#------------------------------------------------------------------------------ #$Date: 2021-05-04 01:04:40 +0300 (Tue, 04 May 2021) $ #$Revision: 264806 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/35/07/4350796.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4350796 loop_ _publ_author_name 'Weber, Jeremy E.' 'Hasanayn, Faraj' 'Fataftah, Majed' 'Mercado, Brandon Q.' 'Crabtree, Robert H.' 'Holland, Patrick L.' _publ_section_title ; Electronic and Spin-State Effects on Dinitrogen Splitting to Nitrides in a Rhenium Pincer System. ; _journal_issue 9 _journal_name_full 'Inorganic chemistry' _journal_page_first 6115 _journal_page_last 6124 _journal_paper_doi 10.1021/acs.inorgchem.0c03778 _journal_volume 60 _journal_year 2021 _chemical_absolute_configuration ad _chemical_formula_moiety 'C22 H42 Cl N2 P2 Re' _chemical_formula_sum 'C22 H42 Cl N2 P2 Re' _chemical_formula_weight 618.16 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.8668(3) _cell_length_b 14.5601(4) _cell_length_c 14.8307(5) _cell_measurement_reflns_used 28107 _cell_measurement_temperature 93(2) _cell_measurement_theta_max 27.4640 _cell_measurement_theta_min 2.3480 _cell_volume 2562.47(13) _computing_cell_refinement 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 93(2) _diffrn_detector_area_resol_mean 6.8 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Rigaku Mercury275R CCD' _diffrn_measurement_method \w _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0882 _diffrn_reflns_av_unetI/netI 0.0363 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 44738 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.555 _diffrn_reflns_theta_min 3.083 _diffrn_source 'fine-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 4.982 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.66854 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.16b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour Orange _exptl_crystal_density_diffrn 1.602 _exptl_crystal_description Block _exptl_crystal_F_000 1240 _exptl_crystal_size_max 0.500 _exptl_crystal_size_mid 0.450 _exptl_crystal_size_min 0.300 _refine_diff_density_max 2.131 _refine_diff_density_min -1.228 _refine_diff_density_rms 0.101 _refine_ls_abs_structure_details ; Flack x determined using 2498 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.025(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.111 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 269 _refine_ls_number_reflns 5886 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.111 _refine_ls_R_factor_all 0.0206 _refine_ls_R_factor_gt 0.0198 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0151P)^2^+1.1905P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0480 _refine_ls_wR_factor_ref 0.0485 _reflns_Friedel_coverage 0.781 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.995 _reflns_number_gt 5774 _reflns_number_total 5886 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ic0c03778_si_003.cif _cod_data_source_block mini-19049 _cod_database_code 4350796 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.190 _shelx_estimated_absorpt_t_max 0.316 _shelx_res_file ; mini-19049.res created by SHELXL-2014/7 TITL mini-19049 CELL 0.71073 11.866801 14.560099 14.830665 90 90 90 ZERR 4 0.000319 0.000393 0.000475 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Cl N P Re UNIT 88 168 4 8 8 4 EADP Re1 Re1B L.S. 20 SIZE 0.5 0.45 0.3 TEMP -180 CONF MORE -1 ACTA BOND $H ACTA OMIT 1 0 1 OMIT 1 1 0 OMIT 0 1 1 OMIT 1 1 1 OMIT -1 1 1 OMIT 0 0 2 OMIT 0 2 0 WGHT 0.015100 1.190500 FVAR 0.26979 0.98674 PART 1 RE1 6 0.517374 0.477417 0.427782 21.00000 0.01074 0.00862 = 0.00942 -0.00050 -0.00107 0.00052 PART 0 N1 4 0.441381 0.382967 0.438236 11.00000 0.01928 0.01531 = 0.01880 0.00095 -0.00503 -0.00097 CL1 3 0.604715 0.473330 0.281942 11.00000 0.02030 0.02191 = 0.01049 -0.00203 0.00111 0.00358 N11 4 0.491777 0.556930 0.539960 11.00000 0.01304 0.01387 = 0.01095 -0.00157 0.00069 0.00085 P11 5 0.373042 0.584126 0.376797 11.00000 0.01218 0.01459 = 0.01016 0.00195 0.00020 0.00214 P21 5 0.684695 0.438803 0.517063 11.00000 0.01043 0.01355 = 0.00992 -0.00148 0.00019 0.00062 C11 1 0.306271 0.608265 0.487033 11.00000 0.01344 0.01813 = 0.01737 0.00263 0.00223 0.00455 AFIX 23 H11A 2 0.263142 0.666418 0.484686 11.00000 -1.20000 H11B 2 0.254513 0.557902 0.504242 11.00000 -1.20000 AFIX 0 C21 1 0.401104 0.615507 0.552557 11.00000 0.01603 0.01544 = 0.01085 0.00223 0.00341 0.00351 C31 1 0.420760 0.669312 0.626269 11.00000 0.02175 0.01664 = 0.01474 -0.00105 0.00408 0.00521 AFIX 43 H31 2 0.371765 0.714918 0.649966 11.00000 -1.20000 AFIX 0 C41 1 0.528799 0.644279 0.661195 11.00000 0.02232 0.01612 = 0.01245 -0.00212 0.00137 0.00162 AFIX 43 H41 2 0.565240 0.670275 0.712202 11.00000 -1.20000 AFIX 0 C51 1 0.570023 0.575262 0.606790 11.00000 0.01525 0.01144 = 0.01352 -0.00160 0.00089 -0.00044 C61 1 0.680675 0.525925 0.607914 11.00000 0.01346 0.01507 = 0.01813 -0.00674 -0.00163 0.00014 AFIX 23 H61A 2 0.691365 0.495622 0.667057 11.00000 -1.20000 H61B 2 0.742717 0.570523 0.599282 11.00000 -1.20000 AFIX 0 C12 1 0.435719 0.696910 0.340665 11.00000 0.02523 0.01609 = 0.01655 0.00427 0.00553 0.00307 PART 1 C22 1 0.551367 0.708536 0.386177 11.00000 0.02889 0.01372 = 0.02371 0.00332 0.00217 -0.00602 AFIX 137 H22A 2 0.542080 0.707212 0.451825 11.00000 -1.50000 H22B 2 0.584404 0.767425 0.368143 11.00000 -1.50000 H22C 2 0.601272 0.658377 0.367550 11.00000 -1.50000 AFIX 0 PART 0 C32 1 0.361597 0.778214 0.370259 11.00000 0.04039 0.01455 = 0.03536 0.00818 0.01351 0.01060 AFIX 137 H32A 2 0.285041 0.769844 0.346880 11.00000 -1.50000 H32B 2 0.393202 0.835491 0.346492 11.00000 -1.50000 H32C 2 0.359342 0.781088 0.436253 11.00000 -1.50000 AFIX 0 C42 1 0.453629 0.700067 0.238684 11.00000 0.02607 0.02411 = 0.01772 0.00692 0.00587 0.00351 AFIX 137 H42A 2 0.499636 0.647499 0.220035 11.00000 -1.50000 H42B 2 0.492265 0.757219 0.222481 11.00000 -1.50000 H42C 2 0.380471 0.697509 0.208129 11.00000 -1.50000 AFIX 0 C52 1 0.259500 0.542487 0.299618 11.00000 0.01735 0.02665 = 0.01672 0.00023 -0.00709 -0.00039 C62 1 0.197348 0.464113 0.348061 11.00000 0.01861 0.03114 = 0.03074 -0.00089 -0.00390 -0.00423 AFIX 137 H62A 2 0.251758 0.417152 0.366646 11.00000 -1.50000 H62B 2 0.141938 0.436789 0.307059 11.00000 -1.50000 H62C 2 0.158720 0.488426 0.401365 11.00000 -1.50000 AFIX 0 C72 1 0.310732 0.503350 0.213413 11.00000 0.03117 0.04656 = 0.01574 -0.00821 -0.00393 -0.00783 AFIX 137 H72A 2 0.343806 0.553273 0.177861 11.00000 -1.50000 H72B 2 0.251837 0.472886 0.178042 11.00000 -1.50000 H72C 2 0.369455 0.458760 0.228978 11.00000 -1.50000 AFIX 0 C82 1 0.172691 0.617641 0.277345 11.00000 0.02149 0.04872 = 0.03844 0.01512 -0.00797 0.00436 AFIX 137 H82A 2 0.145227 0.645356 0.333409 11.00000 -1.50000 H82B 2 0.109305 0.590445 0.244463 11.00000 -1.50000 H82C 2 0.208252 0.664986 0.239978 11.00000 -1.50000 AFIX 0 C13 1 0.829838 0.452275 0.468220 11.00000 0.01354 0.02610 = 0.01575 -0.00074 0.00293 0.00027 C23 1 0.924836 0.454828 0.538779 11.00000 0.01314 0.04115 = 0.02095 -0.00274 0.00166 0.00044 AFIX 137 H23A 2 0.904540 0.497573 0.587169 11.00000 -1.50000 H23B 2 0.994865 0.475287 0.510087 11.00000 -1.50000 H23C 2 0.935612 0.393249 0.564023 11.00000 -1.50000 AFIX 0 C33 1 0.852070 0.375749 0.400262 11.00000 0.01933 0.04407 = 0.01820 -0.00660 0.00407 0.00674 AFIX 137 H33A 2 0.859012 0.317041 0.432099 11.00000 -1.50000 H33B 2 0.922126 0.388615 0.367633 11.00000 -1.50000 H33C 2 0.789354 0.372426 0.357395 11.00000 -1.50000 AFIX 0 C43 1 0.829231 0.545336 0.418475 11.00000 0.02185 0.03456 = 0.02519 0.00722 -0.00002 -0.00992 AFIX 137 H43A 2 0.772948 0.543833 0.370141 11.00000 -1.50000 H43B 2 0.903887 0.556847 0.392584 11.00000 -1.50000 H43C 2 0.810472 0.594441 0.461102 11.00000 -1.50000 AFIX 0 C53 1 0.666501 0.326275 0.578294 11.00000 0.01923 0.01363 = 0.01240 -0.00033 -0.00227 0.00080 C63 1 0.646916 0.247477 0.510394 11.00000 0.02833 0.01291 = 0.02235 -0.00337 -0.00747 0.00205 AFIX 137 H63A 2 0.586283 0.264510 0.468763 11.00000 -1.50000 H63B 2 0.625736 0.191574 0.543060 11.00000 -1.50000 H63C 2 0.716298 0.236337 0.476265 11.00000 -1.50000 AFIX 0 C73 1 0.561487 0.335838 0.637152 11.00000 0.02095 0.02357 = 0.01706 0.00460 -0.00049 -0.00355 AFIX 137 H73A 2 0.573953 0.383791 0.682436 11.00000 -1.50000 H73B 2 0.546221 0.277319 0.667429 11.00000 -1.50000 H73C 2 0.496929 0.352536 0.599345 11.00000 -1.50000 AFIX 0 C83 1 0.766641 0.303212 0.639290 11.00000 0.02625 0.01752 = 0.02231 -0.00022 -0.00562 0.00810 AFIX 137 H83A 2 0.831222 0.285175 0.602106 11.00000 -1.50000 H83B 2 0.746251 0.252447 0.679494 11.00000 -1.50000 H83C 2 0.786559 0.357249 0.675318 11.00000 -1.50000 AFIX 0 PART 2 RE1B 6 0.545913 0.538403 0.408048 -21.00000 0.01074 0.00862 = 0.00942 -0.00050 -0.00107 0.00052 HKLF 4 REM mini-19049 REM R1 = 0.0198 for 5774 Fo > 4sig(Fo) and 0.0206 for all 5886 data REM 269 parameters refined using 0 restraints END WGHT 0.0195 0.4078 REM Highest difference peak 2.131, deepest hole -1.228, 1-sigma level 0.101 Q1 1 0.4412 0.4772 0.4285 11.00000 0.05 2.13 Q2 1 0.5993 0.4766 0.4277 11.00000 0.05 1.58 Q3 1 0.5402 0.4773 0.4854 11.00000 0.05 1.11 Q4 1 0.5063 0.4790 0.3668 11.00000 0.05 0.98 Q5 1 0.5144 0.4702 0.3024 11.00000 0.05 0.55 Q6 1 0.5187 0.5724 0.4239 11.00000 0.05 0.50 Q7 1 0.4366 0.5603 0.4208 11.00000 0.05 0.49 Q8 1 0.6516 0.4770 0.4371 11.00000 0.05 0.49 Q9 1 0.5191 0.4752 0.7142 11.00000 0.05 0.47 Q10 1 0.7710 0.4403 0.5032 11.00000 0.05 0.44 Q11 1 0.5153 0.4779 0.5431 11.00000 0.05 0.43 Q12 1 0.3155 0.5740 0.3390 11.00000 0.05 0.38 Q13 1 0.3656 0.4642 0.4111 11.00000 0.05 0.36 Q14 1 0.6157 0.4425 0.4974 11.00000 0.05 0.36 Q15 1 0.3244 0.5901 0.4295 11.00000 0.05 0.36 Q16 1 0.4762 0.6592 0.6502 11.00000 0.05 0.34 Q17 1 0.3646 0.6151 0.5166 11.00000 0.05 0.33 Q18 1 0.4444 0.5793 0.3597 11.00000 0.05 0.31 Q19 1 0.4527 0.6031 0.3692 11.00000 0.05 0.31 Q20 1 0.3648 0.4707 0.4564 11.00000 0.05 0.30 ; _shelx_res_checksum 24455 _shelx_hkl_file ; 0 0 2 2332.92 26.85 0 0 -2 2098.56 27.44 0 0 2 3180.11 31.24 0 0 2 2710.81 31.24 0 0 3 3.24 1.80 0 0 3 6.71 1.45 0 0 -3 4.92 2.28 0 0 3 5.06 2.16 0 0 3 9.75 2.82 0 0 4 1023.44 27.25 0 0 4 730.78 15.11 0 0 4 912.10 24.17 0 0 4 1073.05 25.72 0 0 -4 609.80 20.71 0 0 -5 0.57 2.01 0 0 5 3.50 1.86 0 0 5 3.55 1.48 0 0 5 4.21 1.54 0 0 5 1.26 3.14 0 0 -6 2284.29 49.77 0 0 6 3451.58 62.05 0 0 6 2468.38 34.11 0 0 6 3277.43 56.19 0 0 6 3685.43 59.33 0 0 7 5.57 2.66 0 0 -7 4.19 3.30 0 0 7 6.93 6.13 0 0 7 7.68 3.73 0 0 7 3.73 3.99 0 0 8 946.18 37.99 0 0 -8 633.56 30.32 0 0 8 919.76 34.85 0 0 8 1045.95 36.81 0 0 -9 0.44 4.70 0 0 9 6.66 4.23 0 0 9 0.46 3.93 0 0 -9 0.72 2.38 0 0 9 6.85 4.46 0 0 10 21.31 4.14 0 0 10 28.49 8.55 0 0 -10 15.11 3.95 0 0 10 22.43 7.64 0 0 -10 17.82 4.30 0 0 11 1.49 4.28 0 0 11 6.64 5.39 0 0 11 6.06 5.08 0 0 -11 -0.58 4.82 0 0 12 256.52 23.92 0 0 12 275.17 26.08 0 0 -12 193.39 21.23 0 0 12 289.24 24.93 0 0 13 2.41 6.59 0 0 13 6.90 6.33 0 0 -13 9.01 10.26 0 0 13 9.61 7.68 0 0 14 2460.71 78.33 0 0 -14 1763.37 71.77 0 0 14 2746.10 81.75 0 0 14 2572.45 86.33 0 0 15 -1.41 6.25 0 0 15 5.98 6.51 0 0 -15 3.44 7.12 0 0 15 -6.12 8.52 0 0 16 227.02 27.09 0 0 -16 197.16 25.84 0 0 16 286.86 33.04 0 0 16 268.21 28.51 0 0 17 4.15 6.83 0 0 17 6.86 5.86 0 0 -17 0.10 4.52 0 0 17 3.80 8.41 0 0 -18 27.44 10.62 0 0 18 29.10 13.83 0 0 18 37.80 13.36 0 0 18 18.86 7.78 0 0 19 25.61 14.22 0 0 -19 22.82 13.08 0 0 19 49.58 16.34 0 0 19 20.95 11.24 0 -1 1 0.83 0.69 0 1 1 0.15 0.35 0 -1 -1 0.08 0.22 0 -1 1 2.13 1.25 0 1 -1 -0.13 0.37 0 1 1 0.35 0.39 0 1 2 4758.89 38.55 0 -1 2 5704.00 48.28 0 1 2 4875.46 44.86 0 1 -2 3752.47 39.17 0 -1 2 5244.43 46.03 0 1 2 5255.12 40.82 0 -1 2 4827.67 33.33 0 -1 -2 3758.08 38.70 0 -1 3 753.92 20.73 0 1 3 611.00 15.59 0 -1 3 693.17 20.23 0 1 3 710.89 18.83 0 1 3 727.73 15.91 0 -1 3 655.32 15.95 0 1 -3 464.32 16.43 0 -1 -3 464.64 16.29 0 1 3 666.01 19.78 0 -1 4 3109.30 49.03 0 1 4 2661.10 35.31 0 -1 4 2734.70 39.07 0 -1 -4 1883.41 38.24 0 -1 4 3304.43 48.73 0 1 -4 1758.43 19.18 0 1 4 2879.89 46.23 0 1 4 3115.37 46.09 0 1 -4 2036.04 39.39 0 1 4 3291.78 40.91 0 1 -5 38.14 3.26 0 -1 5 59.31 6.27 0 1 5 57.14 7.37 0 -1 -5 43.75 6.46 0 -1 5 67.97 8.45 0 1 5 44.27 5.22 0 -1 5 67.84 7.45 0 1 -5 39.22 6.42 0 1 5 59.45 7.66 0 1 5 66.24 6.85 0 1 6 658.37 23.83 0 1 6 495.91 17.71 0 -1 6 633.75 27.43 0 -1 6 634.65 25.96 0 1 -6 439.55 22.10 0 1 6 613.14 25.68 0 -1 6 547.89 21.64 0 -1 -6 400.22 21.64 0 1 -6 366.70 11.17 0 1 6 608.03 25.41 0 -1 7 343.95 18.14 0 1 7 410.74 23.24 0 -1 7 433.12 23.02 0 1 -7 270.05 19.06 0 1 7 264.50 14.07 0 1 7 390.65 22.27 0 -1 7 403.02 23.53 0 1 7 390.83 20.41 0 -1 -7 255.38 18.63 0 1 -7 240.66 10.00 0 1 8 2549.39 54.41 0 -1 8 2245.70 52.44 0 -1 8 2514.22 59.81 0 -1 -8 1563.62 48.87 0 -1 8 2424.54 61.57 0 1 8 1832.14 37.82 0 1 8 2420.25 59.48 0 1 -8 1612.43 49.61 0 1 -8 1401.49 25.66 0 1 8 2244.25 56.47 0 1 9 36.80 8.83 0 1 -9 18.49 3.39 0 -1 9 30.25 7.45 0 1 9 40.07 8.11 0 1 9 24.49 5.50 0 1 -9 24.19 8.03 0 -1 -9 19.53 4.94 0 -1 9 35.94 8.98 0 1 9 23.64 4.89 0 -1 9 40.53 9.17 0 -1 10 2444.39 70.15 0 1 10 1806.80 40.80 0 1 10 2545.56 69.37 0 1 -10 1759.11 58.68 0 -1 10 2350.45 60.99 0 -1 -10 1676.46 57.14 0 -1 10 2717.99 69.36 0 1 10 2764.28 64.51 0 1 10 2445.79 66.07 0 1 11 55.27 10.37 0 -1 -11 18.84 7.29 0 1 11 38.31 10.11 0 -1 11 48.64 11.37 0 -1 11 43.37 10.17 0 -1 11 41.85 9.64 0 1 -11 34.57 9.93 0 1 11 44.70 9.17 0 1 12 2355.40 66.33 0 1 -12 1494.42 59.80 0 -1 12 2058.67 63.64 0 -1 -12 1464.30 59.01 0 -1 12 2146.83 73.31 0 1 12 2004.45 66.54 0 1 12 2193.92 70.99 0 -1 12 2301.71 70.52 0 1 -13 160.69 21.13 0 1 13 215.77 21.15 0 1 13 184.85 20.19 0 -1 13 226.56 25.02 0 1 13 246.64 25.62 0 -1 13 187.09 20.07 0 -1 13 230.45 23.26 0 -1 -13 163.37 21.07 0 -1 14 6.24 4.68 0 1 14 0.29 4.99 0 -1 14 0.97 7.38 0 -1 -14 2.37 5.07 0 1 14 17.84 13.52 0 1 -14 2.90 4.24 0 -1 14 4.15 8.07 0 1 14 10.93 8.41 0 1 15 33.68 11.33 0 1 15 36.22 12.96 0 1 -15 19.69 8.14 0 1 15 38.03 10.19 0 -1 15 15.30 6.05 0 -1 15 22.12 7.99 0 -1 15 22.80 7.38 0 -1 -15 27.37 11.44 0 -1 16 1043.44 60.77 0 1 16 949.19 54.97 0 -1 -16 765.14 51.89 0 -1 16 1116.81 58.25 0 1 -16 770.91 51.79 0 1 16 1012.28 58.82 0 1 16 1099.47 54.46 0 -1 16 950.17 52.12 0 1 -17 13.39 8.27 0 -1 17 20.87 7.83 0 -1 17 31.01 14.44 0 1 17 12.54 7.94 0 1 17 12.28 10.28 0 1 17 30.58 10.36 0 -1 17 47.48 14.27 0 -1 -17 10.12 6.39 0 -1 18 909.51 55.14 0 -1 18 979.26 64.25 0 1 -18 735.81 55.35 0 1 18 974.41 55.74 0 1 18 965.45 62.52 0 -1 18 994.99 59.43 0 1 18 940.74 58.78 0 -1 -18 634.96 52.23 0 -1 19 31.77 11.24 0 1 19 64.39 18.18 0 1 -19 17.86 12.40 0 -1 19 57.06 14.80 0 1 19 45.52 15.72 0 -1 -19 41.92 14.04 0 -1 19 35.34 14.55 0 2 0 9999.00 59.48 0 2 1 4.41 1.29 0 2 -1 5.31 1.70 0 -2 1 5.86 1.81 0 2 1 6.28 1.60 0 2 -1 7.84 1.23 0 -2 1 3.37 1.00 0 -2 -1 4.52 1.87 0 2 -2 2658.58 25.85 0 -2 2 2919.02 38.64 0 2 2 2860.54 28.08 0 2 -2 2254.23 34.56 0 -2 2 2777.40 36.21 0 -2 -2 2300.76 34.23 0 2 2 2780.41 37.88 0 2 2 2526.70 35.29 0 2 3 771.20 20.92 0 -2 3 775.22 15.54 0 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996.29 48.62 0 4 12 609.99 30.05 0 -4 12 629.71 40.88 0 4 12 588.76 36.63 0 -4 12 534.70 29.95 0 4 12 438.99 27.22 0 4 12 527.68 37.01 0 4 -12 411.58 32.76 0 -4 -12 426.42 33.37 0 -4 12 572.04 39.72 0 4 13 238.47 25.39 0 -4 -13 155.09 20.75 0 -4 13 251.79 27.09 0 -4 13 212.33 20.54 0 4 13 216.20 25.20 0 -4 13 218.36 26.65 0 4 -13 171.54 21.25 0 4 13 167.62 17.27 0 4 13 211.67 19.03 0 4 14 1613.39 53.97 0 4 -14 1228.47 61.86 0 -4 14 1667.56 71.25 0 -4 -14 1114.27 58.98 0 -4 14 1452.50 54.34 0 4 14 1544.79 64.75 0 -4 14 1618.08 71.21 0 4 14 1071.79 44.63 0 4 14 1511.30 68.39 0 4 15 130.75 20.59 0 -4 15 108.73 18.41 0 -4 -15 83.17 17.24 0 4 15 91.07 17.43 0 -4 15 103.64 15.67 0 -4 15 113.61 18.04 0 4 -15 95.39 18.30 0 -4 16 63.28 14.21 0 4 16 76.84 16.32 0 -4 -16 59.39 14.85 0 4 -16 35.76 10.79 0 -4 16 74.38 17.28 0 4 16 74.07 17.52 0 -4 16 68.60 12.88 0 -4 17 13.63 9.94 0 -4 17 26.43 7.20 0 4 17 -1.28 9.34 0 -4 -17 16.18 6.74 0 4 -17 16.03 5.70 0 4 17 23.04 8.68 0 4 18 54.04 12.71 0 -4 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693.44 29.21 0 6 11 661.89 37.12 0 -6 11 777.04 46.14 0 -6 12 464.13 25.82 0 6 -12 424.93 35.02 0 6 12 529.74 32.77 0 -6 12 592.87 41.75 0 -6 12 526.69 38.92 0 6 12 523.75 39.26 0 6 12 411.89 29.97 0 -6 -12 378.00 32.39 0 6 13 417.77 31.18 0 6 13 404.45 35.95 0 -6 13 462.38 38.30 0 -6 13 376.07 24.47 0 6 -13 354.86 33.51 0 -6 13 480.72 39.44 0 -6 -13 304.08 30.36 0 6 13 340.38 28.28 0 6 14 1180.66 63.32 0 6 14 1156.44 54.12 0 -6 -14 914.93 54.29 0 6 -14 929.64 55.81 0 -6 14 1214.85 65.56 0 6 14 910.00 45.96 0 -6 14 1240.12 64.97 0 -6 -15 202.42 26.70 0 -6 15 278.37 32.98 0 -6 15 240.11 28.76 0 6 15 247.76 29.60 0 6 15 171.81 21.04 0 6 15 240.51 26.29 0 6 -15 205.39 28.09 0 6 -16 15.62 8.24 0 6 16 10.39 9.05 0 -6 16 36.72 11.20 0 -6 16 12.65 7.59 0 -6 -16 8.84 7.72 0 6 16 9.21 7.53 0 6 17 296.24 35.06 0 -6 -17 254.22 32.40 0 6 -17 251.34 31.75 0 6 17 281.29 31.19 0 -6 17 296.69 36.47 0 -6 17 327.48 37.10 0 -6 18 28.14 12.99 0 -6 -18 16.68 10.10 0 6 18 5.73 6.88 0 6 -18 19.13 11.42 0 -6 18 25.50 13.32 0 6 18 17.05 8.47 0 7 0 5.68 3.03 0 -7 0 4.55 3.30 0 -7 0 1.87 1.35 0 -7 0 2.54 2.06 0 7 0 8.16 3.34 0 7 -1 3017.77 62.06 0 7 1 3249.67 56.33 0 -7 -1 3294.72 43.56 0 7 -1 2912.37 63.10 0 7 1 3124.74 65.07 0 -7 1 2983.42 42.28 0 7 -1 3009.15 44.98 0 -7 1 3318.28 55.55 0 -7 -1 3154.22 66.05 0 -7 -2 367.09 22.89 0 -7 -2 352.97 11.97 0 7 -2 378.62 21.03 0 7 2 365.75 22.60 0 7 -2 377.86 14.54 0 -7 2 392.04 20.94 0 7 -2 339.06 22.21 0 7 2 375.34 20.43 0 7 -3 109.51 11.33 0 -7 -3 103.19 11.66 0 7 3 103.76 12.83 0 7 -3 99.49 6.85 0 7 -3 100.24 12.61 0 -7 3 114.77 13.22 0 7 3 89.51 10.86 0 -7 3 93.12 10.73 0 7 -4 1568.94 40.91 0 7 4 1663.79 48.76 0 -7 4 1597.22 49.07 0 7 -4 1385.65 47.01 0 -7 -4 1446.58 47.49 0 7 4 1380.59 24.84 0 7 4 1466.71 48.81 0 -7 4 1166.54 21.92 0 -7 5 369.43 25.63 0 7 -5 356.81 18.79 0 7 5 322.86 14.13 0 -7 5 268.78 10.73 0 -7 -5 356.25 24.62 0 7 5 334.22 23.88 0 7 -5 284.97 22.13 0 7 5 355.74 23.70 0 7 -6 563.76 32.40 0 -7 -6 669.08 34.68 0 7 6 709.30 35.59 0 7 6 736.16 35.97 0 7 6 685.99 23.29 0 7 -6 695.33 25.49 0 -7 6 710.73 36.09 0 -7 7 1956.89 60.83 0 7 7 2087.88 63.88 0 7 -7 1615.10 57.38 0 -7 7 2128.53 65.99 0 7 7 1868.44 59.17 0 -7 -7 1816.26 59.31 0 7 -7 2025.48 41.66 0 7 7 1964.88 43.86 0 -7 -8 124.20 16.45 0 7 -8 109.86 15.19 0 7 8 131.06 12.42 0 -7 8 130.01 17.06 0 7 8 114.51 15.07 0 -7 8 143.79 17.84 0 7 8 136.59 17.02 0 7 9 238.44 17.64 0 -7 9 254.94 24.02 0 7 9 217.67 21.08 0 7 9 234.50 24.05 0 -7 -9 199.61 21.13 0 -7 9 292.48 26.65 0 7 -9 203.37 21.81 0 7 10 368.33 24.22 0 -7 -10 324.38 28.04 0 7 10 433.01 33.29 0 -7 10 441.33 33.65 0 -7 10 399.14 31.43 0 7 10 359.69 28.05 0 7 -10 306.75 28.29 0 -7 11 7.07 6.52 0 7 -11 8.93 4.69 0 7 11 4.85 4.40 0 7 11 8.31 5.60 0 -7 -11 7.84 5.31 0 -7 11 10.07 6.72 0 7 11 7.25 6.30 0 7 12 175.33 18.61 0 7 -12 154.86 20.96 0 -7 12 175.58 23.74 0 7 12 138.69 18.72 0 -7 -12 138.32 18.15 0 7 12 194.13 24.03 0 -7 12 179.23 22.06 0 7 13 1208.54 51.91 0 7 13 1027.76 50.98 0 7 -13 992.85 57.44 0 -7 13 1311.21 66.12 0 7 13 1205.32 63.03 0 -7 -13 1011.24 56.20 0 -7 13 1296.43 64.74 0 -7 -14 95.41 17.76 0 -7 14 140.62 23.09 0 7 14 133.51 19.51 0 -7 14 135.77 22.62 0 7 14 85.86 15.94 0 7 -14 101.85 19.38 0 7 14 129.31 22.68 0 -7 15 795.59 54.76 0 7 15 708.19 52.09 0 7 15 719.46 44.21 0 7 15 547.51 38.74 0 -7 -15 476.04 43.22 0 7 -15 638.27 49.16 0 -7 15 815.16 55.76 0 7 -16 278.27 33.91 0 -7 -16 280.45 32.36 0 -7 16 364.76 37.95 0 7 16 299.45 34.24 0 -7 16 323.14 36.80 0 7 16 349.93 32.45 0 7 17 8.63 12.16 0 -7 17 12.66 8.87 0 -7 17 -7.39 9.75 0 7 17 -5.90 10.77 0 7 -17 22.47 14.13 0 -7 -17 0.20 5.23 0 -8 0 67.41 10.16 0 8 0 57.71 9.27 0 8 0 65.89 7.88 0 -8 0 72.73 8.21 0 -8 0 57.17 5.39 0 -8 1 1597.95 32.42 0 -8 -1 1689.13 34.00 0 8 1 1656.83 42.88 0 -8 -1 1757.80 52.70 0 8 1 1529.19 49.28 0 8 -1 1594.37 48.49 0 8 -1 1580.84 35.53 0 8 2 43.70 7.41 0 -8 -2 26.97 3.93 0 -8 2 25.21 5.88 0 -8 2 26.28 6.79 0 8 2 38.47 7.82 0 8 -2 29.58 7.92 0 8 -2 28.30 6.64 0 8 -2 27.72 4.54 0 -8 -2 34.83 7.51 0 -8 3 2302.43 56.38 0 8 3 2124.69 54.94 0 -8 -3 2113.67 59.27 0 8 3 2049.84 59.11 0 8 -3 1894.96 32.43 0 8 -3 2086.24 52.55 0 8 -3 1831.49 56.60 0 -8 4 4.77 4.18 0 -8 4 7.72 2.78 0 -8 -4 6.31 4.45 0 8 -4 1.01 2.57 0 8 -4 4.68 3.46 0 -8 4 2.54 1.31 0 8 4 1.67 4.01 0 8 4 -3.16 4.34 0 8 5 1228.78 46.15 0 8 -5 1145.10 36.85 0 8 -5 1031.09 44.28 0 8 5 1040.39 45.25 0 -8 5 1195.64 45.98 0 -8 -5 1099.99 44.93 0 -8 6 706.18 37.61 0 8 -6 557.39 33.65 0 8 6 624.70 35.29 0 8 6 648.19 35.87 0 -8 6 622.67 33.44 0 8 6 609.96 20.93 0 -8 -6 629.95 35.48 0 8 -6 731.59 28.57 0 8 -7 64.52 8.62 0 -8 -7 61.28 12.40 0 -8 7 64.35 11.84 0 -8 7 93.79 14.98 0 8 7 68.11 8.09 0 8 7 69.13 12.89 0 8 7 63.17 11.35 0 8 -7 49.16 10.05 0 8 8 862.64 44.67 0 -8 8 912.12 46.50 0 8 8 824.42 30.30 0 8 -8 829.43 28.26 0 -8 -8 766.63 41.84 0 8 -8 666.37 40.06 0 -8 8 867.80 42.03 0 8 8 794.78 41.67 0 8 9 639.24 29.16 0 -8 -9 615.99 39.08 0 -8 9 654.01 39.84 0 8 -9 568.21 38.17 0 8 9 587.54 37.59 0 8 9 687.44 41.10 0 -8 9 706.60 43.25 0 -8 10 10.91 8.25 0 8 10 4.20 8.81 0 -8 -10 8.83 6.41 0 8 10 0.11 5.23 0 -8 10 4.79 7.99 0 8 -10 7.80 4.47 0 8 10 4.58 5.11 0 -8 -11 724.15 45.04 0 -8 11 923.76 50.32 0 8 11 827.03 50.01 0 8 11 868.32 38.55 0 -8 11 973.18 53.45 0 8 11 815.05 44.95 0 8 -11 765.89 47.46 0 8 12 198.82 19.66 0 -8 12 209.32 24.71 0 -8 12 233.51 27.30 0 8 12 177.11 21.55 0 8 -12 179.06 23.97 0 8 12 189.92 23.02 0 -8 -12 149.03 21.55 0 8 13 272.42 30.65 0 -8 13 330.16 32.99 0 -8 13 350.29 34.18 0 8 13 305.18 25.46 0 8 -13 253.04 29.56 0 8 13 260.53 25.90 0 -8 -13 245.91 27.30 0 8 14 427.85 39.12 0 -8 -14 332.36 34.77 0 -8 14 413.79 39.30 0 8 14 370.30 29.88 0 -8 14 414.07 39.91 0 8 -14 339.44 34.65 0 8 14 337.53 30.79 0 -8 15 333.42 35.74 0 8 15 299.14 34.67 0 -8 15 255.52 33.02 0 8 -15 236.08 31.11 0 8 15 197.47 24.36 0 -8 -15 234.02 30.24 0 8 15 284.69 27.69 0 8 -16 33.13 11.05 0 -8 16 30.54 14.91 0 -8 -16 26.79 10.09 0 8 16 48.94 13.95 0 -8 16 42.00 14.54 0 8 16 34.36 12.53 0 -8 17 557.43 51.27 0 -8 17 544.60 49.49 0 8 17 529.71 50.57 0 -8 -17 430.32 44.26 0 8 -17 447.57 45.37 0 9 0 8.86 5.50 0 9 0 6.61 2.99 0 -9 0 5.17 2.78 0 -9 0 4.08 4.06 0 -9 0 1.53 2.38 0 9 1 3354.15 78.78 0 9 1 3602.13 66.26 0 -9 1 3575.88 81.22 0 -9 -1 3512.40 80.38 0 -9 1 3463.38 49.49 0 -9 1 3739.12 65.92 0 9 -1 3591.01 76.34 0 9 -1 3450.91 56.01 0 -9 -1 3678.27 53.93 0 9 -2 397.08 25.13 0 -9 -2 411.06 15.46 0 9 -2 412.55 27.76 0 -9 -2 434.67 28.02 0 -9 2 433.56 19.85 0 9 -2 427.72 18.17 0 9 2 436.73 24.23 0 9 2 428.26 28.21 0 -9 3 14.89 6.71 0 -9 -3 23.23 8.09 0 9 -3 19.99 4.76 0 9 -3 25.99 6.57 0 9 3 25.34 5.86 0 9 -3 19.06 5.81 0 9 3 13.79 6.05 0 -9 3 11.46 5.03 0 -9 -4 598.14 34.38 0 -9 4 576.06 28.01 0 9 4 629.61 33.23 0 9 4 604.33 35.12 0 -9 4 601.65 33.40 0 9 -4 555.06 33.28 0 9 -4 615.15 29.69 0 -9 5 1013.51 38.94 0 9 -5 986.45 37.24 0 -9 5 1099.50 45.22 0 -9 -5 999.36 45.44 0 9 -5 917.92 43.80 0 9 5 1028.17 46.39 0 9 5 1053.86 44.81 0 9 -6 64.96 9.05 0 9 -6 63.00 12.56 0 -9 -6 66.79 12.01 0 9 6 84.89 12.62 0 9 6 69.97 11.95 0 -9 6 69.87 12.68 0 -9 6 72.28 11.28 0 9 -7 1743.64 65.25 0 9 -7 2130.54 51.51 0 9 7 2216.82 71.02 0 -9 7 2253.45 72.42 0 -9 -7 2008.38 67.89 0 -9 7 2207.93 64.60 0 9 7 2013.33 68.15 0 9 -8 4.34 1.97 0 9 -8 2.87 5.73 0 -9 8 0.16 5.72 0 -9 8 16.31 8.18 0 -9 -8 0.37 3.79 0 9 8 -1.03 7.82 0 9 8 -1.05 6.67 0 -9 9 227.03 25.75 0 -9 -9 191.43 24.00 0 9 9 218.96 23.47 0 9 9 220.55 23.81 0 9 -9 190.36 22.26 0 -9 9 201.49 23.44 0 9 10 6.67 5.27 0 -9 10 18.42 8.87 0 9 10 6.20 10.09 0 9 -10 12.36 5.55 0 -9 10 5.94 4.87 0 -9 -10 11.84 8.49 0 -9 11 -5.33 7.61 0 9 -11 -1.04 9.06 0 9 11 1.27 5.10 0 -9 11 6.47 8.05 0 9 11 -11.24 12.28 0 -9 -11 -6.21 9.88 0 9 12 -9.63 12.96 0 -9 -12 1.49 5.29 0 -9 12 -6.70 8.46 0 9 -12 -8.62 11.12 0 9 12 9.39 6.82 0 -9 12 9.84 6.63 0 -9 13 866.66 55.20 0 -9 -13 757.69 51.94 0 9 -13 751.15 51.52 0 9 13 755.23 48.32 0 -9 13 965.78 58.58 0 9 13 832.83 55.28 0 9 -14 44.80 13.87 0 -9 -14 35.89 12.50 0 9 14 42.32 12.93 0 9 14 31.08 12.75 0 -9 14 48.33 11.45 0 -9 14 60.24 16.91 0 -9 15 932.09 62.73 0 9 15 853.33 60.36 0 9 15 683.31 46.96 0 -9 15 911.77 61.09 0 -9 -15 746.65 53.63 0 9 -15 742.17 54.81 0 -9 16 105.45 21.81 0 9 16 77.63 16.78 0 9 -16 75.44 17.18 0 9 16 94.05 22.78 0 -9 -16 92.32 20.58 0 -9 16 119.27 22.18 0 -10 0 12.48 4.85 0 -10 0 8.23 2.05 0 10 0 11.06 6.06 0 10 0 1.77 3.97 0 -10 1 1454.47 55.12 0 -10 -1 1517.95 37.29 0 10 -1 1546.41 54.23 0 10 1 1507.05 45.03 0 -10 -1 1533.40 56.83 0 10 1 1536.04 55.44 0 10 -1 1483.65 39.13 0 -10 1 1453.43 33.07 0 -10 2 43.17 6.70 0 10 2 45.36 10.24 0 -10 -2 43.70 8.73 0 10 -2 46.34 9.89 0 -10 -2 34.23 4.42 0 -10 2 48.17 9.17 0 10 -2 43.04 6.41 0 10 2 37.53 7.41 0 10 3 3162.67 82.65 0 10 -3 3443.64 76.87 0 -10 3 3293.87 61.25 0 -10 -3 3302.24 83.58 0 10 -3 2926.36 79.29 0 10 3 3347.80 75.77 0 10 4 151.41 18.25 0 -10 4 145.89 15.66 0 -10 -4 147.04 18.21 0 10 4 150.62 17.68 0 10 -4 139.92 17.78 0 10 -4 175.48 17.10 0 10 5 1350.72 57.47 0 -10 5 1613.03 56.80 0 -10 -5 1448.19 57.24 0 10 -5 1569.91 49.93 0 -10 5 1579.45 50.07 0 10 -5 1269.09 55.16 0 10 5 1512.15 56.54 0 10 6 255.30 24.74 0 -10 6 249.41 20.80 0 -10 -6 231.49 23.92 0 10 -6 262.44 20.83 0 10 6 273.26 23.67 0 10 -6 228.40 23.81 0 -10 6 292.34 25.62 0 -10 7 18.36 5.28 0 10 7 27.55 10.40 0 -10 -7 16.81 6.10 0 -10 7 12.56 7.82 0 10 -7 23.46 9.10 0 10 7 3.68 4.95 0 10 -7 8.80 2.38 0 10 -8 8.68 4.16 0 -10 8 3.04 5.76 0 -10 8 10.85 5.29 0 10 8 4.79 5.71 0 10 8 10.20 7.25 0 10 -8 0.59 3.97 0 -10 -8 6.52 4.97 0 -10 -9 746.88 46.43 0 10 9 725.03 44.81 0 -10 9 860.57 45.79 0 10 9 814.97 48.82 0 10 -9 678.29 44.21 0 -10 9 911.86 50.77 0 10 10 15.25 5.00 0 -10 10 13.59 4.81 0 10 10 25.38 5.86 0 -10 -10 18.12 8.44 0 10 -10 6.07 3.68 0 -10 10 6.70 5.87 0 -10 11 1091.64 56.29 0 -10 -11 935.72 54.40 0 10 11 979.10 54.27 0 -10 11 1193.14 63.30 0 10 11 1127.52 61.73 0 10 -11 972.99 56.36 0 10 12 -4.49 8.22 0 -10 -12 -0.53 9.06 0 -10 12 -10.15 8.40 0 -10 12 1.60 6.22 0 10 -12 -1.08 7.99 0 10 12 -7.85 10.77 0 -10 13 372.98 38.08 0 10 13 380.24 38.20 0 10 -13 311.25 34.32 0 10 13 284.43 30.64 0 -10 13 392.66 37.82 0 -10 -13 333.76 35.37 0 10 -14 27.34 10.21 0 -10 14 9.56 7.33 0 -10 -14 1.37 9.71 0 10 14 12.14 8.61 0 -10 14 29.32 14.17 0 10 14 21.78 10.29 0 -10 15 507.68 48.10 0 -10 -15 383.60 39.13 0 -10 15 483.69 45.64 0 10 15 353.21 35.84 0 10 15 446.25 44.66 0 10 -15 387.88 42.11 0 -10 16 108.25 23.33 0 10 -16 69.65 16.59 0 -10 -16 61.53 15.58 0 -10 16 76.35 18.49 0 10 16 57.59 16.97 0 10 16 55.11 14.92 0 -11 0 8.48 2.99 0 -11 0 4.53 5.14 0 11 0 3.43 3.04 0 11 0 -4.21 5.97 0 11 -1 1498.92 57.23 0 11 -1 1541.91 41.98 0 -11 1 1569.67 47.68 0 -11 1 1533.19 34.95 0 -11 -1 1595.97 60.95 0 -11 1 1588.84 60.96 0 -11 -1 1534.66 39.01 0 11 1 1566.58 48.04 0 11 1 1544.76 59.19 0 11 -2 7.36 3.46 0 -11 2 4.16 3.71 0 -11 2 -4.37 6.42 0 11 2 4.57 4.38 0 -11 -2 2.88 3.75 0 11 -2 -4.21 5.77 0 -11 2 0.23 4.43 0 11 2 8.48 2.76 0 -11 3 23.41 5.80 0 11 3 21.93 8.38 0 -11 -3 34.67 10.69 0 -11 3 29.15 7.72 0 11 -3 17.22 7.62 0 11 3 28.70 6.73 0 11 -3 20.82 7.56 0 11 4 4.67 7.03 0 -11 4 10.87 3.47 0 11 4 13.19 4.81 0 -11 -4 9.06 4.00 0 11 -4 1.46 5.42 0 -11 4 5.98 5.28 0 11 -4 10.21 5.58 0 -11 5 1270.72 52.18 0 -11 -5 1179.91 54.37 0 11 -5 1284.23 48.29 0 11 -5 1090.76 52.94 0 11 5 1282.92 53.09 0 11 5 1233.59 56.24 0 -11 -6 41.31 10.02 0 11 6 39.33 11.09 0 -11 6 37.88 9.98 0 -11 6 34.46 9.90 0 11 -6 25.83 7.09 0 11 6 22.66 7.62 0 11 -6 13.39 4.20 0 11 7 2956.49 90.90 0 11 7 2991.72 88.65 0 11 -7 2453.77 83.43 0 -11 7 3218.57 90.62 0 -11 7 2927.81 77.38 0 11 -7 3000.37 70.70 0 -11 -7 2881.75 88.30 0 11 -8 83.02 15.84 0 11 8 83.01 16.12 0 -11 8 132.50 20.32 0 -11 8 103.57 15.60 0 11 8 110.02 16.68 0 -11 -8 113.95 18.03 0 11 -8 83.46 11.67 0 -11 -9 507.38 39.62 0 11 9 492.20 38.13 0 11 9 577.25 41.60 0 -11 9 535.76 37.60 0 11 -9 486.14 38.56 0 -11 9 527.06 41.17 0 -11 -10 37.19 13.13 0 -11 10 15.64 6.05 0 11 10 5.11 4.18 0 -11 10 25.16 6.86 0 11 10 16.43 6.38 0 11 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180.25 29.04 -2 10 -16 109.78 23.54 2 10 16 137.35 24.68 2 -10 -16 129.31 23.18 2 -11 15 621.51 52.27 2 11 -15 461.26 45.03 -2 11 15 566.49 52.82 -2 11 15 417.10 41.96 -2 -11 -15 454.50 44.70 2 -11 15 615.69 54.02 2 -11 14 93.55 19.44 2 -11 14 105.66 21.80 -2 -11 -14 72.37 17.78 2 11 -14 69.19 16.72 -2 11 14 108.94 22.13 -2 11 14 66.66 18.02 -2 11 13 1018.10 64.84 2 11 -13 819.85 57.49 2 -11 13 982.70 60.55 -2 11 13 845.99 56.03 2 -11 13 1062.09 66.33 -2 -11 -13 805.16 57.85 2 -11 12 29.14 11.59 2 -11 12 16.97 9.65 -2 -11 -12 5.62 8.21 2 11 -12 10.58 5.64 -2 11 12 23.02 11.74 -2 11 12 20.54 9.90 2 -11 11 142.50 23.40 -2 11 11 160.45 24.22 -2 11 11 113.68 19.04 -2 -11 -11 142.46 22.60 2 -11 11 150.78 23.15 2 11 -11 139.39 23.56 -2 -11 -10 16.91 9.64 2 -11 10 28.94 11.91 -2 11 10 25.03 9.34 2 -11 10 35.51 9.10 2 11 -10 14.36 6.07 -2 11 10 25.75 9.97 -2 11 9 319.87 32.14 -2 -11 -9 311.37 32.85 2 11 -9 327.62 24.23 2 11 -9 302.43 31.17 -2 11 9 332.35 33.02 2 -11 9 354.71 33.48 -2 11 8 250.73 27.01 2 -11 8 238.62 28.04 2 11 -8 199.59 24.88 -2 -11 -8 236.34 27.31 -2 11 8 228.16 26.52 2 11 -8 227.52 20.59 2 11 -7 1783.74 71.14 2 -11 7 2077.55 75.49 2 -11 7 1933.00 67.63 2 11 -7 2070.35 63.08 -2 -11 -7 1970.15 76.11 -2 11 7 2213.58 77.42 -2 11 7 1908.36 76.10 -2 -11 -6 130.41 19.33 2 -11 6 130.51 19.49 -2 11 6 144.78 20.78 2 11 -6 143.04 16.93 -2 11 6 154.56 21.13 2 -11 6 114.44 17.63 2 11 -6 141.21 19.67 -2 11 5 495.48 37.32 2 11 -5 462.42 35.21 -2 11 5 577.59 37.14 2 -11 5 426.60 22.93 2 -11 5 588.21 35.44 2 -11 5 527.01 31.10 -2 -11 -5 549.44 38.86 2 11 -5 520.57 32.88 2 -11 4 19.33 4.81 -2 11 4 17.82 6.10 2 -11 4 12.58 7.22 2 11 -4 18.06 4.32 -2 -11 -4 13.27 6.21 2 11 -4 23.59 8.28 -2 11 4 13.68 7.19 2 11 -3 295.78 25.10 -2 11 3 317.13 25.30 2 -11 3 300.88 21.75 -2 -11 -3 325.80 28.87 -2 11 3 311.82 28.73 -2 11 2 59.86 10.93 2 11 -2 56.37 10.35 -2 11 2 58.31 11.70 -2 -11 -2 74.06 13.89 2 -11 2 43.00 10.64 -2 -11 -2 48.80 6.97 2 -11 2 59.42 9.44 -2 11 1 2735.39 69.00 2 -11 1 2747.55 78.63 2 11 -1 2687.47 77.65 -2 -11 -1 2884.28 83.60 -2 11 1 2924.75 53.82 -2 11 1 2749.12 79.20 2 -11 1 2878.87 65.85 -2 -11 -1 2569.58 54.37 2 -11 0 52.07 10.52 -2 -11 0 44.23 11.37 2 11 0 42.67 7.20 -2 -11 0 53.69 9.44 2 -11 0 50.93 8.78 2 -11 0 31.58 5.95 -2 11 0 40.93 9.23 -2 11 0 50.11 12.81 2 11 0 39.56 9.47 -2 11 -1 2635.05 62.62 2 -11 -1 2340.77 50.03 2 -11 -1 2719.81 77.25 -2 11 -1 2674.45 74.35 2 11 1 2522.70 59.58 2 11 1 2589.34 77.46 -2 -11 1 2555.76 79.92 -2 -11 1 2577.83 62.66 -2 11 -2 61.23 9.81 2 -11 -2 46.72 6.64 -2 11 -2 43.01 10.19 2 11 2 43.56 10.21 2 -11 -2 55.57 10.92 2 11 2 41.21 6.84 -2 -11 2 39.94 8.60 -2 11 -2 49.27 9.72 -2 -11 2 48.17 9.27 2 11 3 290.01 27.55 -2 -11 3 301.43 18.64 -2 -11 3 296.40 26.34 -2 11 -3 315.08 20.32 2 11 3 306.57 22.84 -2 11 -3 293.51 24.59 -2 11 -3 292.90 26.62 2 -11 -3 311.91 26.01 -2 -11 3 326.81 25.95 -2 -11 4 17.15 5.21 -2 11 -4 13.28 5.24 2 11 4 13.01 5.75 -2 11 -4 21.91 4.45 2 11 4 3.38 5.09 -2 -11 4 9.34 4.96 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112.07 20.64 2 11 12 8.99 8.22 -2 11 -12 22.22 10.27 -2 -11 12 25.13 10.20 2 11 12 21.13 11.88 2 -11 -12 14.22 8.08 -2 -11 12 27.69 12.59 -2 -11 13 1211.63 67.39 2 11 13 1083.76 67.57 -2 11 -13 923.97 61.74 2 -11 -13 984.20 59.07 2 11 13 969.01 58.72 -2 -11 13 1280.68 71.24 2 11 14 60.37 14.83 -2 -11 14 104.26 21.82 -2 -11 14 125.19 25.50 -2 11 -14 76.86 19.24 2 -11 -14 68.80 12.76 2 11 14 85.70 19.28 -2 -11 15 618.78 51.62 2 11 15 619.57 53.31 2 -11 -15 515.25 45.72 -2 11 -15 523.76 49.50 2 11 15 458.59 41.71 -2 -11 15 619.12 55.11 -2 -12 -14 48.24 15.93 -2 12 14 31.19 12.79 2 -12 14 22.53 10.66 -2 12 14 29.32 11.90 2 12 -14 31.68 15.84 2 -12 14 53.39 19.74 -2 12 13 350.32 38.76 2 -12 13 306.40 35.59 -2 -12 -13 278.91 34.57 2 12 -13 261.58 33.56 2 -12 13 364.23 40.05 -2 12 13 245.82 31.79 2 12 -12 20.64 11.86 2 -12 12 29.16 13.25 -2 12 12 14.44 11.98 -2 12 12 19.52 9.87 -2 -12 -12 18.93 6.73 2 -12 12 24.32 9.03 -2 12 11 1301.22 69.80 -2 -12 -11 1111.09 65.63 2 -12 11 1291.37 70.62 2 12 -11 1077.04 63.43 -2 12 11 1069.21 62.88 2 -12 11 1145.66 63.17 2 -12 10 21.40 7.74 -2 12 10 12.89 4.80 -2 -12 -10 26.90 12.89 -2 12 10 24.75 10.48 2 12 -10 35.49 11.69 2 -12 10 18.08 9.06 2 -12 9 1194.64 59.12 -2 12 9 1131.33 63.03 -2 -12 -9 1165.99 64.02 -2 12 9 1335.62 67.71 2 -12 9 1275.87 65.52 2 12 -9 1098.36 61.32 -2 12 8 83.43 16.98 2 -12 8 66.91 13.65 -2 -12 -8 73.78 17.06 -2 12 8 68.52 15.01 2 12 -8 62.42 13.91 2 -12 8 89.68 17.70 -2 -12 -7 31.57 9.45 2 -12 7 40.82 13.01 2 12 -7 34.32 11.19 -2 12 7 35.88 12.73 -2 12 7 40.03 11.49 2 -12 7 27.57 7.51 2 12 -7 31.37 8.01 -2 12 6 106.23 18.49 2 -12 6 118.66 19.50 -2 -12 -6 128.33 20.25 2 12 -6 121.51 15.80 -2 12 6 118.88 18.12 2 -12 6 139.88 17.33 2 12 -6 100.81 15.26 -2 -12 -5 1025.83 55.31 2 12 -5 922.61 51.15 2 12 -5 1072.37 48.84 -2 12 5 1079.45 52.71 2 -12 5 977.04 45.04 -2 12 5 985.26 54.66 2 12 -4 49.64 10.49 -2 12 4 59.23 13.54 -2 -12 -4 46.84 11.34 -2 12 4 46.13 11.81 2 -12 4 40.91 10.93 2 -12 4 38.54 8.50 -2 12 3 1716.98 69.29 -2 12 3 1858.99 63.71 2 12 -3 1751.02 64.55 2 -12 3 1761.14 52.58 -2 -12 -3 1841.95 71.39 2 -12 2 161.84 19.57 2 -12 2 160.97 16.73 2 12 -2 155.51 20.07 -2 12 2 157.06 21.19 2 -12 2 156.88 15.27 -2 12 2 159.58 17.67 -2 -12 -2 174.74 22.12 -2 -12 -1 412.25 33.58 -2 12 1 369.38 26.46 2 -12 1 376.47 24.58 2 12 -1 364.76 30.43 2 -12 1 370.55 30.48 2 -12 1 301.69 19.27 -2 12 1 391.66 32.18 -2 -12 -1 359.95 21.73 2 12 0 33.27 9.58 -2 -12 0 55.01 11.91 2 12 0 33.37 6.75 2 -12 0 46.52 9.62 2 -12 0 38.26 7.78 -2 12 0 42.42 7.51 -2 -12 0 43.06 8.27 -2 12 0 43.07 11.63 2 -12 0 27.19 5.71 2 12 1 316.93 21.45 2 -12 -1 300.80 19.08 -2 -12 1 347.90 24.25 -2 12 -1 322.92 23.58 -2 -12 1 331.05 30.20 2 -12 -1 374.23 30.37 2 12 1 330.36 29.60 -2 12 -1 300.90 27.56 2 -12 -2 179.53 20.92 -2 -12 2 165.92 17.63 2 12 2 166.24 21.32 -2 12 -2 161.78 16.07 -2 -12 2 162.74 20.20 2 12 2 156.70 16.60 -2 12 -2 150.16 20.01 2 -12 -3 1587.53 62.93 -2 12 -3 1560.08 46.57 2 12 3 1528.11 64.90 -2 -12 3 1584.01 65.35 -2 12 -3 1634.23 59.28 2 12 3 1628.34 55.31 -2 -12 3 1724.43 58.50 -2 12 -3 1401.23 60.27 -2 12 -4 35.68 8.94 -2 -12 4 32.98 8.19 -2 12 -4 24.68 8.10 2 12 4 18.57 5.30 2 12 4 19.30 7.22 2 -12 -4 28.31 8.43 -2 -12 4 26.49 9.60 2 12 5 991.01 53.68 -2 -12 5 1044.90 40.89 2 12 5 1060.11 48.68 2 -12 -5 1050.51 52.29 -2 12 -5 1006.65 44.95 -2 -12 5 1055.90 50.29 -2 12 -5 937.54 51.23 -2 12 -6 101.14 18.12 2 12 6 101.40 17.08 2 12 6 129.31 17.69 2 -12 -6 131.36 18.69 -2 12 -6 116.99 14.58 -2 -12 6 131.44 16.64 -2 -12 6 135.58 18.87 -2 12 -7 17.53 7.25 -2 -12 7 35.63 10.67 -2 12 -7 23.75 8.79 2 12 7 22.85 5.74 -2 -12 7 23.75 9.16 2 12 7 12.57 6.06 2 -12 -7 34.35 10.15 -2 -12 8 69.07 14.05 2 12 8 36.43 10.00 2 -12 -8 70.87 15.39 -2 12 -8 56.06 13.46 -2 -12 8 67.88 13.22 2 12 8 55.70 11.92 -2 -12 9 1143.52 54.51 2 -12 -9 1071.94 56.71 2 12 9 995.70 57.57 2 12 9 1078.39 59.29 -2 12 -9 973.02 58.08 -2 -12 9 1139.52 61.49 2 12 10 8.66 7.33 2 -12 -10 3.76 5.43 2 12 10 -0.95 8.43 -2 -12 10 9.90 11.01 -2 -12 10 8.98 5.26 -2 12 -10 -3.64 9.90 -2 -12 11 1325.85 65.21 2 12 11 1392.32 71.36 -2 12 -11 1078.39 63.72 2 -12 -11 1154.08 63.04 2 12 11 1175.93 65.38 -2 -12 11 1379.97 72.18 -2 -12 12 33.11 13.32 -2 12 -12 27.70 8.95 2 12 12 11.40 5.18 2 12 12 23.59 10.57 -2 -12 12 41.55 9.53 2 -12 -12 18.20 6.42 -2 -12 13 367.88 38.42 2 -12 -13 258.88 31.89 -2 12 -13 307.39 36.43 2 12 13 368.20 40.61 -2 -12 13 422.88 42.35 2 12 13 304.58 34.33 -2 -12 14 41.38 16.82 -2 12 -14 31.70 10.23 2 12 14 47.50 14.09 2 -12 -14 53.32 15.10 2 12 14 52.93 17.05 -2 -12 14 40.54 12.37 2 13 -13 588.98 51.59 -2 -13 -13 598.48 52.53 2 -13 13 680.36 53.77 -2 13 13 608.45 52.07 2 -13 13 640.42 54.80 -2 13 13 653.24 54.79 2 -13 12 116.69 23.05 -2 13 12 102.41 23.43 2 -13 12 99.70 22.79 -2 -13 -12 99.12 20.72 -2 13 12 70.31 17.60 2 13 -12 71.08 18.15 2 13 -11 98.09 19.44 -2 -13 -11 65.48 18.11 -2 13 11 95.80 19.68 -2 13 11 82.56 19.10 2 -13 11 96.07 16.94 2 -13 11 100.95 22.94 2 -13 10 110.19 18.89 -2 13 10 70.24 15.74 -2 13 10 107.18 19.71 -2 -13 -10 141.69 24.03 2 13 -10 92.85 18.69 2 -13 10 125.64 22.87 -2 13 9 271.46 30.88 -2 -13 -9 259.46 30.90 2 -13 9 306.77 33.99 2 13 -9 265.30 31.22 -2 13 9 304.99 34.08 2 -13 9 317.05 30.28 -2 13 8 62.23 16.71 2 13 -8 41.40 11.28 -2 13 8 56.25 13.84 2 -13 8 48.94 11.53 -2 -13 -8 52.60 14.41 2 13 -8 46.69 14.19 2 -13 8 72.30 16.03 2 -13 7 974.22 56.68 2 -13 7 955.23 50.27 2 13 -7 1085.43 50.76 -2 13 7 968.48 58.26 -2 13 7 1098.66 58.00 2 13 -7 948.51 56.00 -2 -13 -7 998.31 59.15 2 -13 6 87.63 13.69 2 13 -6 116.03 18.51 2 13 -6 94.29 18.33 -2 -13 -6 138.42 20.84 2 -13 6 115.59 18.05 -2 13 6 110.30 17.98 -2 13 6 110.59 19.58 -2 13 5 480.32 36.43 2 -13 5 409.32 29.15 2 13 -5 441.80 33.46 -2 13 5 478.86 39.57 -2 -13 -5 450.48 38.44 -2 13 4 128.00 20.53 -2 -13 -4 119.99 20.81 2 13 -4 119.42 18.29 2 -13 4 142.26 16.10 -2 13 4 127.66 16.69 2 -13 4 119.82 18.48 2 13 -3 113.92 17.55 -2 -13 -3 120.14 19.75 -2 13 3 108.41 15.88 -2 13 3 131.64 21.21 2 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4 151.74 22.28 -2 -13 4 166.87 20.73 -2 -13 5 451.62 27.70 -2 -13 5 468.89 34.77 -2 13 -5 407.48 34.62 2 13 5 408.13 36.72 2 13 5 430.41 33.17 -2 13 -5 423.38 31.10 2 -13 -5 498.11 38.32 2 -13 -6 156.77 22.06 -2 -13 6 181.00 18.78 -2 -13 6 168.24 22.95 2 13 6 164.92 21.33 2 13 6 132.89 20.29 -2 13 -6 123.65 15.95 -2 13 -6 143.42 22.04 -2 13 -7 915.78 55.14 2 13 7 907.03 55.22 2 13 7 1023.15 54.91 -2 -13 7 1053.94 47.20 -2 -13 7 1099.79 57.63 -2 13 -7 942.86 43.68 2 -13 -7 968.73 53.87 -2 -13 8 71.85 16.80 -2 13 -8 37.49 11.56 2 -13 -8 60.56 13.86 2 13 8 31.65 6.34 2 13 8 41.49 11.41 -2 -13 8 64.19 13.83 -2 13 -9 300.06 32.98 -2 -13 9 313.42 29.92 2 -13 -9 308.47 31.84 2 13 9 302.40 33.24 2 13 9 321.84 32.90 -2 -13 9 284.17 33.81 2 13 10 124.22 22.34 2 -13 -10 147.86 22.83 -2 13 -10 94.70 20.00 -2 -13 10 117.70 18.00 2 13 10 106.40 18.78 -2 -13 10 107.11 20.98 -2 13 -11 54.75 15.37 -2 -13 11 65.55 14.83 2 -13 -11 53.00 15.01 2 13 11 51.82 14.39 2 13 11 67.15 17.88 -2 -13 11 80.50 18.02 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12.69 2 -14 7 46.90 9.82 -2 14 7 28.42 8.42 2 -14 7 51.67 14.43 2 14 -6 230.23 25.15 2 14 -6 195.55 27.20 -2 14 6 226.88 28.69 -2 14 6 248.30 27.81 2 -14 6 208.70 21.76 -2 -14 -6 242.15 30.06 2 -14 6 239.52 28.88 -2 14 5 638.60 42.67 -2 14 5 603.32 47.05 -2 -14 -5 682.30 49.02 2 14 -5 645.76 41.82 2 -14 5 635.13 42.74 2 -14 5 553.11 33.97 -2 14 4 97.52 14.54 -2 -14 -4 102.63 19.28 2 14 -4 113.02 18.41 2 -14 4 107.23 13.90 -2 14 4 101.94 19.86 2 -14 4 116.67 19.05 -2 14 3 1120.76 53.16 2 -14 3 1089.95 50.38 -2 14 3 1034.11 59.54 2 14 -3 1098.13 55.91 -2 -14 -3 1063.26 61.02 2 -14 3 1059.45 58.23 2 14 -2 250.24 27.57 2 -14 2 269.37 28.59 -2 -14 -2 275.72 30.12 -2 14 2 254.34 24.74 -2 14 2 285.87 30.24 2 -14 2 286.55 25.21 -2 -14 -1 290.05 31.81 2 14 -1 244.04 26.70 -2 14 1 273.35 29.22 2 -14 1 240.78 21.00 2 -14 1 272.45 29.42 -2 14 1 274.55 24.85 -2 14 0 187.43 19.61 2 14 0 194.36 23.75 -2 14 0 201.92 24.01 -2 -14 0 234.98 27.68 -2 -14 0 184.58 17.54 2 -14 0 210.27 25.90 -2 14 -1 274.80 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18.23 -5 -7 0 207.03 13.84 -5 7 0 207.36 18.70 5 7 0 198.25 19.55 5 7 0 195.66 14.92 -5 -7 1 500.68 28.45 5 7 1 508.31 25.50 -5 7 -1 532.78 28.70 -5 -7 1 590.74 30.77 -5 -7 1 531.75 23.47 -5 7 -1 519.48 28.77 5 7 1 498.64 31.37 -5 7 -1 509.68 25.77 -5 7 -1 566.42 30.42 -5 7 -1 566.18 31.30 5 -7 -1 574.08 25.60 5 7 2 675.57 36.24 -5 7 -2 758.55 35.17 -5 -7 2 669.10 28.32 -5 -7 2 701.41 35.09 5 7 2 677.62 30.98 -5 7 -2 673.62 33.87 -5 7 -2 723.41 34.88 -5 7 -2 649.95 31.51 -5 -7 2 818.16 36.40 -5 7 -2 669.58 30.86 5 -7 -2 742.63 28.75 -5 7 -3 487.26 28.44 5 -7 -3 523.63 24.45 5 7 3 445.13 29.89 -5 7 -3 526.61 30.49 -5 -7 3 512.26 30.71 -5 -7 3 481.80 25.40 -5 7 -3 483.75 27.14 -5 7 -3 478.12 26.28 5 7 3 489.48 27.67 -5 7 -3 500.09 30.34 -5 -7 3 541.40 29.87 5 -7 -4 1885.41 46.95 5 7 4 1872.51 57.06 -5 7 -4 2123.33 64.04 -5 -7 4 1963.34 54.24 -5 7 -4 1724.47 53.83 5 7 4 1780.85 60.29 -5 7 -4 2043.62 62.66 -5 -7 4 1910.48 61.74 -5 7 -5 1158.21 46.13 -5 -7 5 1263.15 46.12 -5 7 -5 1374.99 53.26 5 -7 -5 1129.12 37.19 5 7 5 1124.14 47.88 5 7 5 1149.09 47.35 -5 7 -5 1433.80 53.85 -5 -7 5 1284.01 52.04 -5 7 -6 95.35 13.34 -5 -7 6 127.14 15.96 -5 7 -6 139.26 17.81 5 -7 -6 101.02 11.47 5 7 6 96.63 14.70 5 7 6 84.37 13.46 -5 -7 6 137.84 17.92 5 7 7 259.55 24.54 -5 -7 7 318.13 25.48 5 7 7 273.26 24.15 -5 7 -7 349.19 29.28 5 -7 -7 271.50 19.82 5 7 7 290.30 18.93 -5 -7 7 322.44 29.15 -5 7 -7 271.81 24.42 -5 -7 8 258.58 23.77 -5 7 -8 289.15 26.95 5 -7 -8 248.28 19.72 5 7 8 289.58 25.68 5 7 8 287.82 26.74 -5 7 -8 244.37 24.43 5 7 8 271.32 18.74 -5 -7 8 323.53 30.20 -5 -7 9 645.63 40.50 5 7 9 548.59 35.59 5 -7 -9 504.63 29.52 5 7 9 595.63 39.43 -5 7 -9 527.74 37.44 -5 -7 9 696.98 44.89 5 7 9 616.91 30.88 -5 7 -10 1343.84 61.78 -5 -7 10 1587.23 66.31 5 7 10 1506.49 66.83 5 7 10 1403.29 58.15 5 7 10 1590.65 51.38 5 -7 -10 1268.65 49.87 -5 -7 10 1709.75 71.52 5 7 11 448.64 29.58 -5 -7 11 453.30 36.08 5 7 11 363.10 29.88 5 7 11 391.53 34.93 5 -7 -11 323.20 25.89 -5 7 -11 355.46 33.00 -5 -7 11 510.12 41.32 5 7 12 583.07 35.65 -5 -7 12 627.72 45.69 5 -7 -12 520.68 41.14 5 7 12 514.31 35.74 5 7 12 501.26 40.15 5 -7 -12 411.83 30.63 -5 7 -12 511.52 40.66 -5 -7 12 639.30 47.88 5 7 13 200.16 20.63 -5 -7 13 221.54 28.64 5 -7 -13 182.49 24.17 5 -7 -13 149.08 18.51 5 7 13 216.87 28.14 5 7 13 185.63 21.67 -5 7 -13 198.79 27.61 -5 -7 13 263.27 31.00 5 -7 -14 114.34 16.92 -5 7 -14 120.13 21.71 -5 -7 14 161.46 26.92 5 -7 -14 125.13 20.53 5 7 14 120.20 18.71 5 7 14 124.76 22.20 -5 -7 14 175.89 27.77 -5 -7 15 308.66 34.93 5 -7 -15 208.31 27.93 5 7 15 241.30 32.40 -5 7 -15 196.61 28.36 5 -7 -15 177.10 22.57 -5 -7 15 278.29 34.55 -5 -7 16 274.98 35.35 5 -7 -16 213.64 28.39 5 7 16 259.96 34.33 -5 7 -16 240.47 33.72 -5 -7 16 332.82 39.30 -5 8 16 344.28 34.74 -5 -8 -16 304.01 38.25 5 8 -16 310.48 35.37 -5 8 16 385.84 43.35 5 -8 16 423.61 45.33 5 -8 16 372.69 42.18 5 8 -15 314.74 33.97 -5 8 15 321.97 33.04 -5 -8 -15 242.69 33.78 -5 8 15 311.07 36.28 5 -8 15 334.76 39.09 5 -8 15 342.76 38.28 -5 8 14 586.66 43.78 5 -8 14 549.57 47.28 5 8 -14 542.00 42.82 -5 -8 -14 463.38 44.76 -5 8 14 566.74 47.89 5 -8 14 558.02 47.82 5 -8 13 112.16 22.04 5 -8 13 83.94 15.61 5 8 -13 95.09 17.33 -5 8 13 96.23 17.83 -5 -8 -13 74.52 14.83 -5 8 13 82.94 17.48 5 -8 13 109.45 18.66 -5 -8 -12 679.27 50.44 -5 8 12 767.11 46.38 5 -8 12 674.92 40.43 5 8 -12 691.35 45.68 -5 8 12 792.10 54.20 -5 8 12 650.78 45.04 5 -8 12 686.11 52.19 5 -8 12 711.37 51.09 5 -8 11 60.66 12.25 -5 8 11 60.84 10.70 5 8 -11 68.30 12.31 -5 -8 -11 55.01 12.47 -5 8 11 86.53 18.09 5 -8 11 57.09 12.40 -5 8 11 66.42 14.83 5 8 -11 65.33 14.52 5 -8 11 70.00 16.78 -5 8 10 143.85 18.11 5 8 -10 150.56 17.53 5 -8 10 138.45 17.65 -5 -8 -10 120.83 19.23 -5 8 10 185.67 24.84 -5 8 10 124.00 18.85 5 -8 10 156.72 21.41 5 8 -10 148.85 20.38 5 -8 10 155.84 21.89 -5 -8 -9 49.20 11.55 5 -8 9 60.09 15.76 -5 8 9 60.55 11.54 5 8 -9 56.22 10.75 5 8 -9 50.47 11.91 5 -8 9 61.99 8.77 -5 8 9 54.46 12.91 -5 8 9 45.17 11.06 5 -8 9 51.68 12.11 -5 -8 -8 1075.92 37.46 5 8 -8 1034.71 48.77 -5 8 8 1091.72 48.08 -5 -8 -8 973.36 52.79 5 8 -8 1046.26 46.34 5 -8 8 971.34 43.90 -5 8 8 1125.93 56.49 -5 8 8 906.39 50.22 5 8 -7 387.04 29.70 -5 -8 -7 410.47 22.93 5 -8 7 357.07 20.63 5 -8 7 352.86 28.99 -5 -8 -7 395.92 32.76 -5 8 7 418.54 28.42 5 8 -7 368.39 27.80 5 -8 7 362.07 26.55 -5 8 7 420.24 32.82 -5 8 7 369.78 31.40 -5 8 6 855.05 30.21 -5 -8 -6 975.25 35.02 5 8 -6 1005.85 45.67 -5 8 6 978.48 50.10 5 -8 6 924.84 34.64 -5 -8 -6 1000.86 49.74 -5 8 6 1054.70 44.33 5 8 -6 921.57 43.28 5 -8 6 960.21 42.17 -5 8 6 1043.56 51.12 5 -8 6 998.04 47.57 5 8 -5 839.51 42.24 5 -8 5 853.34 39.73 -5 -8 -5 877.41 33.35 -5 8 5 802.49 29.73 -5 -8 -5 896.67 45.61 -5 8 5 914.17 40.28 5 8 -5 867.45 41.91 -5 8 5 975.28 48.07 -5 8 5 870.36 46.15 -5 -8 -4 89.69 11.41 -5 8 4 83.65 9.99 -5 -8 -4 80.82 14.00 -5 8 4 81.86 11.70 5 -8 4 77.56 12.27 5 8 -4 78.71 12.32 -5 8 4 103.41 14.99 -5 8 4 69.42 12.92 -5 -8 -3 673.99 29.88 -5 8 3 664.06 28.21 -5 -8 -3 664.42 37.48 -5 8 3 668.57 33.27 5 8 -3 630.84 36.33 -5 8 3 712.06 38.70 -5 8 3 653.96 37.95 -5 -8 -2 1294.53 42.42 -5 -8 -2 1291.93 51.26 -5 8 2 1250.90 40.04 -5 8 2 1330.67 51.66 5 8 -2 1200.94 49.50 5 8 -2 1212.79 31.08 -5 8 2 1225.40 50.38 -5 -8 -2 1141.47 28.00 -5 8 2 1302.61 46.02 -5 -8 -1 878.90 36.72 -5 -8 -1 920.45 42.14 -5 8 1 905.49 35.28 -5 8 1 906.92 42.04 -5 -8 -1 886.71 25.66 5 8 -1 851.87 42.16 -5 8 1 901.04 38.53 5 8 -1 838.89 28.77 -5 8 1 870.98 41.02 -5 -8 0 610.79 31.06 -5 -8 0 628.93 35.16 -5 8 0 642.88 31.07 -5 -8 0 620.13 23.30 5 8 0 566.66 34.87 -5 8 0 652.08 32.99 5 8 0 581.67 25.99 -5 8 0 634.37 34.21 -5 8 0 596.39 33.83 -5 -8 1 853.41 38.43 -5 8 -1 882.18 36.21 -5 8 -1 996.84 40.01 -5 -8 1 897.55 29.61 5 8 1 822.27 41.69 5 8 1 836.74 33.54 -5 8 -1 951.87 40.35 -5 8 -1 955.89 41.73 5 -8 -1 964.01 36.52 -5 8 -1 858.32 39.38 -5 -8 1 1022.97 43.30 -5 -8 2 1191.01 46.69 -5 8 -2 1239.18 46.78 -5 8 -2 1323.40 47.90 -5 8 -2 1146.83 42.72 -5 -8 2 1188.42 36.94 5 8 2 1130.44 41.63 -5 8 -2 1119.71 43.88 5 8 2 1054.21 48.34 -5 8 -2 1268.00 47.36 -5 -8 2 1238.94 48.51 5 -8 -2 1269.51 41.13 -5 -8 3 616.25 34.83 5 -8 -3 633.76 29.29 -5 8 -3 692.84 36.03 -5 -8 3 641.64 29.26 5 8 3 589.78 35.43 5 8 3 596.40 31.33 -5 8 -3 674.59 35.15 -5 8 -3 599.89 30.84 -5 8 -3 648.87 33.67 -5 8 -3 589.71 31.81 -5 -8 3 682.17 35.50 -5 -8 4 87.23 14.37 -5 -8 4 104.61 13.82 -5 8 -4 84.18 12.69 5 -8 -4 110.01 12.31 -5 8 -4 121.66 15.48 -5 -8 4 98.98 13.29 5 8 4 90.35 14.23 -5 8 -4 99.79 14.43 5 8 4 91.12 12.06 -5 8 -4 93.65 11.79 -5 -8 5 934.39 40.13 5 -8 -5 932.33 36.67 -5 8 -5 1072.32 48.59 -5 8 -5 838.19 41.15 5 8 5 886.17 44.59 5 8 5 832.31 41.22 -5 -8 5 937.15 46.28 5 8 6 986.84 47.72 -5 -8 6 1105.60 45.60 -5 8 -6 1146.10 51.92 -5 8 -6 930.26 44.69 5 -8 -6 992.71 38.73 5 8 6 936.60 45.72 -5 -8 6 1088.72 51.77 5 8 7 489.20 34.12 -5 8 -7 459.02 32.93 -5 -8 7 509.71 32.71 -5 8 -7 595.48 39.00 5 -8 -7 498.99 28.50 5 8 7 540.00 35.87 -5 -8 7 587.43 38.95 -5 8 -8 922.44 48.31 -5 -8 8 1155.85 51.64 5 -8 -8 883.19 39.72 5 8 8 955.46 48.62 5 8 8 966.70 50.70 -5 -8 8 1096.82 55.60 -5 -8 9 74.32 16.66 -5 -8 9 55.72 12.15 5 8 9 55.07 10.70 -5 8 -9 35.81 7.74 5 8 9 27.79 8.68 5 -8 -9 45.43 8.74 -5 -8 10 158.27 21.18 5 -8 -10 131.49 16.45 5 8 10 151.74 20.97 5 8 10 156.01 19.94 -5 -8 10 191.53 25.81 -5 8 -10 138.23 19.72 5 8 11 57.24 11.83 -5 -8 11 63.04 14.75 -5 8 -11 71.04 15.51 -5 -8 11 89.40 18.35 5 8 11 63.69 13.05 5 -8 -11 54.92 10.36 -5 -8 12 843.44 52.88 5 8 12 666.17 43.47 5 -8 -12 577.50 37.45 5 8 12 741.19 51.33 -5 8 -12 652.35 47.50 -5 -8 12 882.99 56.79 -5 -8 13 80.41 18.60 5 8 13 55.98 15.95 -5 -8 13 65.81 14.38 5 -8 -13 69.23 13.29 -5 8 -13 40.78 12.72 5 8 13 31.08 9.74 5 -8 -13 54.84 12.25 -5 -8 14 626.40 49.11 5 -8 -14 588.85 46.64 5 8 14 437.02 35.92 5 -8 -14 383.14 32.99 -5 8 -14 467.65 43.75 -5 -8 14 669.25 53.12 -5 -8 15 342.17 37.41 5 -8 -15 277.11 31.17 5 8 15 273.98 34.10 5 -8 -15 226.12 26.80 -5 8 -15 261.27 34.22 -5 -8 15 395.71 41.94 -5 -8 16 361.48 40.71 5 -8 -16 335.76 36.79 5 8 16 406.10 44.82 -5 8 -16 352.39 40.77 -5 -8 16 402.86 43.98 5 -9 15 88.26 22.46 -5 9 15 56.58 15.59 5 9 -15 67.03 16.84 -5 9 15 83.08 21.97 -5 -9 -15 55.32 14.93 5 -9 15 99.51 21.62 -5 9 14 31.82 10.75 5 -9 14 33.44 10.71 -5 9 14 59.46 11.99 -5 -9 -14 45.59 15.50 5 9 -14 34.82 11.89 5 -9 14 30.21 11.69 5 -9 13 138.83 24.43 -5 -9 -13 125.64 20.53 -5 9 13 141.43 20.60 5 9 -13 146.75 22.26 -5 9 13 171.64 26.32 -5 9 13 115.16 18.19 5 -9 13 126.45 21.55 -5 9 12 223.84 24.73 -5 9 12 200.38 26.14 -5 -9 -12 223.54 29.21 5 -9 12 205.45 22.36 -5 9 12 251.15 31.08 5 -9 12 215.27 29.93 5 9 -12 216.55 27.46 5 -9 12 248.47 31.43 5 -9 11 239.16 23.87 -5 9 11 251.26 25.92 -5 -9 -11 226.54 27.53 5 9 -11 252.46 23.48 5 -9 11 252.15 30.44 -5 9 11 258.25 31.67 -5 9 11 196.24 26.49 5 9 -11 225.89 26.40 5 -9 11 249.78 30.09 5 -9 10 1498.20 70.31 5 9 -10 1436.11 63.48 -5 9 10 1564.12 61.07 -5 -9 -10 1381.68 69.76 5 -9 10 1381.70 53.87 5 9 -10 1431.65 55.76 -5 9 10 1552.46 73.23 -5 9 10 1350.38 65.28 5 -9 10 1481.19 69.64 5 -9 9 173.73 18.86 5 9 -9 168.25 21.95 -5 9 9 183.26 20.71 -5 -9 -9 200.42 25.55 5 9 -9 196.01 20.97 -5 9 9 225.73 26.72 -5 9 9 160.24 23.16 5 -9 9 187.08 22.86 5 -9 9 173.07 23.66 5 -9 8 145.74 17.20 -5 9 8 173.62 18.70 -5 -9 -8 162.16 22.15 -5 9 8 145.55 21.01 5 9 -8 176.85 21.40 5 9 -8 167.04 19.58 -5 9 8 172.68 22.70 5 -9 8 149.26 20.89 5 -9 8 167.90 21.05 5 -9 7 64.30 9.26 5 -9 7 69.66 11.36 5 9 -7 70.56 13.19 -5 9 7 89.83 13.46 -5 -9 -7 69.80 15.57 5 9 -7 89.83 14.79 -5 9 7 61.75 13.23 -5 9 7 80.27 15.70 5 -9 7 37.97 10.69 -5 -9 -6 195.64 15.82 -5 -9 -6 202.09 22.80 -5 9 6 192.35 18.72 5 9 -6 196.86 21.12 5 9 -6 131.73 18.06 5 -9 6 199.40 19.48 -5 9 6 221.95 24.57 -5 9 6 166.02 22.28 5 -9 6 197.95 20.89 -5 -9 -5 374.18 21.73 -5 -9 -5 389.81 31.29 -5 9 5 386.86 31.31 -5 9 5 386.89 26.13 5 9 -5 401.59 29.54 -5 9 5 395.27 32.74 5 -9 5 389.42 27.27 -5 -9 -4 1921.31 50.37 -5 9 4 1879.87 46.34 -5 9 4 2107.60 70.69 -5 -9 -4 2013.12 69.71 -5 9 4 2002.01 59.31 5 9 -4 1901.35 64.49 5 -9 4 1893.06 59.26 -5 9 4 1821.69 67.28 -5 -9 -3 749.12 32.29 -5 -9 -3 806.52 43.06 -5 9 3 777.30 30.90 -5 9 3 770.67 42.75 -5 9 3 836.00 43.55 -5 9 3 791.84 36.80 5 9 -3 726.43 40.22 -5 -9 -2 710.09 32.50 -5 -9 -2 732.48 40.62 -5 9 2 761.53 32.05 -5 9 2 686.58 39.38 5 9 -2 624.72 38.16 -5 9 2 720.15 34.63 -5 9 2 758.76 40.77 -5 -9 -1 155.01 15.58 -5 -9 -1 186.89 20.79 5 9 -1 150.66 12.23 -5 9 1 181.67 16.13 -5 9 1 164.09 16.09 -5 9 1 171.33 19.46 5 9 -1 160.53 18.55 -5 9 1 175.28 19.45 -5 -9 0 132.82 15.51 -5 -9 0 133.86 17.50 5 9 0 134.76 17.48 -5 9 0 137.28 14.68 5 -9 0 134.51 15.00 -5 -9 0 124.00 9.87 -5 9 0 127.99 16.93 -5 9 0 136.93 15.37 5 9 0 124.26 12.01 -5 9 0 135.81 16.73 -5 -9 1 93.38 12.75 -5 9 -1 114.36 14.65 -5 9 -1 135.11 15.25 -5 9 -1 124.20 15.51 -5 -9 1 117.55 10.73 5 9 1 101.34 10.69 -5 9 -1 119.13 14.63 5 9 1 106.23 15.54 -5 9 -1 120.33 15.35 5 -9 -1 120.92 13.14 -5 -9 1 137.45 17.42 -5 9 -2 583.61 33.52 -5 -9 2 617.88 26.48 -5 9 -2 728.42 36.53 5 9 2 615.85 37.82 -5 -9 2 630.33 34.94 5 9 2 625.40 30.76 -5 9 -2 620.14 33.48 -5 9 -2 695.45 35.94 -5 9 -2 694.94 36.18 -5 -9 2 679.29 37.54 5 -9 -2 662.40 32.56 -5 -9 3 661.66 37.76 5 -9 -3 746.76 34.43 -5 9 -3 657.95 35.27 -5 9 -3 755.92 39.36 -5 -9 3 634.03 29.10 -5 9 -3 729.88 38.29 5 9 3 628.92 33.37 5 9 3 584.80 37.32 -5 9 -3 675.44 34.47 -5 9 -3 716.23 36.56 -5 -9 3 780.66 41.11 -5 -9 4 2099.15 67.00 5 -9 -4 1900.06 54.97 -5 -9 4 1833.28 52.62 -5 9 -4 2051.49 66.01 -5 9 -4 1753.84 54.16 -5 9 -4 1734.21 59.33 -5 9 -4 2001.78 65.74 5 9 4 1845.16 59.23 5 9 4 1796.66 66.10 -5 -9 4 1956.12 65.69 5 -9 -5 280.65 21.59 5 9 5 254.84 25.25 -5 -9 5 290.21 22.91 -5 9 -5 335.85 28.01 -5 9 -5 257.37 23.57 -5 9 -5 272.40 20.52 5 9 5 253.60 22.65 -5 -9 5 289.39 26.86 -5 -9 6 180.33 19.96 -5 9 -6 204.28 22.39 5 -9 -6 181.11 17.87 5 9 6 150.63 20.63 -5 9 -6 154.65 18.73 5 9 6 178.77 19.23 -5 -9 6 182.69 22.07 -5 -9 7 67.75 14.62 -5 9 -7 61.43 12.90 -5 -9 7 52.53 8.68 5 9 7 27.66 4.74 5 -9 -7 60.18 9.94 5 9 7 43.48 10.26 -5 -9 8 167.47 19.99 -5 9 -8 152.03 20.00 5 -9 -8 144.35 17.05 5 9 8 144.48 19.50 5 9 8 167.39 21.10 -5 -9 8 179.17 24.10 5 9 9 182.53 22.33 -5 -9 9 183.31 20.02 -5 9 -9 174.72 22.53 5 -9 -9 167.60 19.06 5 9 9 198.06 23.64 -5 -9 9 231.46 28.26 5 9 10 1517.47 70.96 -5 9 -10 1421.34 66.47 -5 -9 10 1924.22 73.45 5 -9 -10 1371.12 55.29 5 9 10 1485.27 64.53 -5 -9 10 1844.42 78.03 -5 9 -11 190.82 25.09 5 9 11 170.68 23.46 -5 -9 11 215.78 26.07 5 -9 -11 190.17 21.93 5 9 11 208.48 25.96 -5 -9 11 249.40 30.47 -5 9 -12 202.76 26.85 -5 -9 12 265.06 28.86 5 -9 -12 199.19 22.64 5 9 12 234.54 27.39 5 9 12 280.32 32.59 -5 -9 12 299.83 35.14 -5 9 -13 145.51 24.02 -5 -9 13 199.42 26.19 5 9 13 149.30 21.52 5 9 13 163.86 25.67 5 -9 -13 114.38 18.06 -5 -9 13 183.07 28.65 -5 -9 14 57.85 17.57 -5 -9 14 57.08 14.17 5 -9 -14 57.98 14.46 -5 9 -14 47.60 13.58 5 9 14 67.20 15.94 5 9 14 48.16 14.75 5 -9 -14 35.93 9.19 -5 -9 15 110.98 23.28 -5 -9 15 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845.53 43.85 -10 -4 -7 784.10 45.58 -10 -4 -7 1027.29 52.29 -10 4 7 945.28 55.56 -10 4 6 428.27 33.86 -10 -4 -6 436.03 35.39 10 -4 6 360.71 28.28 10 4 -6 362.45 34.29 -10 4 6 445.24 37.81 10 -4 6 395.01 35.95 -10 -4 -6 365.68 30.06 -10 -4 -6 468.10 34.78 -10 4 6 419.15 36.46 -10 4 5 493.63 36.91 -10 -4 -5 532.53 39.23 10 -4 5 431.35 31.33 10 4 -5 388.43 35.63 -10 4 5 553.27 41.08 10 4 -5 415.16 31.60 10 -4 5 513.41 39.85 -10 -4 -5 450.41 31.34 -10 -4 -5 529.53 36.49 -10 4 5 510.96 40.14 -10 4 4 297.32 28.70 -10 -4 -4 263.71 26.95 10 -4 4 246.90 24.04 10 4 -4 222.22 27.30 -10 4 4 309.59 30.25 10 4 -4 235.01 23.79 10 -4 4 305.31 30.08 -10 -4 -4 256.16 22.74 -10 -4 -4 298.19 27.48 -10 4 4 297.38 30.61 -10 4 3 69.54 13.08 -10 -4 -3 84.69 15.05 10 -4 3 71.85 14.89 10 4 -3 56.74 14.83 -10 4 3 68.50 13.97 10 -4 3 62.58 15.24 10 4 -3 61.59 11.75 -10 -4 -3 71.11 12.31 -10 -4 -3 62.03 10.04 -10 4 3 82.38 15.19 -10 -4 -2 332.38 30.32 -10 4 2 296.51 27.82 10 -4 2 287.74 27.04 10 4 -2 280.73 28.96 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7.83 -15 0 3 26.37 9.30 -15 0 -3 35.19 13.71 -15 0 4 1059.42 72.06 -15 0 -4 1122.92 74.31 15 0 -4 993.55 68.85 15 0 4 973.30 64.81 -15 0 4 1104.92 72.44 15 0 -4 1014.53 66.90 15 0 4 980.76 68.70 -15 0 -4 1054.57 70.03 -15 1 4 150.08 29.25 -15 -1 -4 160.28 29.33 15 1 -4 138.24 28.70 15 -1 4 128.12 23.74 -15 1 4 160.94 30.48 15 1 -4 143.71 25.53 15 -1 4 130.91 23.75 -15 -1 -4 146.97 26.59 -15 1 3 38.90 15.26 -15 -1 -3 33.20 13.00 15 1 -3 46.63 18.84 15 -1 3 30.96 12.43 15 1 -3 20.69 10.96 15 -1 3 36.88 11.17 -15 1 3 4.95 9.72 -15 -1 -3 38.34 14.69 -15 1 2 254.40 35.95 -15 -1 -2 259.02 33.50 15 1 -2 273.39 35.19 15 -1 2 229.77 32.61 -15 1 2 253.82 34.20 15 1 -2 220.07 30.87 15 -1 2 240.82 33.70 -15 -1 -2 269.34 35.32 -15 1 1 -23.96 19.34 -15 -1 -1 -12.08 14.71 15 -1 1 -3.27 7.82 15 1 -1 13.21 10.71 15 1 -1 -4.77 12.70 15 -1 1 13.29 10.78 -15 1 1 6.73 13.86 -15 -1 -1 -15.32 15.07 -15 -1 0 746.03 58.54 -15 1 0 698.33 56.68 15 -1 0 661.14 53.80 15 1 0 670.37 55.71 15 -1 0 735.96 57.21 15 1 0 762.55 56.78 -15 -1 0 717.74 56.74 -15 1 0 781.23 59.87 -15 -1 1 17.49 7.66 -15 1 -1 -12.46 13.95 15 -1 -1 1.18 11.21 15 1 1 14.55 8.23 15 -1 -1 -14.99 12.37 15 1 1 -18.31 17.91 -15 -1 1 -4.36 13.68 -15 1 -1 2.50 8.54 -15 -1 2 169.69 28.04 -15 1 -2 201.27 31.42 15 1 2 169.54 28.58 15 -1 -2 181.72 29.04 15 -1 -2 195.22 28.91 15 1 2 198.04 31.64 -15 1 -2 200.82 32.01 -15 -1 2 165.48 26.97 -15 -1 3 33.60 14.21 -15 1 -3 16.55 11.43 15 -1 -3 33.76 9.98 15 1 3 37.71 12.32 15 -1 -3 33.88 14.90 15 1 3 38.47 13.56 -15 -1 3 37.43 9.09 -15 1 -3 52.57 17.85 -15 -1 4 146.67 26.31 -15 1 -4 139.55 27.52 15 -1 -4 136.48 25.18 15 1 4 136.62 25.70 15 -1 -4 149.35 27.50 -15 -1 4 158.39 29.03 15 1 4 135.29 27.27 -15 1 -4 147.69 26.07 -15 2 3 8.72 8.80 -15 -2 -3 26.04 12.73 15 -2 3 8.68 6.84 15 2 -3 12.59 9.21 15 2 -3 -1.15 12.22 15 -2 3 4.23 14.83 -15 2 3 -0.68 14.20 -15 -2 -3 13.80 13.60 -15 2 2 555.03 50.74 -15 -2 -2 603.54 53.25 15 -2 2 559.35 49.21 15 2 -2 572.12 51.65 -15 2 2 595.70 53.27 15 2 -2 536.50 46.46 15 -2 2 626.60 54.49 -15 -2 -2 673.25 53.92 -15 -2 -1 10.54 9.03 -15 2 1 18.87 6.54 15 -2 1 14.14 8.04 15 2 -1 37.35 11.60 15 -2 1 36.47 11.13 15 2 -1 18.45 10.32 -15 2 1 20.77 11.19 -15 -2 -1 45.63 16.66 -15 -2 0 27.06 13.02 -15 2 0 31.59 10.26 15 -2 0 12.24 10.25 15 2 0 19.76 11.19 15 -2 0 17.17 7.85 15 2 0 23.53 9.15 -15 -2 0 25.51 10.00 -15 2 0 38.93 12.41 -15 -2 1 40.76 15.51 -15 2 -1 32.84 10.47 15 -2 -1 24.93 15.43 15 2 1 49.52 17.18 15 -2 -1 40.27 11.70 15 2 1 21.47 7.05 -15 -2 1 18.25 11.66 -15 2 -1 42.28 10.99 -15 -2 2 607.28 55.37 -15 2 -2 638.10 55.73 15 -2 -2 538.09 50.68 15 2 2 528.77 49.58 -15 -2 2 610.89 51.98 15 -2 -2 634.40 52.83 15 2 2 532.79 48.06 -15 2 -2 667.36 56.05 -15 -2 3 3.91 8.05 -15 2 -3 6.55 7.56 15 -2 -3 6.87 8.34 15 2 3 2.86 7.79 15 -2 -3 7.17 8.29 15 2 3 14.43 10.15 -15 -2 3 5.17 10.25 -15 2 -3 -12.91 10.93 15 2 4 777.71 59.22 -15 3 3 128.24 22.41 -15 -3 -3 130.47 25.14 15 -3 3 122.98 22.87 15 3 -3 152.02 26.44 -15 3 3 167.47 27.87 -15 -3 -3 165.69 28.92 -15 -3 -2 220.39 32.61 -15 3 2 253.88 34.66 15 -3 2 218.15 30.38 15 3 -2 224.83 33.33 -15 3 2 254.99 34.38 15 3 -2 264.92 32.26 15 -3 2 223.41 30.58 -15 -3 -2 269.21 35.62 -15 -3 -1 19.87 13.75 -15 3 1 -13.06 11.27 15 -3 1 21.05 8.82 15 3 -1 13.48 7.77 15 -3 1 3.19 7.73 15 3 -1 1.04 9.37 -15 3 1 6.56 13.59 -15 -3 -1 19.21 8.88 -15 -3 0 544.68 50.10 -15 3 0 517.51 48.90 15 -3 0 505.61 47.29 15 3 0 425.10 46.13 15 -3 0 516.20 49.02 15 3 0 437.39 44.68 -15 -3 0 551.15 48.80 -15 3 0 530.20 51.05 -15 -3 1 16.77 13.28 -15 3 -1 12.31 7.17 15 -3 -1 14.90 6.84 15 3 1 16.04 12.98 15 -3 -1 16.58 8.31 15 3 1 5.80 10.80 -15 -3 1 6.23 6.76 -15 3 -1 17.30 11.38 -15 -3 2 224.07 31.52 -15 3 -2 225.16 33.55 15 -3 -2 216.91 30.40 15 3 2 200.32 28.89 -15 -3 2 207.86 29.81 15 -3 -2 249.32 36.22 15 3 2 213.86 30.23 -15 3 -2 268.72 36.26 -15 3 -3 216.97 31.82 15 -3 -3 152.25 26.26 15 3 3 164.98 26.63 -15 -3 3 185.95 31.22 -15 3 -3 197.23 28.39 -15 -4 -1 48.03 13.94 -15 4 1 82.00 18.83 15 -4 1 94.12 17.89 15 4 -1 90.13 20.46 15 -4 1 85.18 16.88 15 4 -1 90.72 16.69 -15 4 1 98.62 23.76 -15 -4 -1 81.96 17.94 -15 -4 0 66.90 19.47 -15 4 0 59.59 18.20 15 -4 0 57.25 17.96 15 4 0 32.92 8.36 15 -4 0 58.00 12.57 15 4 0 54.94 18.06 -15 -4 0 47.74 15.75 -15 4 0 36.09 15.81 -15 -4 1 139.09 26.20 -15 4 -1 163.37 28.73 15 -4 -1 151.81 25.85 15 4 1 125.47 23.88 15 -4 -1 160.78 25.23 15 4 1 108.74 21.80 -15 -4 1 132.86 24.64 -15 4 -1 139.19 26.65 0 0 0 0.00 0.00 TITL mini-19049 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 0.71073 11.884516 14.603974 14.886185 90.0000 90.0000 90.0000 ZERR 1.00 0.000690 0.000869 0.001025 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C N O S Cl Re UNIT 1.00 1.00 1.00 1.00 1.00 1.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 46209 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Re1 Re 0.51737(2) 0.47742(2) 0.42778(2) 0.00959(5) Uani 0.9867(5) 1 d . . P A 1 N1 N 0.4414(3) 0.3830(3) 0.4382(3) 0.0178(8) Uani 1 1 d . . . . . Cl1 Cl 0.60471(9) 0.47333(8) 0.28194(7) 0.0176(2) Uani 1 1 d . . . . . N11 N 0.4918(3) 0.5569(2) 0.5400(2) 0.0126(7) Uani 1 1 d . . . . . P11 P 0.37304(10) 0.58413(8) 0.37680(8) 0.0123(2) Uani 1 1 d . . . . . P21 P 0.68470(9) 0.43880(8) 0.51706(8) 0.0113(2) Uani 1 1 d . . . . . C11 C 0.3063(4) 0.6083(3) 0.4870(3) 0.0163(9) Uani 1 1 d . . . . . H11A H 0.2631 0.6664 0.4847 0.020 Uiso 1 1 calc R U . . . H11B H 0.2545 0.5579 0.5042 0.020 Uiso 1 1 calc R U . . . C21 C 0.4011(4) 0.6155(3) 0.5526(3) 0.0141(9) Uani 1 1 d . . . . . C31 C 0.4208(4) 0.6693(3) 0.6263(3) 0.0177(10) Uani 1 1 d . . . . . H31 H 0.3718 0.7149 0.6500 0.021 Uiso 1 1 calc R U . . . C41 C 0.5288(4) 0.6443(3) 0.6612(3) 0.0170(9) Uani 1 1 d . . . . . H41 H 0.5652 0.6703 0.7122 0.020 Uiso 1 1 calc R U . . . C51 C 0.5700(4) 0.5753(3) 0.6068(3) 0.0134(9) Uani 1 1 d . . . . . C61 C 0.6807(4) 0.5259(3) 0.6079(3) 0.0156(9) Uani 1 1 d . . . . . H61A H 0.6914 0.4956 0.6671 0.019 Uiso 1 1 calc R U . . . H61B H 0.7427 0.5705 0.5993 0.019 Uiso 1 1 calc R U . . . C12 C 0.4357(4) 0.6969(3) 0.3407(3) 0.0193(10) Uani 1 1 d . . . . . C22 C 0.5514(4) 0.7085(3) 0.3862(4) 0.0221(11) Uani 1 1 d . . . B 1 H22A H 0.5421 0.7072 0.4518 0.033 Uiso 1 1 calc R U . B 1 H22B H 0.5844 0.7674 0.3681 0.033 Uiso 1 1 calc R U . B 1 H22C H 0.6013 0.6584 0.3676 0.033 Uiso 1 1 calc R U . B 1 C32 C 0.3616(5) 0.7782(3) 0.3703(4) 0.0301(13) Uani 1 1 d . . . . . H32A H 0.2850 0.7698 0.3469 0.045 Uiso 1 1 calc R U . . . H32B H 0.3932 0.8355 0.3465 0.045 Uiso 1 1 calc R U . . . H32C H 0.3593 0.7811 0.4363 0.045 Uiso 1 1 calc R U . . . C42 C 0.4536(4) 0.7001(4) 0.2387(3) 0.0226(11) Uani 1 1 d . . . . . H42A H 0.4996 0.6475 0.2200 0.034 Uiso 1 1 calc R U . . . H42B H 0.4923 0.7572 0.2225 0.034 Uiso 1 1 calc R U . . . H42C H 0.3805 0.6975 0.2081 0.034 Uiso 1 1 calc R U . . . C52 C 0.2595(4) 0.5425(3) 0.2996(3) 0.0202(11) Uani 1 1 d . . . . . C62 C 0.1973(4) 0.4641(4) 0.3481(4) 0.0268(12) Uani 1 1 d . . . . . H62A H 0.2518 0.4172 0.3666 0.040 Uiso 1 1 calc R U . . . H62B H 0.1419 0.4368 0.3071 0.040 Uiso 1 1 calc R U . . . H62C H 0.1587 0.4884 0.4014 0.040 Uiso 1 1 calc R U . . . C72 C 0.3107(5) 0.5034(4) 0.2134(4) 0.0312(14) Uani 1 1 d . . . . . H72A H 0.3438 0.5533 0.1779 0.047 Uiso 1 1 calc R U . . . H72B H 0.2518 0.4729 0.1780 0.047 Uiso 1 1 calc R U . . . H72C H 0.3695 0.4588 0.2290 0.047 Uiso 1 1 calc R U . . . C82 C 0.1727(5) 0.6176(4) 0.2773(5) 0.0362(14) Uani 1 1 d . . . . . H82A H 0.1452 0.6454 0.3334 0.054 Uiso 1 1 calc R U . . . H82B H 0.1093 0.5904 0.2445 0.054 Uiso 1 1 calc R U . . . H82C H 0.2083 0.6650 0.2400 0.054 Uiso 1 1 calc R U . . . C13 C 0.8298(4) 0.4523(3) 0.4682(4) 0.0185(10) Uani 1 1 d . . . . . C23 C 0.9248(4) 0.4548(4) 0.5388(4) 0.0251(12) Uani 1 1 d . . . . . H23A H 0.9045 0.4976 0.5872 0.038 Uiso 1 1 calc R U . . . H23B H 0.9949 0.4753 0.5101 0.038 Uiso 1 1 calc R U . . . H23C H 0.9356 0.3932 0.5640 0.038 Uiso 1 1 calc R U . . . C33 C 0.8521(5) 0.3757(4) 0.4003(4) 0.0272(12) Uani 1 1 d . . . . . H33A H 0.8590 0.3170 0.4321 0.041 Uiso 1 1 calc R U . . . H33B H 0.9221 0.3886 0.3676 0.041 Uiso 1 1 calc R U . . . H33C H 0.7894 0.3724 0.3574 0.041 Uiso 1 1 calc R U . . . C43 C 0.8292(4) 0.5453(3) 0.4185(4) 0.0272(12) Uani 1 1 d . . . . . H43A H 0.7729 0.5438 0.3701 0.041 Uiso 1 1 calc R U . . . H43B H 0.9039 0.5568 0.3926 0.041 Uiso 1 1 calc R U . . . H43C H 0.8105 0.5944 0.4611 0.041 Uiso 1 1 calc R U . . . C53 C 0.6665(4) 0.3263(3) 0.5783(4) 0.0151(9) Uani 1 1 d . . . . . C63 C 0.6469(5) 0.2475(3) 0.5104(4) 0.0212(10) Uani 1 1 d . . . . . H63A H 0.5863 0.2645 0.4688 0.032 Uiso 1 1 calc R U . . . H63B H 0.6257 0.1916 0.5431 0.032 Uiso 1 1 calc R U . . . H63C H 0.7163 0.2363 0.4763 0.032 Uiso 1 1 calc R U . . . C73 C 0.5615(4) 0.3358(3) 0.6372(4) 0.0205(10) Uani 1 1 d . . . . . H73A H 0.5740 0.3838 0.6824 0.031 Uiso 1 1 calc R U . . . H73B H 0.5462 0.2773 0.6674 0.031 Uiso 1 1 calc R U . . . H73C H 0.4969 0.3525 0.5993 0.031 Uiso 1 1 calc R U . . . C83 C 0.7666(4) 0.3032(3) 0.6393(4) 0.0220(11) Uani 1 1 d . . . . . H83A H 0.8312 0.2852 0.6021 0.033 Uiso 1 1 calc R U . . . H83B H 0.7463 0.2524 0.6795 0.033 Uiso 1 1 calc R U . . . H83C H 0.7866 0.3572 0.6753 0.033 Uiso 1 1 calc R U . . . Re1B Re 0.5459(10) 0.5384(8) 0.4080(8) 0.00959(5) Uani 0.0133(5) 1 d . . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Re1 0.01074(8) 0.00862(8) 0.00942(8) -0.00050(7) -0.00107(6) 0.00052(6) N1 0.0193(18) 0.0153(18) 0.019(2) 0.0010(17) -0.0050(17) -0.0010(14) Cl1 0.0203(5) 0.0219(5) 0.0105(5) -0.0020(5) 0.0011(4) 0.0036(5) N11 0.0130(18) 0.0139(16) 0.0109(17) -0.0016(13) 0.0007(14) 0.0008(14) P11 0.0122(5) 0.0146(6) 0.0102(6) 0.0019(4) 0.0002(4) 0.0021(4) P21 0.0104(5) 0.0135(5) 0.0099(6) -0.0015(4) 0.0002(4) 0.0006(4) C11 0.013(2) 0.018(2) 0.017(2) 0.0026(19) 0.0022(18) 0.0046(17) C21 0.016(2) 0.015(2) 0.011(2) 0.0022(17) 0.0034(16) 0.0035(17) C31 0.022(2) 0.017(2) 0.015(2) -0.0011(19) 0.0041(19) 0.0052(18) C41 0.022(2) 0.016(2) 0.012(2) -0.0021(17) 0.0014(19) 0.0016(19) C51 0.015(2) 0.011(2) 0.014(2) -0.0016(17) 0.0009(16) -0.0004(17) C61 0.013(2) 0.015(2) 0.018(2) -0.007(2) -0.0016(16) 0.0001(19) C12 0.025(2) 0.016(2) 0.017(2) 0.0043(19) 0.006(2) 0.0031(19) C22 0.029(3) 0.014(2) 0.024(3) 0.0033(19) 0.002(2) -0.0060(19) C32 0.040(3) 0.015(2) 0.035(3) 0.008(2) 0.014(3) 0.011(2) C42 0.026(3) 0.024(2) 0.018(3) 0.007(2) 0.006(2) 0.004(2) C52 0.017(2) 0.027(3) 0.017(2) 0.0002(19) -0.0071(17) -0.0004(18) C62 0.019(2) 0.031(3) 0.031(3) -0.001(2) -0.004(2) -0.004(2) C72 0.031(3) 0.047(4) 0.016(3) -0.008(2) -0.004(2) -0.008(2) C82 0.021(3) 0.049(4) 0.038(4) 0.015(3) -0.008(3) 0.004(2) C13 0.014(2) 0.026(3) 0.016(2) -0.0007(19) 0.0029(18) 0.0003(17) C23 0.013(2) 0.041(3) 0.021(2) -0.003(2) 0.0017(18) 0.0004(19) C33 0.019(3) 0.044(3) 0.018(3) -0.007(2) 0.0041(19) 0.007(2) C43 0.022(2) 0.035(3) 0.025(3) 0.007(2) 0.000(2) -0.0099(19) C53 0.019(2) 0.014(2) 0.012(2) -0.0003(19) -0.0023(19) 0.0008(16) C63 0.028(3) 0.013(2) 0.022(3) -0.003(2) -0.007(2) 0.0021(19) C73 0.021(2) 0.024(2) 0.017(2) 0.005(2) 0.000(2) -0.004(2) C83 0.026(3) 0.018(2) 0.022(3) 0.000(2) -0.006(2) 0.008(2) Re1B 0.01074(8) 0.00862(8) 0.00942(8) -0.00050(7) -0.00107(6) 0.00052(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Re1 N11 108.25(18) . . ? N1 Re1 Cl1 107.45(15) . . ? N11 Re1 Cl1 144.08(11) . . ? N1 Re1 P11 100.17(14) . . ? N11 Re1 P11 77.71(11) . . ? Cl1 Re1 P11 92.28(4) . . ? N1 Re1 P21 101.57(14) . . ? N11 Re1 P21 79.12(11) . . ? Cl1 Re1 P21 97.55(4) . . ? P11 Re1 P21 152.17(4) . . ? C21 N11 C51 107.8(4) . . ? C21 N11 Re1 124.9(3) . . ? C51 N11 Re1 126.2(3) . . ? C21 N11 Re1B 116.6(4) . . ? C51 N11 Re1B 119.5(5) . . ? C11 P11 C52 107.1(2) . . ? C11 P11 C12 104.8(2) . . ? C52 P11 C12 113.2(2) . . ? C11 P11 Re1B 105.7(4) . . ? C52 P11 Re1B 134.5(4) . . ? C12 P11 Re1B 87.5(4) . . ? C11 P11 Re1 98.52(15) . . ? C52 P11 Re1 119.39(16) . . ? C12 P11 Re1 111.58(16) . . ? C61 P21 C13 103.5(2) . . ? C61 P21 C53 104.0(2) . . ? C13 P21 C53 112.4(2) . . ? C61 P21 Re1 102.42(14) . . ? C13 P21 Re1 120.68(17) . . ? C53 P21 Re1 111.50(15) . . ? C61 P21 Re1B 93.0(3) . . ? C13 P21 Re1B 105.6(3) . . ? C53 P21 Re1B 132.7(3) . . ? C21 C11 P11 105.4(3) . . ? C21 C11 H11A 110.7 . . ? P11 C11 H11A 110.7 . . ? C21 C11 H11B 110.7 . . ? P11 C11 H11B 110.7 . . ? H11A C11 H11B 108.8 . . ? C31 C21 N11 109.2(4) . . ? C31 C21 C11 133.8(4) . . ? N11 C21 C11 117.1(4) . . ? C21 C31 C41 107.3(4) . . ? C21 C31 H31 126.4 . . ? C41 C31 H31 126.4 . . ? C51 C41 C31 107.0(4) . . ? C51 C41 H41 126.5 . . ? C31 C41 H41 126.5 . . ? C41 C51 N11 108.8(4) . . ? C41 C51 C61 130.9(4) . . ? N11 C51 C61 120.3(4) . . ? C51 C61 P21 110.1(3) . . ? C51 C61 H61A 109.6 . . ? P21 C61 H61A 109.6 . . ? C51 C61 H61B 109.6 . . ? P21 C61 H61B 109.6 . . ? H61A C61 H61B 108.2 . . ? C32 C12 C42 109.8(4) . . ? C32 C12 C22 107.5(4) . . ? C42 C12 C22 107.9(4) . . ? C32 C12 P11 111.4(3) . . ? C42 C12 P11 111.3(4) . . ? C22 C12 P11 108.9(3) . . ? C12 C22 H22A 109.5 . . ? C12 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C12 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C12 C32 H32A 109.5 . . ? C12 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C12 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C12 C42 H42A 109.5 . . ? C12 C42 H42B 109.5 . . ? H42A C42 H42B 109.5 . . ? C12 C42 H42C 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? C82 C52 C62 107.9(5) . . ? C82 C52 C72 110.6(5) . . ? C62 C52 C72 107.8(4) . . ? C82 C52 P11 112.5(4) . . ? C62 C52 P11 107.5(3) . . ? C72 C52 P11 110.3(4) . . ? C52 C62 H62A 109.5 . . ? C52 C62 H62B 109.5 . . ? H62A C62 H62B 109.5 . . ? C52 C62 H62C 109.5 . . ? H62A C62 H62C 109.5 . . ? H62B C62 H62C 109.5 . . ? C52 C72 H72A 109.5 . . ? C52 C72 H72B 109.5 . . ? H72A C72 H72B 109.5 . . ? C52 C72 H72C 109.5 . . ? H72A C72 H72C 109.5 . . ? H72B C72 H72C 109.5 . . ? C52 C82 H82A 109.5 . . ? C52 C82 H82B 109.5 . . ? H82A C82 H82B 109.5 . . ? C52 C82 H82C 109.5 . . ? H82A C82 H82C 109.5 . . ? H82B C82 H82C 109.5 . . ? C33 C13 C23 109.9(4) . . ? C33 C13 C43 109.0(4) . . ? C23 C13 C43 107.9(4) . . ? C33 C13 P21 109.7(3) . . ? C23 C13 P21 114.3(4) . . ? C43 C13 P21 105.8(3) . . ? C13 C23 H23A 109.5 . . ? C13 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C13 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C13 C33 H33A 109.5 . . ? C13 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C13 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C13 C43 H43A 109.5 . . ? C13 C43 H43B 109.5 . . ? H43A C43 H43B 109.5 . . ? C13 C43 H43C 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? C73 C53 C83 108.4(4) . . ? C73 C53 C63 108.5(4) . . ? C83 C53 C63 109.8(4) . . ? C73 C53 P21 106.8(3) . . ? C83 C53 P21 112.7(3) . . ? C63 C53 P21 110.4(3) . . ? C53 C63 H63A 109.5 . . ? C53 C63 H63B 109.5 . . ? H63A C63 H63B 109.5 . . ? C53 C63 H63C 109.5 . . ? H63A C63 H63C 109.5 . . ? H63B C63 H63C 109.5 . . ? C53 C73 H73A 109.5 . . ? C53 C73 H73B 109.5 . . ? H73A C73 H73B 109.5 . . ? C53 C73 H73C 109.5 . . ? H73A C73 H73C 109.5 . . ? H73B C73 H73C 109.5 . . ? C53 C83 H83A 109.5 . . ? C53 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C53 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? N11 Re1B P11 82.6(4) . . ? N11 Re1B Cl1 161.9(6) . . ? P11 Re1B Cl1 104.2(5) . . ? N11 Re1B P21 72.4(4) . . ? P11 Re1B P21 147.9(6) . . ? Cl1 Re1B P21 94.8(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Re1 N1 1.652(4) . ? Re1 N11 2.049(4) . ? Re1 Cl1 2.3992(11) . ? Re1 P11 2.4330(11) . ? Re1 P21 2.4519(11) . ? Cl1 Re1B 2.210(12) . ? N11 C21 1.386(6) . ? N11 C51 1.384(6) . ? N11 Re1B 2.077(13) . ? P11 C11 1.850(5) . ? P11 C52 1.869(5) . ? P11 C12 1.881(5) . ? P11 Re1B 2.206(12) . ? P21 C61 1.851(5) . ? P21 C13 1.879(5) . ? P21 C53 1.886(5) . ? P21 Re1B 2.726(12) . ? C11 C21 1.491(6) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C21 C31 1.365(7) . ? C31 C41 1.430(7) . ? C31 H31 0.9500 . ? C41 C51 1.378(6) . ? C41 H41 0.9500 . ? C51 C61 1.497(6) . ? C61 H61A 0.9900 . ? C61 H61B 0.9900 . ? C12 C32 1.539(7) . ? C12 C42 1.528(7) . ? C12 C22 1.539(7) . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C42 H42A 0.9800 . ? C42 H42B 0.9800 . ? C42 H42C 0.9800 . ? C52 C82 1.539(7) . ? C52 C62 1.537(7) . ? C52 C72 1.526(8) . ? C62 H62A 0.9800 . ? C62 H62B 0.9800 . ? C62 H62C 0.9800 . ? C72 H72A 0.9800 . ? C72 H72B 0.9800 . ? C72 H72C 0.9800 . ? C82 H82A 0.9800 . ? C82 H82B 0.9800 . ? C82 H82C 0.9800 . ? C13 C33 1.525(7) . ? C13 C23 1.539(7) . ? C13 C43 1.543(7) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C53 C73 1.528(7) . ? C53 C83 1.531(7) . ? C53 C63 1.544(7) . ? C63 H63A 0.9800 . ? C63 H63B 0.9800 . ? C63 H63C 0.9800 . ? C73 H73A 0.9800 . ? C73 H73B 0.9800 . ? C73 H73C 0.9800 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C52 P11 C11 C21 164.6(3) . . . . ? C12 P11 C11 C21 -74.9(3) . . . . ? Re1B P11 C11 C21 16.6(5) . . . . ? Re1 P11 C11 C21 40.2(3) . . . . ? C51 N11 C21 C31 -0.6(5) . . . . ? Re1 N11 C21 C31 -169.3(3) . . . . ? Re1B N11 C21 C31 -138.1(5) . . . . ? C51 N11 C21 C11 179.5(4) . . . . ? Re1 N11 C21 C11 10.8(6) . . . . ? Re1B N11 C21 C11 41.9(6) . . . . ? P11 C11 C21 C31 143.5(5) . . . . ? P11 C11 C21 N11 -36.6(5) . . . . ? N11 C21 C31 C41 0.6(5) . . . . ? C11 C21 C31 C41 -179.5(5) . . . . ? C21 C31 C41 C51 -0.3(5) . . . . ? C31 C41 C51 N11 0.0(5) . . . . ? C31 C41 C51 C61 176.6(5) . . . . ? C21 N11 C51 C41 0.3(5) . . . . ? Re1 N11 C51 C41 168.8(3) . . . . ? Re1B N11 C51 C41 136.5(5) . . . . ? C21 N11 C51 C61 -176.7(4) . . . . ? Re1 N11 C51 C61 -8.2(6) . . . . ? Re1B N11 C51 C61 -40.6(6) . . . . ? C41 C51 C61 P21 179.5(4) . . . . ? N11 C51 C61 P21 -4.2(5) . . . . ? C13 P21 C61 C51 137.2(3) . . . . ? C53 P21 C61 C51 -105.2(4) . . . . ? Re1 P21 C61 C51 11.0(4) . . . . ? Re1B P21 C61 C51 30.3(4) . . . . ? C11 P11 C12 C32 -35.2(4) . . . . ? C52 P11 C12 C32 81.2(4) . . . . ? Re1B P11 C12 C32 -140.7(5) . . . . ? Re1 P11 C12 C32 -140.8(4) . . . . ? C11 P11 C12 C42 -158.1(3) . . . . ? C52 P11 C12 C42 -41.7(4) . . . . ? Re1B P11 C12 C42 96.4(5) . . . . ? Re1 P11 C12 C42 96.3(3) . . . . ? C11 P11 C12 C22 83.1(4) . . . . ? C52 P11 C12 C22 -160.5(3) . . . . ? Re1 P11 C12 C22 -22.5(4) . . . . ? C11 P11 C52 C82 67.0(4) . . . . ? C12 P11 C52 C82 -48.0(5) . . . . ? Re1B P11 C52 C82 -158.7(6) . . . . ? Re1 P11 C52 C82 177.6(3) . . . . ? C11 P11 C52 C62 -51.6(4) . . . . ? C12 P11 C52 C62 -166.6(3) . . . . ? Re1B P11 C52 C62 82.7(6) . . . . ? Re1 P11 C52 C62 58.9(4) . . . . ? C11 P11 C52 C72 -168.9(4) . . . . ? C12 P11 C52 C72 76.1(4) . . . . ? Re1B P11 C52 C72 -34.6(7) . . . . ? Re1 P11 C52 C72 -58.3(4) . . . . ? C61 P21 C13 C33 172.3(4) . . . . ? C53 P21 C13 C33 60.8(4) . . . . ? Re1 P21 C13 C33 -74.1(4) . . . . ? Re1B P21 C13 C33 -90.7(4) . . . . ? C61 P21 C13 C23 48.4(4) . . . . ? C53 P21 C13 C23 -63.2(4) . . . . ? Re1 P21 C13 C23 161.9(3) . . . . ? Re1B P21 C13 C23 145.4(4) . . . . ? C61 P21 C13 C43 -70.2(4) . . . . ? C53 P21 C13 C43 178.2(3) . . . . ? Re1 P21 C13 C43 43.3(4) . . . . ? Re1B P21 C13 C43 26.8(4) . . . . ? C61 P21 C53 C73 52.2(4) . . . . ? C13 P21 C53 C73 163.4(3) . . . . ? Re1 P21 C53 C73 -57.5(3) . . . . ? Re1B P21 C53 C73 -55.4(5) . . . . ? C61 P21 C53 C83 -66.8(4) . . . . ? C13 P21 C53 C83 44.5(4) . . . . ? Re1 P21 C53 C83 -176.4(3) . . . . ? Re1B P21 C53 C83 -174.4(4) . . . . ? C61 P21 C53 C63 170.0(3) . . . . ? C13 P21 C53 C63 -78.8(4) . . . . ? Re1 P21 C53 C63 60.3(3) . . . . ? Re1B P21 C53 C63 62.4(5) . . . . ?