicarboxylate and linear N,N′-donor Schiff base linkers
Authors of publication	Bhattacharya, Biswajit; Maity, Dilip Kumar; Pachfule, Pradip; Colacio, Enrique; Ghoshal, Debajyoti
Journal of publication	Inorg. Chem. Front.
Year of publication	2014
Journal volume	1
Journal issue	5
Pages of publication	414
a	19.6754 ± 0.0003 Å
b	11.3812 ± 0.0003 Å
c	27.5363 ± 0.0005 Å
α	90°
β	107.342 ± 0.001°
γ	90°
Cell volume	5885.9 ± 0.2 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0482
Residual factor for significantly intense reflections	0.0418
Weighted residual factors for significantly intense reflections	0.1246
Weighted residual factors for all reflections included in the refinement	0.128
Goodness-of-fit parameter for all reflections included in the refinement	1.122
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
232828 (current)	2019-11-23	cif/ Adding structures of 4348207, 4348208 via cif-deposit CGI script.	4348208.cif