Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4514630
Preview
| Coordinates | 4514630.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29 H33 F6 N3 O11 S2 U |
|---|---|
| Calculated formula | C29 H33 F6 N3 O11 S2 U |
| Title of publication | Breaking C‒O Bonds with Uranium: Uranyl Complexes as Selective Catalysts in the Hydrosilylation of Aldehydes |
| Authors of publication | Monsigny, Louis; Thuéry, Pierre; Berthet, Jean-Claude; Cantat, Thibault |
| Journal of publication | ACS Catalysis |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 10 |
| Pages of publication | 9025 |
| a | 9.2981 ± 0.0004 Å |
| b | 22.059 ± 0.0017 Å |
| c | 18.3163 ± 0.0012 Å |
| α | 90° |
| β | 102.709 ± 0.004° |
| γ | 90° |
| Cell volume | 3664.8 ± 0.4 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0576 |
| Residual factor for significantly intense reflections | 0.0367 |
| Weighted residual factors for significantly intense reflections | 0.082 |
| Weighted residual factors for all reflections included in the refinement | 0.0882 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 219813 (current) | 2019-10-28 | cif/ Adding structures of 4514628, 4514629, 4514630 via cif-deposit CGI script. |
4514630.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.