Crystallography Open Database

Information card for entry 4512298

Preview

Coordinates	4512298.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H106 Fe4 Lu2 N2 O116 Sb2 W18
Calculated formula	C8 H18 Fe4 Lu2 N2 O116 Sb2 W18
Title of publication	First Tungstoantimonate-Based Transition-Metal‒Lanthanide Heterometallic Hybrids Functionalized by Amino Acid Ligands
Authors of publication	Zhao, Jun-Wei; Cao, Jing; Li, Yan-Zhou; Zhang, Jing; Chen, Li-Juan
Journal of publication	Crystal Growth & Design
Year of publication	2014
Journal volume	14
Journal issue	12
Pages of publication	6217
a	12.5684 ± 0.0007 Å
b	13.4822 ± 0.0007 Å
c	16.0879 ± 0.0008 Å
α	106.5 ± 0.001°
β	99.82 ± 0.001°
γ	97.278 ± 0.001°
Cell volume	2530.9 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0697
Residual factor for significantly intense reflections	0.0658
Weighted residual factors for significantly intense reflections	0.1878
Weighted residual factors for all reflections included in the refinement	0.1918
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179669 (current)	2016-03-24	cif/4/51/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/51/22.	4512298.cif
131336	2015-02-07	cif/ Updating files of 4512292, 4512293, 4512294, 4512295, 4512296, 4512297, 4512298 Original log message: Adding full bibliography for 4512292--4512298.cif.	4512298.cif
127345	2014-11-16	cif/ Adding structures of 4512292, 4512293, 4512294, 4512295, 4512296, 4512297, 4512298 via cif-deposit CGI script.	4512298.cif