Crystallography Open Database

Information card for entry 4512160

Preview

Coordinates	4512160.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H120 K4 Na16 O148 Tb4 W20
Calculated formula	C8 K4 Na16 O148 Tb4 W20
Title of publication	Rectangle versus Square Oxalate-Connective Tetralanthanide Cluster Anchored in Lacunary Lindqvist Isopolytungstates: Syntheses, Structures, and Properties
Authors of publication	Zhao, Junwei; Li, Hailou; Li, Yanzhou; Li, Chunyang; Wang, Zhenling; Chen, Lijuan
Journal of publication	Crystal Growth & Design
Year of publication	2014
Journal volume	14
Journal issue	11
Pages of publication	5495
a	10.015 ± 0.007 Å
b	19.598 ± 0.013 Å
c	19.64 ± 0.014 Å
α	106.185 ± 0.01°
β	92.996 ± 0.011°
γ	95.207 ± 0.011°
Cell volume	3675 ± 4 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0891
Residual factor for significantly intense reflections	0.0612
Weighted residual factors for significantly intense reflections	0.1482
Weighted residual factors for all reflections included in the refinement	0.1615
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179668 (current)	2016-03-24	cif/4/51/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/51/21.	4512160.cif
126821	2014-11-11	cif/ Updating files of 4512153, 4512154, 4512155, 4512156, 4512157, 4512158, 4512159, 4512160 Original log message: Adding full bibliography for 4512153--4512160.cif.	4512160.cif
125501	2014-10-17	cif/ Adding structures of 4512153, 4512154, 4512155, 4512156, 4512157, 4512158, 4512159, 4512160 via cif-deposit CGI script.	4512160.cif