Crystallography Open Database

Information card for entry 4513663

Preview

Coordinates	4513663.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H42 Ag N2
Calculated formula	C32 H42 Ag N2
Title of publication	Abnormal Mesoionic Carbene Silver Complex: Synthesis, Reactivity, and Mechanistic Insight on Oxidative Fluorination
Authors of publication	Liu, Qilun; Yuan, Zheliang; Wang, Hao-yang; Li, Yang; Wu, Yichen; Xu, Tao; Leng, Xuebing; Chen, Pinhong; Guo, Yin-long; Lin, Zhenyang; Liu, Guosheng
Journal of publication	ACS Catalysis
Year of publication	2015
Journal volume	5
Journal issue	11
Pages of publication	6732
a	16.043 ± 0.002 Å
b	6.7774 ± 0.001 Å
c	27.121 ± 0.004 Å
α	90°
β	94.443 ± 0.003°
γ	90°
Cell volume	2940 ± 0.7 Å³
Cell temperature	140 ± 2 K
Ambient diffraction temperature	140 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0847
Residual factor for significantly intense reflections	0.0536
Weighted residual factors for significantly intense reflections	0.1523
Weighted residual factors for all reflections included in the refinement	0.1716
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
170774 (current)	2015-12-06	cif/ Updating files of 4513663, 4513664 Original log message: Adding full bibliography for 4513663--4513664.cif.	4513663.cif
167815	2015-10-14	cif/ Adding structures of 4513663 via cif-deposit CGI script.	4513663.cif