Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4513275
Preview
| Coordinates | 4513275.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | 1666 bm AgClO4-eggcrate squeezed |
|---|---|
| Chemical name | Silver perchlorate / 4-[di(pyrazol-1-yl)methyl]pyridine / hexamethylene- teramine 3:3:1 coordination polymer, 2-dimensional, with unknown solvent squeezed and not contained in chemical formula and quantities derived thereof. |
| Formula | C42 H45 Ag3 Cl3 N19 O12 |
| Calculated formula | C42 H45 Ag3 Cl3 N19 O12 |
| Title of publication | Robust 2D Coordination Networks from a Two-Step Assembly Process with Predesigned Silver Cyclic Dimers and Hexamethylenetetramine |
| Authors of publication | Durá, Gema; Carrión, M. Carmen; Jalón, Félix A.; Manzano, Blanca R.; Rodríguez, Ana M.; Mereiter, Kurt |
| Journal of publication | Crystal Growth & Design |
| Year of publication | 2015 |
| Journal volume | 15 |
| Journal issue | 7 |
| Pages of publication | 3321 |
| a | 22.5686 ± 0.0005 Å |
| b | 22.5686 ± 0.0005 Å |
| c | 22.2724 ± 0.0005 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 9824.4 ± 0.4 Å3 |
| Cell temperature | 297 ± 2 K |
| Ambient diffraction temperature | 297 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 166 |
| Hermann-Mauguin space group symbol | R -3 m :H |
| Hall space group symbol | -R 3 2" |
| Residual factor for all reflections | 0.0843 |
| Residual factor for significantly intense reflections | 0.064 |
| Weighted residual factors for significantly intense reflections | 0.2089 |
| Weighted residual factors for all reflections included in the refinement | 0.2277 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.124 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176428 (current) | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
4513275.cif |
| 140076 | 2015-07-05 | cif/ Updating files of 4513274, 4513275, 4513276 Original log message: Adding full bibliography for 4513274--4513276.cif. |
4513275.cif |
| 139513 | 2015-06-24 | cif/ Adding structures of 4513274, 4513275, 4513276 via cif-deposit CGI script. |
4513275.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.