#------------------------------------------------------------------------------ #$Date: 2014-10-07 08:19:40 +0300 (Tue, 07 Oct 2014) $ #$Revision: 124960 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/20/4512073.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4512073 loop_ _publ_author_name '\/Oien, Sigurd' 'Wragg, David' 'Reinsch, Helge' 'Svelle, Stian' 'Bordiga, Silvia' 'Lamberti, Carlo' 'Lillerud, Karl Petter' _publ_section_title ; Detailed Structure Analysis of Atomic Positions and Defects in Zirconium Metal--Organic Frameworks ; _journal_name_full 'Crystal Growth & Design' _journal_page_first 141003125543007 _journal_paper_doi 10.1021/cg501386j _journal_year 2014 _chemical_formula_moiety 'n[C84 H48 O32 Zr6]' _chemical_formula_sum 'C84 H48 O32 Zr6' _chemical_formula_weight 2116.54 _chemical_name_common UiO-67 _chemical_name_systematic ; Zr(IV) biphenyl dicarboxylate metal-organic framework ; _space_group_crystal_system cubic _space_group_IT_number 225 _space_group_name_Hall '-F 4 2 3' _space_group_name_H-M_alt 'F m -3 m' _symmetry_space_group_name_Hall '-F 4 2 3' _symmetry_space_group_name_H-M 'F m -3 m' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _audit_creation_date 2014-04-30 _audit_creation_method ; Olex2 1.2 (compiled 2014.03.20 svn.r2914 for OlexSys, GUI svn.r4816) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 26.8809(3) _cell_length_b 26.8809(3) _cell_length_c 26.8809(3) _cell_measurement_reflns_used 7493 _cell_measurement_temperature 100 _cell_measurement_theta_max 33.40 _cell_measurement_theta_min 2.29 _cell_volume 19423.7(4) _computing_cell_refinement 'APEX2 v2013.6--2 (Bruker AXS)' _computing_data_collection 'APEX2 v2013.6--2 (Bruker AXS)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Diamond v3.2i (Brandenburg, 2012)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'APEX2 v2013.6--2 (Bruker AXS)' _diffrn_ambient_temperature 100 _diffrn_detector 'CCD area detector' _diffrn_detector_area_resol_mean 13.6986 _diffrn_detector_type 'Marmosaic 225' _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Beamline I911-3' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_collimation 'Rh-coated Si focusing mirrors' _diffrn_radiation_monochromator 'Silicon 111' _diffrn_radiation_probe x-ray _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.760 _diffrn_reflns_av_R_equivalents 0.0266 _diffrn_reflns_av_unetI/netI 0.0124 _diffrn_reflns_laue_measured_fraction_full 0.994 _diffrn_reflns_laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 38 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 38 _diffrn_reflns_limit_k_min -38 _diffrn_reflns_limit_l_max 38 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 22259 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 27.129 _diffrn_reflns_theta_max 32.782 _diffrn_reflns_theta_min 2.292 _diffrn_source synchrotron _diffrn_source_type 'Wiggler, Station I911-3, MAX II, MAXLAB' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.418 _exptl_absorpt_correction_T_max 0.7466 _exptl_absorpt_correction_T_min 0.6996 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0945 before and 0.0318 after correction. The Ratio of minimum to maximum transmission is 0.9370. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 0.724 _exptl_crystal_description octahedral _exptl_crystal_F_000 4192 _exptl_crystal_size_max 0.07 _exptl_crystal_size_mid 0.07 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.488 _refine_diff_density_min -0.640 _refine_diff_density_rms 0.046 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 55 _refine_ls_number_reflns 1514 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0232 _refine_ls_R_factor_gt 0.0206 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0306P)^2^+31.5444P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0546 _refine_ls_wR_factor_ref 0.0553 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1382 _reflns_number_total 1514 _reflns_threshold_expression 'I > 2\s(I)' _[local]_cod_data_source_file cg501386j_si_003.cif _[local]_cod_data_source_block dh67_a _cod_original_cell_volume 19423.7(7) _cod_database_code 4512073 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Others Sof(O2B)=0.16667*(1-FVAR(2)) Sof(O2A)=0.16667*FVAR(2) Fixed Sof: C3(0.5) C4(0.5) H3(0.5) H4(0.5) ; _shelx_res_file ; TITL DH67 in Fm-3m CELL 0.76 26.8809 26.8809 26.8809 90 90 90 ZERR 4 0.0003 0.0003 0.0003 0 0 0 LATT 4 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,-Z SYMM -Y,-X,-Z SYMM +Y,-X,+Z SYMM -Y,+X,+Z SYMM +X,+Z,-Y SYMM -X,+Z,+Y SYMM -X,-Z,-Y SYMM +X,-Z,+Y SYMM +Z,+Y,-X SYMM +Z,-Y,+X SYMM -Z,+Y,+X SYMM -Z,-Y,-X SFAC C H O Zr DISP C 0.004 0.002 13.247 DISP H -0 0 0.627 DISP O 0.014 0.007 38.676 DISP Zr -1.967 0.657 2986.787 UNIT 336 192 128.00064 24 L.S. 10 PLAN 20 TEMP -173.15 REM Solution 1 R1 0.136 Rweak 0.007, Alpha = 0.0358 in Fm-3m BOND BOND $H LIST 4 MORE -1 CONF fmap 2 acta SHEL 999 0.7 REM D:/frames/guest/DHMN72_1770/work/DH67_a.hkl WGHT 0.030600 31.544401 FVAR 0.11496 0.48398 ZR1 4 0.407609 0.000000 0.500000 10.12500 0.00219 0.00421 = 0.00421 0.00000 0.00000 0.00000 O1 3 0.368094 0.000000 0.427582 10.50000 0.00719 0.01692 = 0.00845 0.00000 -0.00306 0.00000 PART 1 O2A 3 0.461582 0.038418 0.538418 20.16667 0.00317 0.00317 = 0.00317 0.00101 -0.00101 -0.00101 PART 0 C1 1 0.382689 0.000000 0.382689 10.25000 0.00937 0.01712 = 0.00937 0.00000 -0.00398 0.00000 C2 1 0.343391 0.000000 0.343391 10.25000 0.01106 0.04333 = 0.01106 0.00000 -0.00559 0.00000 C5 1 0.269583 0.000000 0.269583 10.25000 0.01233 0.08739 = 0.01233 0.00000 -0.00740 0.00000 PART 2 O2B 3 0.448085 0.051915 0.551915 -20.16667 0.00674 0.00674 = 0.00674 -0.00121 0.00121 0.00121 PART 0 C3 1 0.355183 -0.011941 0.294643 10.50000 0.01083 0.07606 = 0.01330 -0.00918 -0.00597 0.00667 C4 1 0.318566 -0.012500 0.258330 10.50000 0.01534 0.10165 = 0.01051 -0.01208 -0.00696 0.00484 H3 2 0.392774 -0.018016 0.287769 10.50000 0.04591 H4 2 0.330092 -0.022155 0.225053 10.50000 0.03696 HKLF 4 REM DH67 in Fm-3m REM R1 = 0.0206 for 1382 Fo > 4sig(Fo) and 0.0232 for all 1514 data REM 55 parameters refined using 0 restraints END WGHT 0.0294 32.9479 REM Highest difference peak 0.488, deepest hole -0.640, 1-sigma level 0.046 Q1 1 0.3786 0.1214 0.6214 10.16667 0.05 0.49 Q2 1 0.4286 0.0714 0.5714 10.16667 0.05 0.44 Q3 1 0.3622 0.0000 0.3622 10.25000 0.05 0.39 Q4 1 0.4754 0.0246 0.5639 10.50000 0.05 0.30 Q5 1 0.2500 0.0000 0.2500 10.12500 0.05 0.29 Q6 1 0.3558 -0.1442 0.3558 10.16667 0.05 0.29 Q7 1 0.3896 0.0000 0.4582 10.50000 0.05 0.28 Q8 1 0.4530 0.0000 0.5000 10.12500 0.05 0.27 Q9 1 0.3401 0.0000 0.2739 10.50000 0.05 0.26 Q10 1 0.3568 0.0000 0.3219 10.50000 0.05 0.23 Q11 1 0.2911 0.0000 0.2646 10.50000 0.05 0.23 Q12 1 0.3703 0.0000 0.4175 10.50000 0.05 0.22 Q13 1 0.3976 0.0000 0.4411 10.50000 0.05 0.20 Q14 1 0.3458 0.0000 0.4586 10.50000 0.05 0.19 Q15 1 0.3997 -0.0172 0.4600 11.00000 0.05 0.19 Q16 1 0.3490 0.0000 0.3208 10.50000 0.05 0.19 Q17 1 0.3703 0.0000 0.5209 10.50000 0.05 0.19 Q18 1 0.4734 0.0485 0.5485 10.50000 0.05 0.18 Q19 1 0.2500 -0.2500 0.2500 10.04167 0.05 0.18 Q20 1 0.3460 0.0142 0.3311 11.00000 0.05 0.17 REM The information below was added by Olex2. REM REM R1 = 0.0206 for 1382 Fo > 4sig(Fo) and 0.0232 for all 22480 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.49, deepest hole -0.64 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0232 REM R1_gt = 0.0206 REM wR_ref = 0.0553 REM GOOF = 1.047 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 22480 REM Reflections_gt = 1382 REM Parameters = n/a REM Hole = -0.64 REM Peak = 0.49 REM Flack = n/a ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_group Zr1 Zr 0.40761(2) 0.0000 0.5000 0.00354(7) Uani 1 8 d S T P . O1 O 0.36809(3) 0.0000 0.42758(3) 0.01086(17) Uani 1 2 d S T P . O2A O 0.4616(2) 0.0384(2) 0.5384(2) 0.0032(15) Uani 0.48(2) 6 d S T P 1 C1 C 0.38269(4) 0.0000 0.38269(4) 0.0120(3) Uani 1 4 d S T P . C2 C 0.34339(5) 0.0000 0.34339(5) 0.0218(4) Uani 1 4 d S T P . C5 C 0.26958(5) 0.0000 0.26958(5) 0.0374(6) Uani 1 4 d S T P . O2B O 0.4481(2) 0.0519(2) 0.5519(2) 0.0067(13) Uani 0.52(2) 6 d S T P 2 C3 C 0.35518(7) -0.01194(11) 0.29464(7) 0.0334(10) Uani 0.5 1 d . . . . C4 C 0.31857(7) -0.01250(15) 0.25833(7) 0.0425(15) Uani 0.5 1 d . . . . H3 H 0.3928(11) -0.0180(10) 0.2878(10) 0.046(9) Uiso 0.5 1 d . . . . H4 H 0.3301(10) -0.0222(9) 0.2251(10) 0.037(8) Uiso 0.5 1 d . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr1 0.00219(9) 0.00421(8) 0.00421(8) 0.000 0.000 0.000 O1 0.0072(4) 0.0169(4) 0.0085(4) 0.000 -0.0031(3) 0.000 O2A 0.0032(15) 0.0032(15) 0.0032(15) 0.0010(14) -0.0010(14) -0.0010(14) C1 0.0094(4) 0.0171(8) 0.0094(4) 0.000 -0.0040(6) 0.000 C2 0.0111(5) 0.0433(12) 0.0111(5) 0.000 -0.0056(6) 0.000 C5 0.0123(6) 0.087(2) 0.0123(6) 0.000 -0.0074(7) 0.000 O2B 0.0067(13) 0.0067(13) 0.0067(13) -0.0012(14) 0.0012(14) 0.0012(14) C3 0.0108(7) 0.076(3) 0.0133(7) -0.0092(9) -0.0060(6) 0.0067(9) C4 0.0153(7) 0.102(4) 0.0105(7) -0.0121(11) -0.0070(6) 0.0048(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0040 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0140 0.0070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zr Zr -1.9670 0.6570 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O1 Zr1 O1 122.76(4) 41_545 138 O1 Zr1 O1 76.736(19) 138 . O1 Zr1 O1 76.736(19) 41_545 . O1 Zr1 O1 76.735(19) 41_545 98_556 O1 Zr1 O1 76.735(19) 138 98_556 O1 Zr1 O1 122.76(4) 98_556 . O1 Zr1 O2B 140.79(5) 98_556 4_556 O1 Zr1 O2B 71.80(19) 138 98_556 O1 Zr1 O2B 140.79(5) 138 4_556 O1 Zr1 O2B 71.80(19) . 4_556 O1 Zr1 O2B 140.79(5) 98_556 98_556 O1 Zr1 O2B 140.79(5) 138 99 O1 Zr1 O2B 71.80(19) . 98_556 O1 Zr1 O2B 140.79(5) . 99 O1 Zr1 O2B 71.80(19) 41_545 99 O1 Zr1 O2B 140.79(5) 41_545 . O1 Zr1 O2B 71.80(19) 98_556 99 O1 Zr1 O2B 71.80(19) 138 . O1 Zr1 O2B 140.79(5) 41_545 98_556 O1 Zr1 O2B 71.80(19) 98_556 . O1 Zr1 O2B 140.79(5) . . O1 Zr1 O2B 71.80(19) 41_545 4_556 O2A Zr1 O1 141.07(5) . 41_545 O2A Zr1 O1 141.07(5) 99 . O2A Zr1 O1 84.1(2) 98_556 138 O2A Zr1 O1 84.1(2) 99 41_545 O2A Zr1 O1 84.1(2) . 138 O2A Zr1 O1 84.1(2) 99 98_556 O2A Zr1 O1 141.07(5) . . O2A Zr1 O1 141.07(5) 98_556 98_556 O2A Zr1 O1 84.1(2) 98_556 . O2A Zr1 O1 141.07(5) 4_556 98_556 O2A Zr1 O1 141.07(5) 99 138 O2A Zr1 O1 141.07(5) 98_556 41_545 O2A Zr1 O1 141.07(5) 4_556 138 O2A Zr1 O1 84.1(2) 4_556 41_545 O2A Zr1 O1 84.1(2) . 98_556 O2A Zr1 O1 84.1(2) 4_556 . O2A Zr1 O2A 60.2(4) 98_556 4_556 O2A Zr1 O2A 90.4(6) . 4_556 O2A Zr1 O2A 90.4(6) 99 98_556 O2A Zr1 O2A 60.2(4) . 99 O2A Zr1 O2A 60.2(4) 99 4_556 O2A Zr1 O2A 60.2(4) . 98_556 O2B Zr1 O2B 76.5(2) . 99 O2B Zr1 O2B 76.5(2) 4_556 98_556 O2B Zr1 O2B 76.5(2) . 98_556 O2B Zr1 O2B 76.5(2) 4_556 99 O2B Zr1 O2B 122.3(5) . 4_556 O2B Zr1 O2B 122.3(5) 99 98_556 C1 O1 Zr1 133.37(8) . . Zr1 O2A Zr1 117.09(17) . 177_556 Zr1 O2A Zr1 117.09(17) 125_655 177_556 Zr1 O2A Zr1 117.09(18) . 125_655 O1 C1 O1 126.02(14) . 22 O1 C1 C2 116.99(7) . . O1 C1 C2 116.99(7) 22 . C3 C2 C1 120.45(10) 120 . C3 C2 C1 120.46(10) . . C3 C2 C1 120.45(10) 22 . C3 C2 C1 120.45(10) 99 . C3 C2 C3 112.3(2) 22 99 C3 C2 C3 26.8(2) . 99 C3 C2 C3 119.1(2) 120 99 C3 C2 C3 119.1(2) . 22 C3 C2 C3 112.3(2) . 120 C3 C2 C3 26.8(2) 120 22 C4 C5 C5 121.01(10) . 145 C4 C5 C5 121.00(10) 120 145 C4 C5 C5 121.00(10) 22 145 C4 C5 C5 121.00(10) 99 145 C4 C5 C4 118.0(2) 99 120 C4 C5 C4 110.7(2) . 120 C4 C5 C4 118.0(2) . 22 C4 C5 C4 27.9(3) 22 120 C4 C5 C4 27.9(3) . 99 C4 C5 C4 110.7(2) 99 22 Zr1 O2B Zr1 102.4(3) 125_655 177_556 Zr1 O2B Zr1 102.4(3) 125_655 . Zr1 O2B Zr1 102.4(3) . 177_556 C2 C3 C4 110.84(19) . 99 C2 C3 H3 115.2(16) . . C3 C3 C2 76.61(12) 99 . C3 C3 C4 90.6(2) 99 . C3 C3 C4 64.65(17) 99 99 C3 C3 H3 99.0(15) 99 . C4 C3 C2 120.39(18) . . C4 C3 C4 26.0(3) . 99 C4 C3 H3 124.3(16) . . C4 C3 H3 125.3(16) 99 . C5 C4 C3 111.4(2) . 99 C5 C4 H4 124.1(16) . . C3 C4 C5 121.06(19) . . C3 C4 C3 24.7(2) . 99 C3 C4 H4 114.9(16) . . C3 C4 H4 119.4(16) 99 . C4 C4 C5 76.04(16) 99 . C4 C4 C3 64.64(17) 99 99 C4 C4 C3 89.4(2) 99 . C4 C4 H4 105.3(15) 99 . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Zr1 O1 2.2176(8) 41_545 Zr1 O1 2.2176(8) . Zr1 O1 2.2176(8) 98_556 Zr1 O1 2.2176(8) 138 Zr1 O2A 2.059(2) . Zr1 O2A 2.059(2) 4_556 Zr1 O2A 2.059(2) 99 Zr1 O2A 2.059(2) 98_556 Zr1 O2B 2.254(5) . Zr1 O2B 2.254(5) 98_556 Zr1 O2B 2.254(5) 99 Zr1 O2B 2.254(5) 4_556 O1 C1 1.2689(11) . O2A Zr1 2.059(2) 177_556 O2A Zr1 2.059(2) 125_655 C1 O1 1.2690(11) 22 C1 C2 1.494(2) . C2 C3 1.386(2) 22 C2 C3 1.386(2) 99 C2 C3 1.386(2) 120 C2 C3 1.386(2) . C5 C5 1.489(4) 145 C5 C4 1.392(2) 120 C5 C4 1.392(2) . C5 C4 1.392(2) 99 C5 C4 1.392(2) 22 O2B Zr1 2.254(5) 125_655 O2B Zr1 2.254(5) 177_556 C3 C3 0.642(6) 99 C3 C4 1.534(3) 99 C3 C4 1.386(2) . C3 H3 1.04(3) . C4 C3 1.534(3) 99 C4 C4 0.672(8) 99 C4 H4 0.98(3) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 Zr1 O1 C1 O1 0.000(0) . 22 Zr1 O1 C1 C2 180.000(0) . . O1 C1 C2 C3 164.41(14) . 99 O1 C1 C2 C3 15.59(14) . 22 O1 C1 C2 C3 164.41(14) 22 120 O1 C1 C2 C3 -164.41(14) . . O1 C1 C2 C3 -164.41(14) 22 22 O1 C1 C2 C3 15.59(14) 22 . O1 C1 C2 C3 -15.59(14) 22 99 O1 C1 C2 C3 -15.59(14) . 120 C1 C2 C3 C3 -98.05(8) . 99 C1 C2 C3 C4 -153.88(16) . 99 C1 C2 C3 C4 179.2(2) . . C2 C3 C4 C5 1.6(5) . . C2 C3 C4 C3 74.8(2) . 99 C2 C3 C4 C4 74.8(2) . 99 C5 C5 C4 C3 179.2(2) 145 . C5 C5 C4 C3 153.73(14) 145 99 C5 C5 C4 C4 98.59(10) 145 99 C3 C2 C3 C3 110.78(19) 120 99 C3 C2 C3 C3 81.95(8) 22 99 C3 C2 C3 C4 -0.8(2) 22 . C3 C2 C3 C4 -82.7(3) 99 . C3 C2 C3 C4 28.1(4) 120 . C3 C2 C3 C4 55.0(3) 120 99 C3 C2 C3 C4 26.12(16) 22 99 C3 C2 C3 C4 -55.8(2) 99 99 C3 C3 C4 C5 -73.2(3) 99 . C3 C3 C4 C4 0.008(1) 99 99 C4 C5 C4 C3 -55.9(4) 120 99 C4 C5 C4 C3 55.1(2) 99 99 C4 C5 C4 C3 -26.28(14) 22 99 C4 C5 C4 C3 80.6(3) 99 . C4 C5 C4 C3 -30.4(5) 120 . C4 C5 C4 C3 -0.8(2) 22 . C4 C5 C4 C4 -81.41(10) 22 99 C4 C5 C4 C4 -111.1(2) 120 99 C4 C3 C4 C5 -73.3(3) 99 . C4 C3 C4 C3 -0.008(1) 99 99 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 0 2 1340.57 29.1 -2 2 0 1361.66 29.3 0 2 2 1337.67 29.2 2 -2 0 1347.27 29.3 2 0 -2 1319.37 29.1 -1 -3 -1 1643.44 35.6 -1 -3 1 1618.94 35.5 -1 1 3 1663.53 35.5 -1 3 -1 1627.24 35.6 -1 3 1 1617.64 35.6 1 -3 -1 1647.04 35.6 1 -3 1 1626.84 35.6 1 -1 -3 1701.53 35.5 1 3 -1 1581.74 35.5 1 3 1 1634.94 35.6 3 -1 -1 1653.73 35.6 -3 1 3 5.6 0.9 -3 3 1 6.1 1.1 -1 -3 -3 8.1 1 -1 -3 3 8.5 0.7 -1 3 3 5.2 0.9 1 -3 -3 6.7 1 1 3 3 9.6 1 3 -3 -1 8.2 1.1 3 -3 1 5.6 1.1 3 -1 -3 7.1 0.9 3 1 -3 7.8 0.7 -3 3 3 3715.13 79.69 3 -3 -3 3606.64 79.59 -2 -4 0 963.3 21.1 -2 4 0 977.5 21.3 0 -2 -4 994.7 21.2 0 2 4 949.51 21.2 2 -4 0 976.2 21.3 2 4 0 968.2 21.2 -2 0 4 985.7 21.1 0 -4 -2 958.6 21.3 0 -4 2 945.41 21.2 0 4 -2 961.6 21.2 0 4 2 953.4 21.3 2 0 -4 967.2 21.1 -4 2 2 172.08 4.3 -2 -4 -2 163.78 4.1 -2 -4 2 165.78 3.9 -2 2 4 159.58 4.1 -2 4 2 168.48 4.3 2 -4 -2 167.88 4.3 2 -4 2 162.78 4.3 2 -2 -4 168.38 4.1 2 4 -2 166.48 3.9 2 4 2 157.78 4.1 4 -2 -2 165.08 4.3 -4 0 4 837.22 18.7 -4 4 0 846.72 19.1 0 -4 -4 869.51 18.9 0 -4 4 856.01 18.8 0 4 4 868.31 18.9 4 -4 0 857.11 19.1 4 0 -4 836.52 18.7 -4 2 4 1146.29 23.8 -4 4 2 1072.49 23.9 -2 -4 4 1064.59 23.4 -2 4 4 1077.59 23.8 2 -4 -4 1097.09 23.8 2 4 4 1087.49 23.8 4 -4 -2 1069.19 23.9 4 -2 -4 995.4 23.7 -4 4 4 319.47 7.9 4 -4 -4 321.47 7.8 -1 -5 -1 1052.79 22.9 -1 -5 1 1025 22.8 -1 1 5 1054.19 22.8 -1 5 -1 1039.9 23 -1 5 1 1007.1 23 1 -5 -1 1038.3 23 1 -5 1 1063.59 22.9 1 -1 -5 1030.5 22.8 1 5 -1 1028 22.8 1 5 1 1025.8 22.9 -5 1 3 1710.93 37.2 5 -3 -1 1744.23 37.4 -1 -5 3 1705.93 37 -3 5 1 1706.73 37.4 -1 3 5 1758.02 37.2 3 -1 -5 1730.23 37.1 -3 -1 5 1684.03 36.9 1 -5 -3 1734.63 37.3 3 -5 1 1729.13 37.3 3 5 -1 1719.13 37.1 1 5 3 1691.73 37.2 -1 5 -3 1566.04 37.2 5 -1 -3 1652.53 37.2 -3 1 5 1721.43 37.1 -1 -5 -3 1681.63 37.2 -3 5 -1 1790.92 37.4 1 3 5 1686.13 37.2 -1 5 3 1685.43 37.3 3 -5 -1 1724.03 37.3 1 -5 3 1712.23 37.2 1 5 -3 1678.03 37 3 5 1 1681.33 37.2 1 -3 -5 1717.23 37.2 3 1 -5 1707.13 36.9 -3 -5 1 1653.43 37 -5 3 3 474.15 10.8 -3 -5 3 457.45 10.3 -3 3 5 461.05 10.7 -3 5 3 468.85 10.8 3 -5 -3 462.25 10.8 3 -5 3 461.65 10.8 3 -3 -5 458.95 10.6 3 5 -3 471.65 10.3 3 5 3 474.25 10.7 5 -3 -3 442.56 10.7 -5 1 5 1162.58 26 -5 5 1 1156.38 26.3 -1 -5 -5 1153.78 26.1 -1 -5 5 1154.48 25.8 -1 5 5 1186.28 26.1 1 -5 -5 1185.58 26.1 1 5 5 1186.78 26.1 5 -5 -1 1188.28 26.3 5 -5 1 1187.98 26.3 5 -1 -5 1191.08 25.9 5 1 -5 1168.48 25.8 -5 3 5 2359.26 50.69 -5 5 3 2367.86 50.79 -3 5 5 2322.17 50.79 3 -5 -5 2304.07 50.69 3 5 5 2320.97 50.69 5 -5 -3 2286.37 50.79 5 -3 -5 2302.17 50.69 5 5 -3 2306.17 50.29 -5 5 5 1575.64 34.7 5 -5 -5 1556.44 34.6 -2 -6 0 427.86 9.6 -2 6 0 428.96 9.9 0 2 6 423.86 9.6 2 -6 0 430.26 9.8 2 6 0 414.16 9.6 2 0 -6 409.66 9.4 0 6 -2 419.26 9.7 0 6 2 415.66 9.8 0 -6 -2 417.06 9.7 0 -6 2 429.66 9.7 -2 0 6 417.16 9.4 2 6 2 116.69 3.6 2 -2 -6 124.89 3.4 2 6 -2 123.79 3.4 2 -6 -2 128.19 3.8 2 -6 2 123.59 3.8 6 -2 -2 128.39 3.8 -2 -6 -2 121.19 3.5 -2 -6 2 120.99 3.3 -2 -2 6 125.09 3 -2 2 6 120.99 3.4 -2 6 -2 122.99 3.8 -2 6 2 122.79 3.8 0 -4 -6 852.61 19.1 0 4 6 857.31 19.1 4 -6 0 836.62 19.3 4 6 0 868.91 18.9 6 0 -4 841.92 18.9 -4 6 0 854.71 19.3 0 6 -4 876.91 19 0 6 4 851.21 19.2 4 0 -6 825.32 18.8 6 -4 0 834.32 19.3 0 -6 4 847.42 18.9 0 -6 -4 874.61 19.1 -4 0 6 830.62 18.8 4 6 -2 1202.28 25.9 2 6 4 1172.18 26.2 -2 -6 4 1173.58 25.9 4 -6 2 1156.48 26.3 2 -6 -4 1187.78 26.3 6 -4 -2 1208.08 26.3 -6 2 4 1170.48 26.2 -4 6 2 1155.98 26.4 -2 4 6 1231.78 26.2 4 -2 -6 1196.48 26.1 -6 4 2 1179.58 26.4 -4 2 6 1172.28 26.1 -2 -6 -4 1176.18 26.2 6 -2 -4 1154.78 26.2 -2 6 4 1150.18 26.3 4 -6 -2 1193.78 26.3 2 -6 4 1210.48 26.2 2 6 -4 1199.08 25.9 4 6 2 1205.38 26.1 2 -4 -6 1175.08 26.1 2 4 6 1187.18 26.2 -6 4 4 826.52 19 -4 4 6 833.82 18.9 -4 6 4 826.82 19.1 4 -6 -4 839.62 19 4 -6 4 870.51 19.1 4 -4 -6 844.52 18.9 4 6 -4 830.52 18.5 4 6 4 856.81 18.9 6 -4 -4 851.11 19 -6 0 6 1307.77 28.9 -6 6 0 1284.47 29.4 0 -6 -6 1353.36 29.2 0 -6 6 1361.16 29 0 6 6 1320.27 29.2 6 -6 0 1184.48 29.3 6 0 -6 1363.66 28.9 -6 2 6 2135.19 47.2 -6 6 2 2103.99 47.5 -2 -6 -6 2149.39 47.2 -2 -6 6 2070.89 46.8 -2 6 6 2206.88 47.4 2 -6 -6 2180.58 47.3 2 6 6 2127.99 47.3 6 -6 -2 2153.78 47.4 6 -6 2 2313.77 47.5 6 -2 -6 2132.99 47.1 6 2 -6 2142.69 46.8 6 6 -2 2177.38 46.9 -6 4 6 3117.99 68.99 -6 6 4 3140.29 69.09 -4 6 6 3143.79 69.09 4 -6 -6 3204.68 68.99 4 6 6 3126.09 68.99 6 -6 -4 3156.18 69.09 6 -4 -6 3140.29 68.89 6 6 -4 3253.97 68.49 -6 6 6 7771.82 166.98 6 -6 -6 7619.54 166.88 -1 -7 -1 2718.03 59.59 -1 -7 1 2751.92 59.59 -1 1 7 2755.32 59.49 -1 7 -1 2696.83 59.69 -1 7 1 2761.42 59.69 1 -7 -1 2735.93 59.69 1 -7 1 2744.93 59.69 1 7 -1 2721.73 59.59 1 7 1 2756.52 59.69 -3 -7 -1 180.78 4.7 1 -7 -3 178.28 4.9 -3 -1 7 171.38 4.3 -3 7 1 179.68 5.1 -1 3 7 179.58 4.7 3 -1 -7 174.18 4.4 7 -3 -1 173.08 5.1 -1 -7 3 178.68 4.6 3 -7 1 176.88 5 3 7 -1 170.58 4.6 -1 7 -3 170.18 4.8 1 7 3 176.98 4.9 3 7 1 177.78 4.7 1 3 7 185.38 4.7 -3 -7 1 178.98 4.5 3 -7 -1 184.18 5 1 7 -3 174.88 4.7 7 -1 -3 175.98 4.9 1 -3 -7 171.58 4.7 -1 7 3 175.38 5 1 -7 3 171.38 4.8 -1 -7 -3 175.58 4.8 -3 1 7 183.58 4.5 -3 7 -1 167.28 5 -3 7 -3 28.5 2.1 -3 3 7 31.4 2 -3 -7 3 27.7 1.5 -3 -7 -3 24.8 1.8 -7 3 3 27.7 2.1 7 -3 -3 26.2 2 3 -7 -3 29.6 2.1 3 -7 3 26.9 2 3 -3 -7 30.1 1.8 3 7 -3 29.3 1.6 3 7 3 22.7 1.7 -3 7 3 25.5 2.1 -5 -1 7 611.04 13.8 5 -7 1 615.74 14.4 5 7 -1 627.74 14 -1 -7 5 622.14 13.9 -1 5 7 594.34 14.2 7 1 -5 615.64 13.9 -7 1 5 618.44 14.2 5 -1 -7 624.54 14 -5 7 1 652.53 14.5 -1 -5 -7 615.34 14.2 1 7 5 633.54 14.3 1 -7 -5 618.04 14.3 7 -5 -1 644.44 14.5 1 7 -5 641.74 14 7 -1 -5 615.04 14.1 -5 7 -1 601.34 14.5 5 1 -7 615.84 13.7 1 5 7 633.04 14.2 7 -5 1 619.14 14.5 -1 7 5 617.74 14.3 1 -5 -7 611.64 14.2 1 -7 5 602.74 14.1 5 7 1 616.44 14.1 5 -7 -1 610.64 14.4 -5 1 7 618.54 14 -1 -7 -5 628.74 14.2 7 -5 -3 1423.46 32.5 5 -7 3 1469.55 32.5 5 7 -3 1453.25 32 5 -3 -7 1495.55 32.2 -7 3 5 1484.25 32.4 -5 7 3 1426.96 32.5 -3 5 7 1438.46 32.4 3 7 5 1455.95 32.4 3 -7 -5 1480.95 32.4 -3 -7 5 1458.95 31.9 3 -5 -7 1469.25 32.3 -5 3 7 1447.56 32.3 -7 5 3 1439.16 32.5 -3 7 5 1441.66 32.5 3 5 7 1461.85 32.3 3 -7 5 1554.24 32.4 3 7 -5 1456.05 31.9 5 -7 -3 1424.56 32.5 5 7 3 1459.55 32.3 7 -3 -5 1522.35 32.4 -7 5 5 2707.83 60.19 -5 5 7 2738.83 60.09 -5 7 5 2813.12 60.29 5 -7 -5 2744.03 60.19 5 -7 5 2670.73 60.29 5 -5 -7 2842.72 60.09 5 7 -5 2775.12 59.59 5 7 5 2731.13 60.09 7 -5 -5 2702.93 60.09 -7 1 7 350.16 8.4 -7 7 1 350.46 9 -1 -7 -7 334.07 8.5 -1 -7 7 349.96 8.1 -1 7 7 353.46 8.7 1 -7 -7 354.26 8.6 1 -7 7 339.97 8.4 1 7 7 334.97 8.6 7 -7 -1 333.77 8.9 7 -7 1 335.57 8.9 7 -1 -7 344.67 8.3 7 1 -7 357.16 8.1 7 7 -1 347.97 8.2 -7 3 7 1653.63 36.3 -7 7 3 1628.94 36.5 -3 -7 7 1662.63 35.7 -3 7 7 1615.24 36.4 3 -7 -7 1585.74 36.3 3 7 7 1599.74 36.3 7 -7 -3 1685.03 36.5 7 -7 3 1649.63 36.6 7 -3 -7 1658.03 36.2 7 3 -7 1671.33 35.7 7 7 -3 1651.23 35.9 -7 5 7 5491.05 122.39 -7 7 5 5525.65 122.49 -5 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11 11 451.45 11.7 11 -11 -5 457.15 12.1 11 -11 5 443.86 12.3 11 -5 -11 452.35 11.6 11 11 -5 453.55 10.8 11 11 5 459.75 11.6 -11 7 11 1916.81 43.8 -11 11 7 1905.41 44 -7 11 11 1905.91 43.9 7 -11 -11 2017.7 43.7 7 -11 11 2002.8 44 7 11 11 1970.3 43.6 11 -11 -7 1945.81 43.8 11 -11 7 1971.6 44.1 11 -7 -11 1909.71 43.6 11 11 -7 1978.8 42.7 11 11 7 1941.81 43.5 -11 9 11 2000.2 45.1 -11 11 9 2014.3 45.2 -9 11 11 1989.9 45.1 9 -11 -11 1929.31 44.8 9 -11 11 2136.29 45.3 9 11 11 1933.51 44.8 11 -11 -9 1992.1 45 11 -11 9 2057.99 45.4 11 -9 -11 1979.6 44.8 11 11 9 2005.5 44.7 -11 11 11 2194.38 48.1 11 -11 -11 2015.2 47.7 11 11 11 2193.98 47.7 0 -12 0 9318.47 197.98 0 0 12 9001.7 197.68 0 12 0 9084.19 198.08 -2 -12 0 399.26 9.8 -2 12 0 394.66 10.2 0 2 12 396.96 9.7 2 -12 0 400.66 10.1 2 12 0 397.66 10 -2 0 12 402.86 9.5 0 -12 -2 402.26 9.9 0 -12 2 400.46 9.9 0 12 -2 390.26 10.1 0 12 2 397.56 10.1 2 -12 2 134.99 4.9 2 2 12 138.79 4.6 2 12 -2 135.39 4.9 2 12 2 136.19 5.1 -2 12 2 133.99 5.3 2 -12 -2 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12 4 -8 151.68 5 -4 8 12 156.78 6.1 -4 12 8 145.49 6.2 -8 4 12 153.18 5.8 12 -8 4 152.98 5.9 4 12 -8 153.48 5 4 -12 8 154.68 6 12 -4 -8 157.38 5.9 4 -8 -12 157.48 5.6 4 8 12 152.08 5.7 8 -12 -4 151.48 6.1 8 12 4 157.18 5.7 6 12 8 2 2.4 6 -12 -8 0.6 2.6 -8 12 6 4 3.1 -6 8 12 2.8 2.8 8 12 -6 1.4 2 12 6 -8 3.1 1.9 12 -8 -6 3.5 2.8 8 -12 6 2.9 2.9 8 -6 -12 4.1 2.4 -12 6 8 4.6 2.9 8 12 6 1.9 2.5 -6 12 8 4.4 3 6 -12 8 1.1 2.9 6 12 -8 0.8 1.9 6 8 12 1.1 2.4 6 -8 -12 4.6 2.5 -8 6 12 2.7 2.6 12 -6 -8 5 2.8 8 -12 -6 1.5 2.7 -12 8 6 3.5 3 8 -8 -12 41.9 3.3 8 8 12 38.3 3.4 -12 8 8 40.3 3.8 8 -12 8 33 3.7 8 12 -8 39.1 2.4 8 12 8 34.2 3.2 8 -12 -8 43.6 3.7 -8 12 8 36.7 3.9 12 -8 -8 38.7 3.7 -8 8 12 40.5 3.6 0 -12 -10 3373.46 74.59 12 0 -10 3452.15 74.29 0 -10 -12 3339.27 74.59 0 -10 12 3394.06 74.29 0 10 12 3394.26 74.69 10 -12 0 3324.07 74.89 10 12 0 3445.86 74.39 12 -10 0 3401.46 74.99 -10 0 12 3424.16 74.29 0 12 10 3362.96 74.69 10 0 -12 3387.46 74.09 0 -12 10 3503.35 74.39 12 2 -10 2319.67 49.99 10 12 -2 2318.77 50.19 -10 12 2 2213.18 50.99 2 -12 -10 2276.57 50.59 -2 10 12 2291.67 50.69 2 12 10 2300.17 50.69 -2 -12 10 2288.17 49.99 12 -10 -2 2247.38 50.89 10 -12 2 2182.08 50.89 2 -10 12 2281.87 50.49 10 -2 -12 2327.77 50.19 10 12 2 2282.47 50.39 2 -12 10 2310.37 50.49 2 -10 -12 2258.07 50.49 12 -10 2 2270.87 50.99 -10 2 12 2322.37 50.39 -2 -12 -10 2278.17 50.49 10 -12 -2 2252.87 50.89 -2 12 10 2248.88 50.79 -2 -10 12 2365.66 49.9 10 2 -12 2349.06 49.8 12 -2 -10 2325.97 50.39 12 10 -2 2266.47 50.19 2 10 12 2198.68 50.59 10 12 -4 625.94 14.8 10 -12 4 613.04 15.9 12 4 -10 664.93 14.5 -4 -12 10 649.04 14.4 -12 4 10 637.34 15.6 -10 12 4 630.24 16 -4 10 12 647.94 15.7 12 -10 -4 634.54 15.9 4 12 10 625.54 15.5 10 -4 -12 641.84 15.2 4 -12 -10 600.74 15.4 12 -4 -10 635.24 15.3 4 10 12 633.94 15.5 10 12 4 638.64 15.3 -4 12 10 631.94 15.7 4 -12 10 673.03 15.6 -12 10 4 599.54 16 -10 4 12 614.04 15.4 4 -10 -12 628.04 15.4 12 -10 4 640.84 16.1 12 10 -4 630.94 14.7 10 -12 -4 639.64 15.8 10 12 -6 368.16 9.1 10 -6 -12 364.36 9.9 10 -12 6 353.76 10.7 -12 6 10 361.16 10.5 6 12 10 360.96 10.1 -6 10 12 381.76 10.4 6 -12 -10 354.86 10.1 -10 12 6 371.26 10.8 12 -10 -6 381.46 10.5 12 -10 6 370.76 11 10 12 6 359.96 10 -10 6 12 361.36 10.4 -6 12 10 348.57 10.5 -12 10 6 358.36 10.7 6 -12 10 375.76 10.5 12 -6 -10 372.16 10.2 6 -10 -12 363.86 10 6 10 12 360.56 10 10 -12 -6 360.86 10.4 12 10 -6 375.26 9 8 -12 -10 1225.38 29.3 -12 8 10 1294.57 29.7 -10 12 8 1282.17 29.7 -8 10 12 1280.97 29.6 10 -8 -12 1274.97 29.3 12 -10 -8 1286.37 29.5 8 12 10 1236.78 29.3 10 -12 8 1322.97 29.8 10 12 -8 1290.67 28.3 10 -12 -8 1245.98 29.5 -12 10 8 1282.67 29.7 -10 8 12 1294.47 29.6 -8 12 10 1236.08 29.6 12 -8 -10 1284.17 29.4 8 -12 10 1346.57 29.7 10 12 8 1250.87 29.3 8 -10 -12 1287.27 29.3 8 10 12 1281.07 29.3 12 -10 8 1341.27 30 -12 10 10 1532.85 36 -10 10 12 1561.14 35.9 -10 12 10 1562.34 36 10 -12 -10 1526.35 35.7 10 -12 10 1568.24 36.1 10 -10 -12 1532.55 35.6 10 10 12 1573.24 35.6 10 12 10 1646.54 35.7 12 -10 -10 1564.64 35.7 12 10 10 1631.54 35.6 0 -12 -12 3878.71 87.79 0 -12 12 4140.39 87.59 0 12 12 4094.09 88.09 12 -12 0 3953.4 88.29 12 0 -12 4071.49 87.39 12 12 0 3928.81 87.59 -12 2 12 1463.05 32.9 -2 -12 12 1442.66 32.3 -2 12 12 1445.06 33.2 2 -12 -12 1444.46 33 2 -12 12 1501.65 32.9 2 12 12 1464.05 33.1 12 -12 -2 1442.76 33.4 12 -12 2 1437.76 33.4 12 -2 -12 1450.85 32.6 12 2 -12 1502.45 32.2 12 12 -2 1427.66 32.5 12 12 2 1457.15 32.8 -12 4 12 623.94 15.3 -12 12 4 595.14 15.8 -4 12 12 612.24 15.5 4 -12 -12 606.54 15.2 4 -12 12 654.23 15.4 4 12 12 621.34 15.3 12 -12 -4 588.14 15.6 12 -12 4 597.64 15.8 12 -4 -12 606.14 14.9 12 12 -4 628.04 14.5 12 12 4 594.54 15 -12 6 12 816.42 19.7 -12 12 6 797.72 20 -6 12 12 798.62 19.8 6 -12 -12 827.82 19.5 6 -12 12 793.82 19.8 6 12 12 820.72 19.5 12 -12 -6 818.02 19.8 12 -12 6 829.52 20.1 12 -6 -12 832.22 19.4 12 12 -6 816.62 18.6 12 12 6 795.12 19.4 -12 8 12 1087.69 25.9 -12 12 8 1067.19 26.1 -8 12 12 1080.29 25.9 8 -12 -12 1116.39 25.6 8 -12 12 1105.69 26.1 8 12 12 1090.29 25.6 12 -12 -8 1061.19 25.8 12 -12 8 1104.59 26.2 12 -8 -12 1115.49 25.6 12 12 -8 1130.59 24.4 12 12 8 1104.19 25.5 -12 10 12 1228.88 29.2 -12 12 10 1258.17 29.4 -10 12 12 1248.48 29.3 10 -12 -12 1239.18 28.9 10 -12 12 1258.97 29.5 10 12 12 1248.08 28.8 12 -12 -10 1204.18 29 12 -12 10 1240.38 29.5 12 -10 -12 1245.18 28.8 12 10 12 1256.67 28.8 12 12 10 1269.57 28.8 -12 12 12 1217.08 28.9 12 -12 -12 1210.78 28.4 12 -12 12 1173.48 29 12 12 12 1253.67 28.4 -1 -13 -1 3643.74 78.99 -1 -13 1 3621.44 78.89 -1 -1 13 3624.64 78.69 -1 1 13 3599.94 78.79 -1 13 -1 3524.55 79.09 -1 13 1 3631.14 79.19 1 -13 -1 3632.64 79.09 1 -13 1 3617.04 78.99 1 1 13 3683.43 78.79 1 13 -1 3608.64 79.09 1 13 1 3576.54 79.09 -3 -13 -1 30.7 2.6 -1 13 -3 37.5 3.1 -1 -13 3 33.8 2.6 -3 13 1 38.3 3.3 -1 3 13 37.6 2.6 -3 -1 13 35.6 2.2 1 -13 -3 32.9 2.7 3 -13 1 35.2 2.9 3 13 -1 34.5 2.7 1 13 3 35.5 3 3 -13 -1 34 3 1 -13 3 33.7 2.8 1 13 -3 35.3 2.9 -3 -13 1 40.8 2.7 3 13 1 34 2.9 -1 13 3 31.6 3 1 3 13 33.3 2.7 -3 1 13 35.5 2.4 -1 -13 -3 35 2.6 -3 13 -1 31.6 3.1 -3 -13 -3 656.63 15.6 -3 -13 3 645.34 15.3 3 3 13 664.83 15.6 3 13 -3 682.83 15.6 3 13 3 657.43 15.8 13 -3 -3 666.13 16 -3 -3 13 640.34 14.9 -3 3 13 672.53 15.5 -3 13 -3 649.04 16 -3 13 3 654.53 16 3 -13 -3 669.83 15.8 3 -13 3 681.53 15.8 -5 -13 -1 53.19 3 13 1 -5 60.79 3.5 -5 -1 13 59.59 2.7 -5 13 1 54.29 3.7 5 -13 1 47 3.3 -1 -13 5 55.09 3.1 -1 13 -5 57.69 3.6 -1 5 13 58.89 3.3 1 -13 -5 53.79 3.5 1 13 5 57.29 3.6 13 -5 -1 55.49 3.9 5 13 -1 59.69 3.3 1 13 -5 60.09 3.4 13 -1 -5 54.39 3.4 -5 -13 1 59.49 3 -5 13 -1 54.09 3.8 -5 1 13 62.79 3 5 -13 -1 60.69 3.6 5 13 1 54.99 3.3 -1 -13 -5 57.59 3.3 1 -13 5 56.49 3.3 1 5 13 62.49 3.4 -1 13 5 48.8 3.5 5 -3 -13 506.25 12.2 -3 5 13 497.05 12.5 5 -13 3 503.55 12.8 13 -5 -3 515.05 13 -5 13 3 521.25 13.1 -5 -13 -3 514.85 12.3 3 13 5 512.65 12.7 -5 -3 13 518.05 11.6 3 -13 -5 514.75 12.7 5 13 -3 503.95 12.3 -3 -13 5 492.95 12 -3 13 -5 503.05 12.8 -5 3 13 501.95 12.4 3 13 -5 522.05 12.4 -3 13 5 503.95 12.9 -3 -5 13 518.85 11.5 13 -3 -5 518.95 12.8 3 -5 -13 506.25 12.3 3 5 13 495.45 12.4 5 13 3 502.45 12.5 3 -13 5 512.05 12.6 -3 -13 -5 511.45 12.5 -5 13 -3 508.35 13 5 -13 -3 493.55 12.7 -5 -13 3 507.35 12 -5 5 13 134.29 5.5 5 13 5 141.99 5.5 5 -5 -13 132.39 5.1 5 5 13 141.89 5.4 5 13 -5 132.09 5 -5 13 5 148.49 5.8 5 -13 -5 139.59 5.7 -5 -13 5 134.39 4.5 -5 -13 -5 135.99 5.3 13 -5 -5 152.38 5.8 5 -13 5 137.19 5.9 1 -13 -7 564.84 14.1 1 13 7 580.34 14.3 7 -1 -13 589.04 13.5 -7 13 1 566.64 14.6 -7 -1 13 637.24 13.5 7 13 -1 587.34 13.9 13 -7 -1 571.44 14.6 -1 7 13 579.94 14.1 13 1 -7 579.74 13.9 7 -13 1 574.14 14.4 -1 -13 7 565.84 13.7 7 -13 -1 569.54 14.4 1 -7 -13 576.24 13.9 1 13 -7 592.34 14 13 -7 1 585.54 14.7 -7 13 -1 570.24 14.6 1 -13 7 573.44 13.9 13 -1 -7 578.14 14 -1 13 7 568.54 14.4 1 7 13 576.84 14 7 13 1 554.94 13.9 -7 1 13 578.64 13.7 -1 -13 -7 583.24 14.1 7 -3 -13 180.38 5.6 -3 -13 7 183.78 5.4 3 -13 -7 176.28 6.2 7 -13 3 164.18 6.6 -7 13 3 181.38 6.9 13 -7 -3 170.68 6.7 -3 7 13 166.28 6.2 7 13 -3 176.28 5.7 3 13 7 180.58 6.3 13 3 -7 167.68 5.7 3 -7 -13 162.88 5.9 13 -3 -7 181.88 6.4 13 -7 3 169.88 7.1 -3 13 7 176.48 6.7 7 13 3 173.78 6.1 3 7 13 159.88 6 7 -13 -3 170.88 6.5 3 -13 7 174.88 6.3 -7 3 13 181.38 6 -3 -13 -7 183.88 6.1 3 13 -7 174.48 5.8 -5 -13 7 347.47 8.5 5 -13 -7 337.37 9.6 -5 7 13 352.86 9.6 -7 13 5 346.07 10.2 7 -5 -13 348.87 9.2 7 13 -5 350.66 8.9 5 13 7 361.26 9.6 7 -13 5 351.26 10 13 -7 -5 353.16 10 7 -13 -5 345.27 9.8 5 -13 7 337.17 9.8 5 13 -7 350.06 8.9 5 7 13 336.17 9.4 -7 5 13 348.87 9.5 -5 13 7 348.87 10 13 -5 -7 364.56 9.8 5 -7 -13 345.87 9.3 7 13 5 343.07 9.4 7 13 -7 683.23 15.7 -7 7 13 676.03 16.5 -7 13 7 653.23 16.8 7 -13 -7 691.63 16.5 7 13 7 662.13 16.4 13 -7 -7 668.03 16.6 7 -7 -13 684.83 16.2 7 7 13 683.43 16.3 7 -13 7 682.63 16.7 1 13 9 2170.88 50.39 9 -1 -13 2370.36 49.8 -1 -13 9 2343.37 49.9 -9 -1 13 2258.87 49.7 13 1 -9 2266.77 49.9 1 -13 -9 2248.38 50.29 9 13 -1 2261.17 49.99 9 -13 1 2301.87 50.59 13 -9 -1 2271.07 50.69 -1 9 13 2246.38 50.29 -9 13 1 2225.78 50.69 -9 13 -1 2318.17 50.69 -1 13 9 2235.78 50.49 -9 1 13 2318.17 49.99 -1 -13 -9 2176.68 50.19 9 13 1 2311.37 50.09 13 -1 -9 2324.27 50.09 1 -13 9 2132.09 49.99 9 -13 -1 2204.18 50.49 9 1 -13 2354.46 49.6 1 9 13 2271.37 50.29 1 -9 -13 2230.18 50.19 13 -9 1 2277.17 50.69 -1 -9 13 2294.17 49.8 -3 9 13 135.19 5.4 3 -13 -9 127.49 5.2 13 3 -9 111.69 4.9 -3 -13 9 118.19 4.5 9 13 -3 117.69 5 3 13 9 138.19 5.6 9 -13 3 123.99 5.4 13 -9 -3 142.79 6 -9 13 3 134.29 6 9 -3 -13 122.99 5 3 -9 -13 122.69 5.4 13 -3 -9 143.19 5.2 -3 13 9 126.89 5.5 -3 -13 -9 141.19 5.2 -9 3 13 130.19 5.1 9 13 3 126.89 5.5 3 -13 9 134.99 5.4 9 -13 -3 116.89 5.2 3 9 13 122.69 4.9 13 -9 3 130.89 5.9 5 13 9 6.2 2.9 9 -13 5 6.9 3.3 -5 -13 9 3.5 1.7 13 -9 -5 3.4 3.2 5 -13 -9 5.5 2.7 9 -5 -13 4.2 2.4 -5 9 13 6.1 3 -9 13 5 6.1 3.3 13 5 -9 4.5 2.2 9 13 -5 2.7 2.3 9 13 5 1.2 2.6 5 -9 -13 2.8 2.6 5 9 13 3.5 2.6 5 -13 9 3.5 3.1 -9 5 13 3.7 2.9 13 -9 5 2.7 3.4 13 -5 -9 3.5 2.8 9 -13 -5 3.7 3 -5 13 9 6.2 3.2 7 -13 -9 10.2 3.1 7 13 9 11.7 3.1 9 -7 -13 10.1 3 -7 9 13 11.3 3.3 9 -13 7 10.9 3.6 13 -9 -7 8.1 3.3 -13 7 9 10.4 3.6 -9 13 7 8.5 3.5 9 13 -7 11.9 2.4 -7 13 9 13.8 3.6 -9 7 13 9.6 3.4 13 9 -7 9.5 2.1 7 -13 9 6.5 3.4 7 9 13 14.6 3.2 9 -13 -7 7.9 3.3 13 -7 -9 9.4 3.2 9 13 7 7.9 2.8 7 -9 -13 8.9 2.9 -13 9 7 6 3.6 7 13 -9 10.9 2.2 9 -13 -9 548.55 14.8 9 -9 -13 583.14 14.6 -13 9 9 572.94 15.2 -9 9 13 581.84 15.1 -9 13 9 587.24 15.4 9 9 13 611.24 14.7 13 -9 -9 592.84 15 9 13 9 563.34 14.7 9 -13 9 609.04 15.4 13 -11 -1 2139.29 47.8 -1 -13 11 2123.89 46.9 1 13 11 2075.79 47.5 11 13 -1 2168.78 47.1 1 -13 -11 2152.98 47.4 13 11 1 2168.18 47.2 -1 11 13 2125.99 47.5 13 1 -11 2177.58 46.9 11 -1 -13 2111.89 46.9 1 -11 13 2100.09 47.1 11 -13 1 2144.29 47.8 11 -13 -1 2108.99 47.8 13 -1 -11 2156.88 47.1 13 -11 1 2100.49 47.8 11 13 1 2147.59 47.2 11 1 -13 2191.98 46.7 -1 -11 13 2174.48 46.9 1 -11 -13 2101.69 47.3 1 -13 11 2062.19 47.1 13 11 -1 2158.58 47.1 -11 1 13 2079.29 47.1 1 11 13 2099.99 47.5 -1 -13 -11 2142.79 47.4 -1 13 11 2087.29 47.6 3 -13 -11 342.27 9.7 3 13 11 335.47 9.8 13 3 -11 354.56 8.7 -11 13 3 340.57 10.6 13 11 3 348.87 9.5 -3 11 13 329.57 10 13 -11 -3 350.86 10.4 3 -11 13 358.26 10 11 -13 3 339.87 10.4 11 13 -3 339.67 9.1 -3 -13 11 349.77 8.7 11 -3 -13 342.67 9.3 3 -11 -13 334.87 9.6 3 -13 11 346.77 9.8 13 -11 3 332.97 10.5 13 11 -3 350.56 9.1 -3 -11 13 336.57 8.4 11 13 3 342.87 9.5 13 -3 -11 347.07 9.6 -11 3 13 335.77 9.8 3 11 13 336.47 9.8 -3 13 11 338.87 10.2 11 -13 -3 340.67 10.2 13 11 5 115.39 5.2 5 -11 13 102.49 5.4 13 -11 -5 127.69 6 5 -13 -11 116.39 5.3 11 13 -5 128.39 4.6 11 -5 -13 123.59 5.1 -13 5 11 123.99 5.6 -11 13 5 109.89 5.8 -5 11 13 118.49 5.7 5 13 11 99.59 5 11 -13 5 101.59 5.6 13 11 -5 118.69 4.4 11 -13 -5 106.59 5.2 5 -13 11 122.49 5.5 -5 13 11 125.49 5.8 -13 11 5 106.59 5.8 13 -5 -11 115.79 5.2 13 -11 5 101.89 5.6 5 -11 -13 121.19 5.2 5 11 13 102.19 5.1 -11 5 13 115.89 5.4 11 13 5 110.09 4.9 -7 11 13 354.36 10.8 11 13 -7 368.56 9.4 11 -7 -13 366.06 10.3 7 -13 -11 363.56 10.4 -13 7 11 353.66 10.9 -11 13 7 373.16 11.3 13 11 7 358.46 10.3 7 13 11 363.86 10.5 11 -13 7 366.46 11.3 13 -11 -7 375.36 10.9 -11 7 13 368.96 10.8 -7 13 11 358.56 10.9 11 13 7 365.76 10.4 13 -7 -11 373.06 10.6 7 11 13 373.46 10.4 13 -11 7 356.56 11.4 13 11 -7 379.46 9.2 7 -13 11 370.36 11 11 -13 -7 346.57 10.8 -13 11 7 350.26 11.2 7 -11 -13 360.76 10.4 11 -13 9 684.33 17.9 9 -13 -11 695.63 17.3 9 13 11 685.33 17.2 11 9 13 703.83 17.2 11 -9 -13 708.33 17.2 -9 11 13 676.73 17.7 -13 9 11 704.43 17.8 -11 13 9 691.63 17.9 13 11 9 717.03 17.2 13 -11 -9 680.63 17.5 -11 9 13 698.73 17.7 -9 13 11 712.13 17.9 11 13 9 686.93 17.2 9 -13 11 685.23 17.8 13 -9 -11 683.93 17.4 9 11 13 714.63 17.3 11 -13 -9 701.43 17.5 -13 11 9 678.93 17.9 13 -11 9 697.43 18.1 9 -11 -13 695.43 17.2 -13 11 11 753.12 18.9 -11 11 13 728.83 18.8 -11 13 11 742.03 18.9 11 -13 -11 713.43 18.3 11 -13 11 711.13 18.9 11 -11 -13 716.63 18.2 11 11 13 753.92 18.2 11 13 11 731.43 18.2 13 -11 -11 746.43 18.5 13 11 11 751.62 18.2 -1 -13 -13 1907.41 43.4 -1 -13 13 1928.51 42.9 -1 13 13 1971.7 43.7 1 -13 -13 1897.41 43.4 1 -13 13 1903.01 43.2 1 13 13 1953.9 43.7 13 -13 -1 1894.91 43.9 13 -13 1 1919.01 43.9 13 -1 -13 2050.99 43 13 1 -13 1980.2 42.8 13 13 -1 1925.81 43.1 13 13 1 1929.71 43.2 -13 3 13 4.5 3.6 -3 -13 13 5.6 2.3 -3 13 13 5 3.7 3 -13 -13 3.4 3.1 3 -13 13 5.4 3.6 3 13 13 1.9 3.3 13 -13 -3 3.7 3.8 13 -13 3 3.4 3.7 13 -3 -13 3.6 3 13 3 -13 3.1 2.2 13 13 -3 4 2.9 13 13 3 6.5 3.3 -13 5 13 43.7 4.4 -13 13 5 41 4.8 -5 13 13 38.4 4.2 5 -13 -13 45.1 4.2 5 -13 13 45.2 4.6 5 13 13 41.2 4.2 13 -13 -5 45.5 4.4 13 -13 5 44.8 4.9 13 -5 -13 45.4 3.9 13 13 -5 46.7 3.4 13 13 5 36.1 4 -13 7 13 77.99 5.5 -13 13 7 73.19 5.2 -7 13 13 77.19 5.3 7 -13 -13 81.39 5 7 -13 13 86.49 5.6 7 13 13 61.19 4.3 13 -13 -7 66.69 4.9 13 -13 7 68.79 5.3 13 -7 -13 77.19 4.8 13 13 -7 76.69 3.7 13 13 7 71.19 4.7 -13 9 13 374.36 11.8 -13 13 9 359.06 11.8 -9 13 13 362.36 11.7 9 -13 -13 367.66 10.8 9 -13 13 360.36 11.8 9 13 13 365.96 11 13 -13 -9 362.66 11.3 13 -13 9 358.76 12 13 -9 -13 370.76 11 13 13 9 363.86 11 -13 11 13 328.17 11.4 -13 13 11 335.07 11.6 -11 13 13 338.17 11.7 11 -13 -13 305.47 10.4 11 -13 13 328.57 11.8 11 13 13 326.77 10.5 13 -13 -11 331.37 10.9 13 -13 11 319.87 11.7 13 -11 -13 324.27 10.6 13 11 13 329.07 10.5 13 13 11 327.77 10.6 -13 13 13 594.74 16.7 13 -13 -13 601.24 16.1 13 -13 13 612.54 17.1 13 13 13 589.14 16 0 -14 0 8389.76 180.08 0 0 14 8332.67 179.78 0 14 0 8175.08 180.18 -2 -14 0 942.21 21.2 -2 14 0 932.41 21.6 0 2 14 912.81 21.1 2 -14 0 923.31 21.4 2 14 0 951.9 21.4 0 -14 2 915.41 21.2 0 14 -2 889.11 21.4 0 14 2 918.11 21.5 0 -14 -2 911.61 21.2 -2 0 14 950.1 20.9 -2 -14 2 314.37 8.3 2 14 2 306.47 8.8 -2 14 -2 313.47 9 -2 14 2 303.17 8.9 2 -14 -2 313.27 8.7 -2 -14 -2 307.87 8.4 -2 -2 14 325.67 7.8 -2 2 14 321.37 8.2 2 -14 2 308.87 8.7 2 2 14 304.87 8.3 2 14 -2 299.07 8.6 0 14 -4 352.26 9.4 0 14 4 340.17 9.5 0 -14 -4 349.37 9.2 0 -14 4 345.87 9.1 4 -14 0 331.07 9.4 4 14 0 351.16 9.3 -4 -14 0 339.97 8.9 0 4 14 335.07 9 -4 0 14 350.16 8.7 -4 14 0 329.87 9.7 -2 4 14 1132.89 25.1 2 14 4 1102.99 25.4 14 -4 -2 1129.09 25.6 4 14 -2 1090.09 25.1 2 -14 -4 1125.89 25.3 -4 -2 14 1091.89 24.5 4 -14 2 1114.39 25.4 -2 14 -4 1071.29 25.4 -2 -14 4 1115.49 24.9 -4 14 2 1094.59 25.6 -4 -14 -2 1094.69 25.1 -4 -14 2 1114.09 24.9 -2 -4 14 1061.89 24.5 2 14 -4 1128.09 25.2 2 4 14 1099.29 25.1 4 -14 -2 1100.89 25.4 -4 2 14 1101.59 24.9 -2 -14 -4 1105.49 25.2 -4 14 -2 1103.59 25.5 -2 14 4 1097.99 25.5 4 14 2 1115.69 25.3 14 -2 -4 1113.69 25.4 2 -14 4 1104.09 25.2 4 -14 4 2844.32 63.29 4 -4 -14 2915.51 62.99 4 4 14 2892.11 63.19 4 14 -4 2893.51 63.09 -4 4 14 2863.11 63.09 -4 14 -4 2923.91 63.49 -4 14 4 2817.52 63.49 -4 -14 4 2918.21 62.89 -4 -4 14 2904.01 62.49 -4 -14 -4 2852.71 63.19 4 -14 -4 2804.32 63.29 14 -4 -4 2874.01 63.49 4 14 4 2867.11 63.29 0 14 6 55.19 3.7 0 14 -6 45 3.4 14 -6 0 49.2 4.1 0 -14 6 46.4 3.3 14 0 -6 48.2 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5.5 14 0 -16 100.39 4.6 16 14 0 84.59 5.2 0 -16 -14 90.79 5.3 0 -14 16 88.89 5.1 16 -14 0 101.79 6.5 0 -16 14 85.19 5.1 14 -16 0 92.89 6.3 16 0 -14 91.99 4.9 0 14 16 100.99 5.9 14 16 0 83.39 5.1 0 16 14 88.79 5.9 2 -16 -14 142.09 6.5 14 -2 -16 148.99 6 -2 14 16 144.69 6.6 16 -14 -2 153.28 7.5 16 2 -14 151.28 5.5 14 -16 2 146.79 7.4 16 14 2 134.79 6.2 -2 -16 14 139.29 5.5 2 16 14 157.98 7.2 2 -14 16 149.29 6.6 14 16 -2 138.89 6.1 16 14 -2 134.19 6 16 -2 -14 139.59 6.1 14 16 2 119.39 6.1 -2 16 14 155.68 7.1 16 -14 2 148.29 7.4 2 -16 14 140.69 6.5 2 -14 -16 159.18 6.5 2 14 16 143.49 6.5 14 2 -16 143.09 5.7 -2 -14 16 146.49 5.4 14 -16 -2 136.59 6.8 16 -14 -4 1974.2 44.8 -4 14 16 1952.9 44.6 16 4 -14 1993.6 43.2 -14 16 4 2051.59 45.1 4 16 14 1976.3 44.5 14 -4 -16 2027.9 44 -4 -16 14 1862.01 43.1 16 14 4 1945.31 44.2 4 -16 -14 2009.5 44.3 4 -14 16 1969 44.5 14 -16 4 1976.9 44.9 14 16 -4 1943.11 43.9 16 -4 -14 1889.91 44.1 -4 16 14 2009.6 44.7 4 -16 14 1945.11 44.5 16 14 -4 1940.91 43.8 4 -14 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670.33 17.9 10 -14 16 123.39 7.8 10 -16 -14 137.49 7.1 16 14 10 145.49 7.1 14 -16 10 140.09 8.1 14 -10 -16 124.79 6.8 14 10 16 152.48 7 -10 14 16 128.19 7.5 -16 10 14 129.19 7.8 -14 16 10 142.29 7.9 10 16 14 120.29 6.5 16 -14 -10 130.29 7.1 -10 16 14 132.49 7.7 10 -14 -16 134.59 6.9 -14 10 16 127.59 7.5 16 -14 10 143.39 8.3 14 -16 -10 147.09 7.5 14 16 10 134.29 6.8 16 -10 -14 106.19 6.6 -16 14 10 155.28 8.5 10 -16 14 115.39 7.6 10 14 16 141.69 7.2 12 16 14 203.28 8.4 14 -12 -16 186.08 8.2 14 12 16 231.38 9.1 14 -16 12 226.28 10.1 12 -16 -14 217.88 8.9 -12 14 16 228.98 9.9 -16 12 14 221.48 9.7 12 -14 16 212.08 9.7 16 14 12 225.88 8.8 -14 16 12 241.58 9.9 16 -14 -12 214.58 9 12 14 16 195.78 8 -14 12 16 204.28 9.4 -12 16 14 236.88 9.8 14 -16 -12 213.78 9 12 -16 14 198.98 9.5 14 16 12 228.48 9.2 16 -12 -14 197.98 8.7 16 12 14 216.78 8.6 -16 14 12 245.68 10.1 16 -14 12 218.48 9.8 12 -14 -16 199.28 8.2 -16 14 14 417.16 14.9 -14 14 16 392.26 14.8 -14 16 14 429.36 14.8 14 -16 -14 403.46 13.5 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19 378.46 13.8 19 -21 -3 357.06 14.9 3 19 21 343.17 14.9 21 -19 3 315.77 12.8 21 19 -3 352.26 14.9 19 21 3 373.76 15.2 19 -21 5 59.79 8.5 21 19 5 57.19 7.8 19 -5 -21 59.99 8 5 21 19 60.89 8.2 21 -19 -5 63.79 8.5 19 21 -5 64.29 8.6 5 -21 -19 57.69 7.4 -5 19 21 60.39 8.6 19 21 5 54.89 8.4 -5 21 19 47.3 7.9 5 19 21 59.59 8.1 5 -19 -21 63.29 7.4 21 -19 5 69.49 9 19 -21 -5 68.29 8.4 21 19 -5 61.19 8.3 21 -5 -19 66.79 7.9 19 -21 7 5.6 8.5 21 19 7 8.3 8 7 -19 21 7 9.5 21 -19 -7 9.3 8.1 19 -7 -21 8.7 7.8 7 -21 -19 13.5 7 7 21 19 6 7.8 -7 19 21 11.7 8.4 19 21 -7 4.5 8.5 21 -19 7 8 8 21 19 -7 5.1 7.9 7 19 21 12.6 7.5 21 -7 -19 5.7 7.8 7 -19 -21 5.8 7 19 21 7 8.5 7.8 19 -21 -7 1.3 7.6 7 -21 19 14 9.4 -7 21 19 6.8 8.1 9 -21 -19 335.77 12.1 21 19 9 296.87 12.2 19 21 -9 303.07 11.9 19 -21 9 314.47 13.5 9 21 19 290.77 12.1 21 -19 -9 330.57 13 -9 19 21 315.27 13.6 19 9 21 317.37 11.7 9 -19 21 319.27 14.2 19 -9 -21 305.87 12.5 9 19 21 312.27 12.1 9 -19 -21 321.07 12 9 -21 19 320.07 14.1 21 -19 9 262.47 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12.3 22 16 0 298.77 13 16 -22 2 103.79 8.1 -2 16 22 115.49 8.5 2 -22 -16 117.79 7.4 22 16 2 119.59 8.2 22 -16 -2 91.09 8.1 16 22 -2 103.99 8.4 16 -2 -22 118.49 7.3 2 22 16 104.19 8.2 22 2 -16 106.89 7.1 2 16 22 95.59 7.6 -2 22 16 105.19 8.4 22 -16 2 109.09 8.8 22 -2 -16 105.09 7.9 22 16 -2 109.39 7.8 2 -22 16 113.69 8.4 16 22 2 103.09 8.2 16 -22 -2 120.39 8.3 16 -22 4 31.9 7.3 4 -22 -16 35.8 6.5 22 4 -16 37.8 5.7 -4 16 22 42.9 7.7 16 22 -4 37.9 7.8 22 16 4 37.3 7.1 4 22 16 27.3 7.2 -4 -22 16 42.2 5.7 22 -16 -4 44 7.6 4 -16 22 36.8 8.5 16 -4 -22 46 6.7 16 -22 -4 45.1 7.3 4 -22 16 41.6 7.9 -4 22 16 40.9 7.2 22 16 -4 43.2 7 22 -4 -16 42.1 7.4 16 22 4 39.2 7.4 4 16 22 32.7 7.1 -16 4 22 37.5 8.6 22 -16 4 41.1 8 22 -16 -6 597.64 18.7 22 16 6 615.24 18.1 6 -22 -16 589.84 17.5 16 22 -6 603.24 18.7 16 -22 6 598.34 18.9 6 -16 22 590.64 19.7 -6 16 22 603.64 19.1 6 22 16 597.24 18.5 16 -6 -22 612.84 17.8 6 -22 16 583.44 19.1 6 -16 -22 594.84 17.6 22 -6 -16 578.04 18.4 22 16 -6 605.54 17.6 -6 22 16 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6 135.39 9.4 22 -6 -18 141.99 9.4 6 18 22 152.68 9.5 6 -22 18 139.99 10.6 18 -22 -6 159.38 9.6 8 22 18 3.9 7.8 18 -8 -22 4.3 8.1 22 18 8 3 7.6 22 -18 -8 4.7 8.1 -8 18 22 -1 8.6 18 -22 8 5.5 8.7 8 -22 -18 2.5 7 18 22 -8 1.7 8.8 8 -18 22 2.8 10.2 -8 22 18 3.2 8.2 8 -22 18 9.2 9.6 8 18 22 2.2 7.7 -18 8 22 4.1 10 8 -18 -22 2.1 7.3 22 18 -8 -0.2 7.7 22 -18 8 0.6 8.4 18 22 8 2.6 8.1 18 -22 -8 3.9 7.5 22 -8 -18 -3.6 7.9 -10 18 22 396.06 15.2 18 10 22 383.76 15.5 10 22 18 387.46 16.5 -18 22 10 403.66 17.6 10 -22 -18 394.96 15.5 18 -22 10 390.96 15.4 10 -18 22 417.76 16.5 22 18 10 392.96 16.2 18 -10 -22 394.56 16.6 22 -18 -10 417.76 16.8 10 18 22 376.96 16.1 10 -18 -22 411.96 16.1 22 -18 10 395.06 15.1 -18 10 22 439.46 16.6 18 22 10 377.56 16.7 -10 22 18 402.36 15 10 -22 18 406.86 15.5 22 -10 -18 388.56 16.8 18 -22 -10 408.26 16.2 -12 18 22 382.06 15.3 -18 22 12 340.37 14.2 18 -22 12 422.76 16.1 18 12 22 378.86 16.5 12 -22 -18 408.96 16.4 12 -18 22 418.56 17.1 22 18 12 391.06 16.8 12 22 18 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23 -15 -21 88.29 13.4 21 -23 -15 66.89 11.4 15 -23 21 89.79 16.4 23 -21 15 77.89 14.2 15 21 23 85.19 11.7 23 15 21 92.89 12.3 21 -23 17 58.19 16.1 23 -21 -17 42.6 13.2 23 -17 21 40.6 15.9 17 23 21 50.69 12.4 21 17 23 42.5 10.9 17 -21 23 47.4 17.4 -17 21 23 46.8 16.1 17 -23 -21 39.4 12.9 21 -17 -23 47.5 14.2 23 21 17 40.4 12.5 21 -23 -17 41.2 12 23 -17 -21 54.99 14.4 23 17 21 34.8 12.2 17 -21 -23 41.8 13.6 23 -21 17 29.1 15.9 -17 23 21 54.69 15.5 21 23 17 46.4 13.6 17 21 23 46.6 12.7 21 -17 23 53.79 17.4 17 -23 21 32.6 16.9 23 -19 21 404.96 20.9 21 -23 19 366.76 21.1 -19 21 23 388.76 21.8 19 -21 23 374.36 22.4 23 -21 -19 455.15 19.9 19 -23 -21 371.46 17.5 21 -19 -23 385.96 19 -19 23 21 362.36 21.2 19 -21 -23 394.26 18.5 19 -23 21 371.36 21.7 23 -19 -21 443.26 20.1 21 -19 23 368.36 21.7 21 -23 -19 396.36 18.6 23 -21 19 361.06 20.5 21 -23 -21 878.11 33.5 21 -23 21 856.21 38.1 21 -21 -23 926.51 33.5 21 -21 23 900.41 39.2 23 -21 -21 882.31 33.8 23 -21 21 887.31 37.3 -1 23 23 1013.9 30 1 23 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