Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4348785
Preview
| Coordinates | 4348785.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H88 F6 K N3 O13 S2 Si6 Th |
|---|---|
| Calculated formula | C36 H78 F6 K N3 O13 S2 Si6 Th |
| Title of publication | Synthesis, Electrochemistry, and Reactivity of the Actinide Trisulfides [K(18-crown-6)][An(η(3)-S3)(NR2)3] (An = U, Th; R = SiMe3). |
| Authors of publication | Smiles, Danil E.; Wu, Guang; Hayton, Trevor W. |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2016 |
| Journal volume | 55 |
| Journal issue | 18 |
| Pages of publication | 9150 - 9153 |
| a | 13.365 ± 0.005 Å |
| b | 14.225 ± 0.005 Å |
| c | 18.947 ± 0.006 Å |
| α | 102.032 ± 0.005° |
| β | 109.232 ± 0.005° |
| γ | 96.868 ± 0.005° |
| Cell volume | 3257 ± 2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 9 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1559 |
| Residual factor for significantly intense reflections | 0.1166 |
| Weighted residual factors for significantly intense reflections | 0.2749 |
| Weighted residual factors for all reflections included in the refinement | 0.3035 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 233336 (current) | 2019-11-23 | cif/ Adding structures of 4348783, 4348784, 4348785 via cif-deposit CGI script. |
4348785.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.