Crystallography Open Database

Information card for entry 4509659

Preview

Coordinates	4509659.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H42 Cu4 N8 O52 P3 V W11
Calculated formula	C40 H42 Cu4 N8 O52 P3 V1.128 W10.872
Title of publication	Hydrothermal Syntheses, Crystal Structures, And Magnetic Properties of a Series of Complexes Constructed from Multinuclear Copper Clusters and Polyoxometalates
Authors of publication	Yang, Hongxun; Guo, Shengping; Tao, Jun; Lin, Jingxiang; Cao, Rong
Journal of publication	Crystal Growth & Design
Year of publication	2009
Journal volume	9
Journal issue	11
Pages of publication	4735
a	12.0086 ± 0.0017 Å
b	12.1777 ± 0.0013 Å
c	13.547 ± 0.002 Å
α	103.265 ± 0.005°
β	108.906 ± 0.006°
γ	90.863 ± 0.004°
Cell volume	1815.6 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.054
Residual factor for significantly intense reflections	0.0395
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.1197
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179632 (current)	2016-03-24	cif/4/50/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/50/96.	4509659.cif
97432	2014-01-29	cif/ Adding structures of 4509656, 4509657, 4509658, 4509659 via cif-deposit CGI script.	4509659.cif