Crystallography Open Database

Information card for entry 4505827

Preview

Coordinates	4505827.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H32 Ag2 B2 F8 N4 O2 Si2
Calculated formula	C24 H28 Ag2 B2 F8 N4 O2 Si2
Title of publication	“Cyclic Tetramer” vs “Dimer of Cyclic Dimer”: Subtle Anion Effects on the Cyclization of AgBF4vs AgClO4with Bis(3-pyridyl)dimethylsilane
Authors of publication	Jung, Ok-Sang; Lee, Young-A; Kim, Yun Ju; Hong, Jongki
Journal of publication	Crystal Growth & Design
Year of publication	2002
Journal volume	2
Journal issue	6
Pages of publication	497
a	8.5296 ± 0.0003 Å
b	13.4064 ± 0.0004 Å
c	14.8556 ± 0.0004 Å
α	80.821 ± 0.002°
β	83.5804 ± 0.0019°
γ	76.8349 ± 0.0016°
Cell volume	1627.89 ± 0.09 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0837
Residual factor for significantly intense reflections	0.0588
Weighted residual factors for significantly intense reflections	0.1575
Weighted residual factors for all reflections included in the refinement	0.1872
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179594 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/58.	4505827.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4505827.cif
53947	2012-04-20	cif/ Adding structures of 4505827, 4505828 via cif-deposit CGI script.	4505827.cif