Crystallography Open Database

Information card for entry 4502581

Preview

Coordinates	4502581.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C177 H208 Dy26 N25 O154 Zn1.5
Calculated formula	C177 H124 Dy26 N25 O154 Zn1.5
Title of publication	Two 3D Coordination Frameworks Based on Nanosized Huge Ln26(Ln = Dy and Gd) Spherical Clusters
Authors of publication	Huang, Lian; Han, Lijie; Feng, Wenjun; Zheng, Lei; Zhang, Zhibin; Xu, Yan; Chen, Qi; Zhu, Dunru; Niu, Shuyun
Journal of publication	Crystal Growth & Design
Year of publication	2010
Journal volume	10
Journal issue	6
Pages of publication	2548
a	21.107 ± 0.002 Å
b	21.185 ± 0.002 Å
c	36.323 ± 0.004 Å
α	89.001 ± 0.002°
β	82.486 ± 0.002°
γ	68.359 ± 0.002°
Cell volume	14959 ± 3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1092
Residual factor for significantly intense reflections	0.067
Weighted residual factors for significantly intense reflections	0.1677
Weighted residual factors for all reflections included in the refinement	0.1906
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4502581.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4502581.cif
36481	2012-03-01	../uploads/cif-deposit/cod/cif Adding structures of 4502581, 4502582 via cif-deposit CGI script.	4502581.cif