Crystallography Open Database

Information card for entry 4503114

Preview

Coordinates	4503114.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H38 Cl O2 P2 Rh
Calculated formula	C34 H38 Cl O2 P2 Rh
Title of publication	Synthesis and Solid-State Behavior of Host‒Guest Carbonyl Rh(I) Polymers Assembled through Bidentate Phosphine Ligands
Authors of publication	Janjic, Nikolina; Peli, Giulia; Garlaschelli, Luigi; Sironi, Angelo; Macchi, Piero
Journal of publication	Crystal Growth & Design
Year of publication	2008
Journal volume	8
Journal issue	3
Pages of publication	854
a	9.369 ± 0.002 Å
b	11.834 ± 0.003 Å
c	16.531 ± 0.004 Å
α	74.323 ± 0.005°
β	88.336 ± 0.005°
γ	76.061 ± 0.005°
Cell volume	1711.4 ± 0.7 Å³
Cell temperature	240 ± 2 K
Ambient diffraction temperature	240 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2576
Residual factor for significantly intense reflections	0.0795
Weighted residual factors for significantly intense reflections	0.1884
Weighted residual factors for all reflections included in the refinement	0.2552
Goodness-of-fit parameter for all reflections included in the refinement	0.957
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179562 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/31.	4503114.cif
120110	2014-07-12	Adding DOIs to range 4/50 structures.	4503114.cif
41356	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4503109, 4503110, 4503111, 4503112, 4503113, 4503114 via cif-deposit CGI script.	4503114.cif