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Information card for entry 4515714
Preview
| Coordinates | 4515714.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H14 Al F16 N4 |
|---|---|
| Calculated formula | C27 H14 Al F16 N4 |
| Title of publication | Switchable C‒H Silylation of Indoles Catalyzed by a Thermally Induced Frustrated Lewis Pair |
| Authors of publication | Han, Yuxi; Zhang, Sutao; He, Jianghua; Zhang, Yuetao |
| Journal of publication | ACS Catalysis |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 9 |
| Pages of publication | 8765 |
| a | 10.4075 ± 0.001 Å |
| b | 10.6369 ± 0.001 Å |
| c | 13.0972 ± 0.0012 Å |
| α | 79.781 ± 0.002° |
| β | 79.01 ± 0.002° |
| γ | 71.612 ± 0.002° |
| Cell volume | 1339.9 ± 0.2 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0493 |
| Residual factor for significantly intense reflections | 0.0419 |
| Weighted residual factors for significantly intense reflections | 0.1297 |
| Weighted residual factors for all reflections included in the refinement | 0.1398 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 225846 (current) | 2019-11-10 | cif/ Adding structures of 4515714 via cif-deposit CGI script. |
4515714.cif |
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Users of the data should acknowledge the original authors of the
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