Crystallography Open Database

Information card for entry 4500911

Preview

Coordinates	4500911.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H24 N2 Ni4 O32
Calculated formula	C24 H24 N2 Ni4 O32
Title of publication	Construction of 5-Aminodiacetic Isophthalate Based Nickel(II) Complexes with Diverse Topologies through Modulating the Auxiliary Ligands
Authors of publication	Ma, Jie; Jiang, Fei-Long; Chen, Lian; Wu, Ming-Yan; Zhang, Shu-Quan; Han, Dong; Feng, Rui; Hong, Mao-Chun
Journal of publication	Crystal Growth & Design
Year of publication	2011
Journal volume	11
Journal issue	7
Pages of publication	3273
a	12.396 ± 0.009 Å
b	13.007 ± 0.008 Å
c	14.582 ± 0.009 Å
α	63.911 ± 0.018°
β	89.96 ± 0.03°
γ	79.954 ± 0.019°
Cell volume	2072 ± 2 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1
Residual factor for significantly intense reflections	0.0711
Weighted residual factors for significantly intense reflections	0.171
Weighted residual factors for all reflections included in the refinement	0.1966
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179540 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/09.	4500911.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4500911.cif
34682	2012-02-25	../uploads/cif-deposit/cod/cif Adding structures of 4500911 via cif-deposit CGI script.	4500911.cif