Crystallography Open Database

Information card for entry 4503112

Preview

Coordinates	4503112.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H21 Cl1.5 O P Rh0.5
Calculated formula	C18 H21 Cl1.5 O P Rh0.5
Title of publication	Synthesis and Solid-State Behavior of Host‒Guest Carbonyl Rh(I) Polymers Assembled through Bidentate Phosphine Ligands
Authors of publication	Janjic, Nikolina; Peli, Giulia; Garlaschelli, Luigi; Sironi, Angelo; Macchi, Piero
Journal of publication	Crystal Growth & Design
Year of publication	2008
Journal volume	8
Journal issue	3
Pages of publication	854
a	9.5077 ± 0.0014 Å
b	18.833 ± 0.003 Å
c	10.5919 ± 0.0016 Å
α	90°
β	109.115 ± 0.003°
γ	90°
Cell volume	1792 ± 0.5 Å³
Cell temperature	240 ± 2 K
Ambient diffraction temperature	240 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0696
Residual factor for significantly intense reflections	0.0453
Weighted residual factors for significantly intense reflections	0.1023
Weighted residual factors for all reflections included in the refinement	0.1148
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4503112.cif
120110	2014-07-12	Adding DOIs to range 4/50 structures.	4503112.cif
41356	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4503109, 4503110, 4503111, 4503112, 4503113, 4503114 via cif-deposit CGI script.	4503112.cif