Crystallography Open Database

Information card for entry 4502594

Preview

Coordinates	4502594.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H19 N5 O4 Pb
Calculated formula	C32 H19 N5 O4 Pb
Title of publication	Coordination Behavior of 5,6-Substituted 1,10-Phenanthroline Derivatives and Structural Diversities by Coligands in the Construction of Lead(II) Complexes
Authors of publication	Wang, Xiu-Li; Chen, Yong-Qiang; Gao, Qiang; Lin, Hong-Yan; Liu, Guo-Cheng; Zhang, Jin-Xia; Tian, Ai-Xiang
Journal of publication	Crystal Growth & Design
Year of publication	2010
Journal volume	10
Journal issue	5
Pages of publication	2174
a	15.0313 ± 0.0015 Å
b	15.0313 ± 0.0015 Å
c	20.896 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	4088.7 ± 0.7 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	152
Hermann-Mauguin space group symbol	P 31 2 1
Hall space group symbol	P 31 2"
Residual factor for all reflections	0.0773
Residual factor for significantly intense reflections	0.0431
Weighted residual factors for significantly intense reflections	0.065
Weighted residual factors for all reflections included in the refinement	0.0742
Goodness-of-fit parameter for all reflections included in the refinement	0.946
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179556 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/25.	4502594.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4502594.cif
36486	2012-03-01	../uploads/cif-deposit/cod/cif Adding structures of 4502587, 4502588, 4502589, 4502590, 4502591, 4502592, 4502593, 4502594 via cif-deposit CGI script.	4502594.cif