Crystallography Open Database

Information card for entry 4348534

Preview

Coordinates	4348534.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H68 Au2.11 Cl8.11 Fe P4
Calculated formula	C69 H68 Au2.1087 Cl8.1087 Fe P4
Title of publication	Gold(I) Complexes of Ferrocenyl Polyphosphines: Aurophilic Gold Chloride Formation and Phosphine-Concerted Shuttling of a Dinuclear [ClAu···AuCl] Fragment.
Authors of publication	Rampazzi, Vincent; Roger, Julien; Amardeil, Régine; Penouilh, Marie-José; Richard, Philippe; Fleurat-Lessard, Paul; Hierso, Jean-Cyrille
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	21
Pages of publication	10907 - 10921
a	13.2298 ± 0.0002 Å
b	22.4425 ± 0.0004 Å
c	23.1174 ± 0.0004 Å
α	90°
β	92.882 ± 0.001°
γ	90°
Cell volume	6855.1 ± 0.2 Å³
Cell temperature	115 K
Ambient diffraction temperature	115 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0575
Residual factor for significantly intense reflections	0.0423
Weighted residual factors for significantly intense reflections	0.0711
Weighted residual factors for all reflections included in the refinement	0.0765
Goodness-of-fit parameter for all reflections included in the refinement	1.164
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
233062 (current)	2019-11-23	cif/ Adding structures of 4348532, 4348533, 4348534 via cif-deposit CGI script.	4348534.cif