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Information card for entry 4515592
Preview
| Coordinates | 4515592.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C31 H48 Co N2 O Si |
|---|---|
| Calculated formula | C31 H48 Co N2 O Si |
| Title of publication | Well-Defined β-Diketiminatocobalt(II) Complexes for Alkene Cyclohydroamination of Primary Amines |
| Authors of publication | Lepori, Clément; Gómez-Orellana, Pablo; Ouharzoune, Allissa; Guillot, Régis; Lledós, Agusti; Ujaque, Gregori; Hannedouche, Jérôme |
| Journal of publication | ACS Catalysis |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 5 |
| Pages of publication | 4446 |
| a | 17.0369 ± 0.0005 Å |
| b | 10.7343 ± 0.0003 Å |
| c | 17.0418 ± 0.0006 Å |
| α | 90° |
| β | 93.483 ± 0.001° |
| γ | 90° |
| Cell volume | 3110.83 ± 0.17 Å3 |
| Cell temperature | 100 ± 1 K |
| Ambient diffraction temperature | 100 ± 1 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0583 |
| Residual factor for significantly intense reflections | 0.04 |
| Weighted residual factors for significantly intense reflections | 0.0954 |
| Weighted residual factors for all reflections included in the refinement | 0.1053 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 225741 (current) | 2019-11-10 | cif/ Adding structures of 4515592 via cif-deposit CGI script. |
4515592.cif |
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Users of the data should acknowledge the original authors of the
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