#------------------------------------------------------------------------------ #$Date: 2019-12-20 23:47:07 +0200 (Fri, 20 Dec 2019) $ #$Revision: 245443 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/72/4517235.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4517235 _cell_angle_alpha 90.000 _cell_angle_beta 93.393 _cell_angle_gamma 90.000 _cell_length_a 15.0217 _cell_length_b 13.5252 _cell_length_c 14.4528 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.7684 _cod_data_source_file phangse_b_jw1933.fcf _cod_data_source_block jw1933 _shelx_title ' jw1933_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 399.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 574.91 532.47 9.88 o 2 0 0 46167.98 45446.30 675.34 o 3 0 0 3.07 23.37 5.93 o 4 0 0 1062.74 1169.33 37.05 o 5 0 0 373.32 325.95 13.40 o 6 0 0 33716.80 34149.90 548.51 o 7 0 0 10084.64 10927.03 143.59 o 8 0 0 18666.94 18044.57 213.58 o 9 0 0 8274.74 8262.52 104.45 o 10 0 0 5561.43 5550.08 85.65 o 11 0 0 543.37 566.38 26.14 o 12 0 0 7559.87 7269.58 124.71 o 13 0 0 5878.00 5821.47 108.03 o 14 0 0 289.84 321.41 38.92 o 15 0 0 394.50 456.38 50.46 o 16 0 0 2059.77 1995.01 73.31 o 17 0 0 675.01 829.01 45.51 o 18 0 0 71.20 23.81 28.89 o 19 0 0 144.78 93.26 70.60 o 1 1 0 28.83 19.86 1.77 o 2 1 0 67334.97 64867.70 799.56 o 3 1 0 1457.86 1579.22 21.82 o 4 1 0 26868.92 27486.04 311.93 o 5 1 0 1598.48 1635.82 22.07 o 6 1 0 2526.44 2257.50 29.74 o 7 1 0 911.29 1147.61 19.12 o 8 1 0 2076.01 2113.01 26.02 o 9 1 0 10.18 -1.38 9.08 o 10 1 0 10902.47 11041.84 105.04 o 11 1 0 7.61 0.55 14.20 o 12 1 0 519.86 513.57 21.37 o 13 1 0 7.91 -5.20 16.59 o 14 1 0 600.25 589.31 28.88 o 15 1 0 29.83 41.05 39.24 o 16 1 0 719.83 763.41 33.34 o 17 1 0 289.92 269.39 30.43 o 18 1 0 283.48 288.39 36.06 o 19 1 0 61.18 26.73 43.30 o 0 2 0 44515.72 43897.02 571.34 o 1 2 0 301.59 275.49 6.12 o 2 2 0 4683.17 4670.51 54.59 o 3 2 0 141.93 120.13 9.24 o 4 2 0 4219.84 4772.19 59.47 o 5 2 0 376.82 431.12 11.43 o 6 2 0 2748.58 3052.71 39.81 o 7 2 0 27.04 44.08 7.99 o 8 2 0 375.07 347.51 13.89 o 9 2 0 827.51 919.98 20.05 o 10 2 0 469.64 500.33 17.72 o 11 2 0 1211.66 1231.03 26.35 o 12 2 0 5764.79 5727.36 70.78 o 13 2 0 593.04 579.46 25.93 o 14 2 0 13.76 17.98 21.65 o 15 2 0 31.78 -2.71 21.39 o 16 2 0 75.84 112.32 20.85 o 17 2 0 652.90 724.51 41.59 o 18 2 0 625.29 660.66 41.15 o 19 2 0 172.64 113.86 47.75 o 1 3 0 423.08 484.45 9.79 o 2 3 0 3202.81 3901.76 50.93 o 3 3 0 7523.97 7934.89 96.48 o 4 3 0 6879.88 6384.12 82.36 o 5 3 0 1968.69 1883.58 29.22 o 6 3 0 18459.04 19120.35 190.96 o 7 3 0 1816.57 1749.36 26.40 o 8 3 0 2036.67 2145.90 29.61 o 9 3 0 201.26 207.40 11.38 o 10 3 0 157.70 166.32 13.90 o 11 3 0 2587.41 2501.78 35.10 o 12 3 0 724.88 720.86 26.42 o 13 3 0 3139.56 3175.99 55.34 o 14 3 0 1484.72 1484.52 34.04 o 15 3 0 280.00 328.15 25.40 o 16 3 0 398.54 431.93 38.09 o 17 3 0 1.95 28.17 27.65 o 18 3 0 35.38 79.02 28.32 o 19 3 0 277.35 334.64 32.60 o 0 4 0 159856.61 150881.77 3267.76 o 1 4 0 3581.37 3634.12 40.99 o 2 4 0 14515.04 15524.67 164.38 o 3 4 0 181.43 153.55 6.96 o 4 4 0 8079.49 8782.11 107.43 o 5 4 0 928.64 972.69 21.30 o 6 4 0 143.94 211.12 8.62 o 7 4 0 2489.13 2614.01 31.31 o 8 4 0 6051.42 6036.81 59.26 o 9 4 0 6328.43 6354.11 63.00 o 10 4 0 4765.62 4812.26 52.48 o 11 4 0 2395.13 2432.01 34.99 o 12 4 0 1600.65 1690.82 34.36 o 13 4 0 774.20 850.37 38.18 o 14 4 0 433.63 346.51 23.83 o 15 4 0 13.11 46.30 19.76 o 16 4 0 1479.60 1403.31 42.92 o 17 4 0 926.65 1130.33 73.06 o 18 4 0 552.40 538.87 37.57 o 1 5 0 4043.21 4362.37 47.39 o 2 5 0 3351.56 3150.18 35.76 o 3 5 0 147.47 136.69 7.21 o 4 5 0 14331.81 14108.86 162.94 o 5 5 0 398.12 392.58 10.55 o 6 5 0 5936.65 6231.15 63.79 o 7 5 0 395.66 377.42 13.51 o 8 5 0 1599.00 1600.04 25.22 o 9 5 0 3.03 -10.10 10.10 o 10 5 0 6571.60 6294.62 66.88 o 11 5 0 796.07 800.29 25.58 o 12 5 0 486.96 449.55 29.98 o 13 5 0 1587.42 1480.22 35.68 o 14 5 0 336.36 324.68 30.30 o 15 5 0 227.88 165.47 22.47 o 16 5 0 997.84 910.71 41.10 o 17 5 0 203.13 222.24 44.48 o 18 5 0 199.08 130.31 61.55 o 0 6 0 10047.58 8228.84 145.55 o 1 6 0 420.50 403.63 9.83 o 2 6 0 23124.11 23037.61 243.81 o 3 6 0 203.31 163.45 7.02 o 4 6 0 14788.65 16293.63 150.93 o 5 6 0 79.98 75.87 9.99 o 6 6 0 20129.85 20286.70 188.93 o 7 6 0 639.15 600.45 16.34 o 8 6 0 19335.79 18922.36 183.79 o 9 6 0 2192.22 2284.73 32.89 o 10 6 0 665.26 603.00 21.26 o 11 6 0 1118.67 1113.06 29.60 o 12 6 0 73.19 75.44 18.99 o 13 6 0 1769.81 1677.55 36.63 o 14 6 0 3377.84 3506.36 63.58 o 15 6 0 587.32 566.45 35.84 o 16 6 0 129.15 116.04 31.61 o 17 6 0 728.77 765.04 58.69 o 18 6 0 28.93 60.46 23.63 o 1 7 0 661.10 734.49 13.34 o 2 7 0 11028.47 10200.10 93.02 o 3 7 0 2681.40 2728.73 30.29 o 4 7 0 16310.33 15595.12 135.27 o 5 7 0 4545.05 4644.30 47.59 o 6 7 0 9007.60 9042.24 87.27 o 7 7 0 494.43 461.90 17.89 o 8 7 0 40.50 50.69 11.78 o 9 7 0 955.60 947.05 25.47 o 10 7 0 8144.82 8036.98 98.17 o 11 7 0 5549.06 5578.21 78.52 o 12 7 0 1209.77 1163.26 41.30 o 13 7 0 1424.58 1503.29 51.74 o 14 7 0 7.70 18.82 30.06 o 15 7 0 72.84 72.69 35.77 o 16 7 0 534.33 588.33 31.25 o 17 7 0 80.01 53.96 23.71 o 0 8 0 47.97 128.02 9.51 o 1 8 0 2362.63 2447.05 28.71 o 2 8 0 4826.05 4927.97 49.80 o 3 8 0 4.89 6.95 6.15 o 4 8 0 20.92 13.62 6.74 o 5 8 0 193.47 224.51 17.03 o 6 8 0 1859.93 1817.90 33.83 o 7 8 0 238.24 204.01 12.46 o 8 8 0 11093.81 11100.70 114.00 o 9 8 0 787.48 841.93 25.48 o 10 8 0 3.91 -15.32 19.63 o 11 8 0 633.14 628.03 26.27 o 12 8 0 136.82 121.35 18.11 o 13 8 0 1586.06 1570.88 42.15 o 14 8 0 643.56 623.47 28.45 o 15 8 0 17.33 10.70 26.43 o 16 8 0 1.45 -20.14 20.14 o 17 8 0 46.50 56.29 28.44 o 1 9 0 259.88 357.55 12.05 o 2 9 0 4546.05 4673.30 49.47 o 3 9 0 393.39 442.81 14.38 o 4 9 0 2830.91 2648.23 32.67 o 5 9 0 1265.81 1190.44 22.15 o 6 9 0 6829.32 6930.06 74.01 o 7 9 0 235.51 243.54 14.71 o 8 9 0 1485.66 1539.68 32.87 o 9 9 0 18.82 18.76 13.07 o 10 9 0 663.88 676.18 28.47 o 11 9 0 147.53 90.36 29.93 o 12 9 0 893.13 873.41 47.42 o 13 9 0 1456.44 1438.84 38.16 o 14 9 0 769.98 841.31 43.38 o 15 9 0 1779.10 1808.76 61.58 o 16 9 0 335.04 277.88 28.69 o 0 10 0 4330.80 4227.82 69.59 o 1 10 0 94.71 97.85 9.53 o 2 10 0 159.61 111.04 11.20 o 3 10 0 42.92 28.48 9.09 o 4 10 0 455.80 438.94 16.19 o 5 10 0 109.21 119.15 12.26 o 6 10 0 1354.28 1335.57 34.74 o 7 10 0 10.77 5.69 17.59 o 8 10 0 1238.06 1336.97 32.78 o 9 10 0 466.19 500.04 25.42 o 10 10 0 2713.57 2718.61 57.88 o 11 10 0 515.97 512.41 25.63 o 12 10 0 424.93 414.26 24.00 o 13 10 0 1.66 29.38 22.35 o 14 10 0 2.58 -0.11 30.03 o 15 10 0 946.62 954.16 33.52 o 16 10 0 312.24 317.90 28.04 o 1 11 0 1471.30 1454.28 27.84 o 2 11 0 195.42 202.00 14.68 o 3 11 0 354.41 382.11 15.27 o 4 11 0 2634.71 2841.83 45.50 o 5 11 0 441.84 443.29 22.98 o 6 11 0 47.89 52.67 14.01 o 7 11 0 218.89 205.64 17.17 o 8 11 0 2762.93 2684.76 45.88 o 9 11 0 260.53 200.05 29.33 o 10 11 0 205.18 180.41 19.41 o 11 11 0 338.01 332.43 21.54 o 12 11 0 484.74 418.07 49.55 o 13 11 0 0.63 3.47 17.72 o 14 11 0 496.30 467.25 33.78 o 15 11 0 514.09 582.71 29.49 o 0 12 0 13109.52 13083.13 221.61 o 1 12 0 390.77 390.01 15.67 o 2 12 0 8540.58 8429.69 97.68 o 3 12 0 192.35 183.94 15.46 o 4 12 0 298.60 316.30 17.23 o 5 12 0 0.02 6.46 11.99 o 6 12 0 3549.73 3418.53 51.98 o 7 12 0 359.23 379.28 23.27 o 8 12 0 2231.06 2303.35 45.47 o 9 12 0 410.15 380.97 22.39 o 10 12 0 53.02 53.92 18.43 o 11 12 0 13.43 -7.11 17.81 o 12 12 0 370.48 340.52 22.80 o 13 12 0 9.57 4.49 20.12 o 14 12 0 778.69 750.16 41.83 o 1 13 0 121.39 104.05 12.28 o 2 13 0 12279.24 12146.02 141.99 o 3 13 0 468.24 431.24 19.31 o 4 13 0 14656.40 14373.85 183.86 o 5 13 0 713.09 716.86 25.79 o 6 13 0 5309.91 5276.05 70.77 o 7 13 0 526.61 506.98 22.61 o 8 13 0 547.78 646.21 25.70 o 9 13 0 984.57 896.29 29.42 o 10 13 0 2972.80 2948.29 52.97 o 11 13 0 536.23 521.85 26.13 o 12 13 0 2881.93 2729.13 50.78 o 13 13 0 526.97 603.39 29.01 o 0 14 0 4438.43 4463.49 88.22 o 1 14 0 22.62 18.28 14.12 o 2 14 0 1985.89 1961.39 38.20 o 3 14 0 1.76 20.91 14.05 o 4 14 0 117.38 111.90 16.10 o 5 14 0 169.23 149.76 16.25 o 6 14 0 2435.59 2475.31 48.16 o 7 14 0 2.46 4.49 16.41 o 8 14 0 1338.83 1360.99 34.38 o 9 14 0 108.21 89.85 18.81 o 10 14 0 6.36 13.27 18.65 o 11 14 0 0.13 -11.13 20.92 o 1 15 0 797.03 787.10 26.43 o 2 15 0 415.42 371.68 20.35 o 3 15 0 378.45 335.91 27.75 o 4 15 0 115.37 108.09 17.18 o 5 15 0 439.50 474.31 30.48 o 6 15 0 158.18 185.80 17.65 o 7 15 0 108.10 131.84 19.89 o 8 15 0 461.73 360.35 25.64 o 9 15 0 34.56 -4.41 28.61 o 10 15 0 7.69 -6.00 20.90 o 0 16 0 336.26 361.42 35.11 o 1 16 0 230.63 215.70 20.56 o 2 16 0 1291.79 1248.02 40.88 o 3 16 0 93.81 91.09 17.49 o 4 16 0 97.78 109.75 22.89 o 5 16 0 90.04 63.65 29.44 o 6 16 0 72.39 46.16 24.00 o 7 16 0 294.92 298.89 38.80 o 8 16 0 1805.19 1765.64 72.31 o 1 17 0 2.63 3.87 24.13 o 2 17 0 128.26 150.95 25.27 o 3 17 0 0.24 -6.57 19.29 o 4 17 0 331.60 327.78 22.83 o 5 17 0 125.43 183.57 36.83 o -19 1 1 27.52 77.12 44.55 o -18 1 1 81.11 126.30 24.06 o -17 1 1 18.18 -1.18 23.11 o -16 1 1 1149.26 1206.01 38.99 o -15 1 1 538.16 515.96 42.17 o -14 1 1 1812.74 1773.34 48.89 o -13 1 1 2188.80 2178.15 45.37 o -12 1 1 343.50 347.55 17.56 o -11 1 1 188.36 197.25 13.87 o -10 1 1 94.95 73.45 11.67 o -9 1 1 7295.33 7276.25 64.09 o -8 1 1 1453.80 1362.27 18.89 o -7 1 1 32560.20 33906.97 281.37 o -6 1 1 114.73 170.36 8.29 o -5 1 1 5286.98 5094.20 56.29 o -4 1 1 326.08 374.06 13.47 o -3 1 1 446.38 448.41 12.03 o -2 1 1 0.22 1.82 2.75 o -1 1 1 154.20 94.79 3.07 o 0 1 1 17.14 12.77 2.00 o 1 1 1 81.48 171.83 6.08 o 2 1 1 361.02 320.56 7.62 o 3 1 1 9712.69 9723.62 111.98 o 4 1 1 6.95 8.37 6.00 o 5 1 1 459.08 510.55 12.01 o 6 1 1 289.51 312.97 11.81 o 7 1 1 7646.08 7846.93 72.98 o 8 1 1 2810.46 2772.41 29.66 o 9 1 1 6140.70 5985.48 58.95 o 10 1 1 4639.87 4419.85 51.02 o 11 1 1 1549.90 1456.04 29.91 o 12 1 1 1297.09 1247.04 28.13 o 13 1 1 245.19 239.28 19.35 o 14 1 1 571.59 523.63 28.93 o 15 1 1 269.20 230.32 37.54 o 16 1 1 1165.42 1132.69 37.45 o 17 1 1 208.97 135.79 39.60 o 18 1 1 267.88 223.60 34.15 o 19 1 1 4.33 -26.16 26.16 o -19 2 1 400.51 143.01 123.36 o -18 2 1 128.76 181.14 33.35 o -17 2 1 42.05 19.08 23.44 o -16 2 1 877.25 941.32 38.22 o -15 2 1 25.14 16.54 24.28 o -14 2 1 275.47 312.35 19.59 o -13 2 1 8033.71 7995.64 94.21 o -12 2 1 3292.69 3366.68 46.78 o -11 2 1 5519.48 5379.53 59.87 o -10 2 1 283.29 290.88 13.62 o -9 2 1 3807.91 3563.68 39.56 o -8 2 1 8077.35 9713.95 92.42 o -7 2 1 4481.03 4832.50 50.01 o -6 2 1 1451.19 1389.13 25.40 o -5 2 1 13035.06 13422.57 178.77 o -4 2 1 759.95 709.88 13.84 o -3 2 1 151829.95 142398.08 2827.49 o -2 2 1 335.24 363.18 11.77 o -1 2 1 5325.88 6228.61 63.98 o 0 2 1 43.05 26.73 3.26 o 1 2 1 14.70 6.28 3.54 o 2 2 1 318.01 259.90 9.62 o 3 2 1 69014.83 71850.63 810.25 o 4 2 1 7918.82 7916.44 92.21 o 5 2 1 37122.60 38158.52 433.13 o 6 2 1 4973.56 4823.68 59.49 o 7 2 1 3796.05 3405.35 36.51 o 8 2 1 143.52 295.32 14.62 o 9 2 1 122.14 124.13 9.70 o 10 2 1 1309.80 1424.85 26.12 o 11 2 1 435.79 412.09 17.59 o 12 2 1 11844.09 11825.82 123.38 o 13 2 1 3635.17 3731.56 53.85 o 14 2 1 2286.43 2392.49 47.50 o 15 2 1 0.76 9.59 21.77 o 16 2 1 1189.70 1259.58 36.93 o 17 2 1 131.92 133.49 23.03 o 18 2 1 42.34 79.85 20.97 o 19 2 1 69.42 157.28 68.42 o -19 3 1 11.50 -36.02 49.31 o -18 3 1 14.66 -17.19 73.18 o -17 3 1 0.08 -9.99 29.49 o -16 3 1 309.46 321.73 24.62 o -15 3 1 0.21 -20.49 20.49 o -14 3 1 629.71 608.92 26.63 o -13 3 1 69.90 51.17 18.26 o -12 3 1 845.64 771.18 26.16 o -11 3 1 680.78 722.20 22.24 o -10 3 1 24.65 5.19 11.37 o -9 3 1 942.51 988.50 24.41 o -8 3 1 746.99 752.41 18.36 o -7 3 1 6512.13 7288.83 72.67 o -6 3 1 1320.36 1529.01 22.11 o -5 3 1 1316.22 1395.33 22.43 o -4 3 1 64.59 46.69 4.86 o -3 3 1 23186.06 24635.29 306.60 o -2 3 1 845.33 901.02 15.15 o -1 3 1 17321.26 18498.90 187.70 o 0 3 1 2036.28 2075.72 27.03 o 1 3 1 12142.98 13744.06 166.91 o 2 3 1 335.56 330.57 18.45 o 3 3 1 95.71 124.24 6.14 o 4 3 1 847.04 959.71 16.87 o 5 3 1 15.99 27.36 6.12 o 6 3 1 38.20 43.81 6.57 o 7 3 1 3.93 18.18 7.59 o 8 3 1 591.95 633.03 16.85 o 9 3 1 259.25 242.11 12.15 o 10 3 1 22.23 28.80 10.73 o 11 3 1 11.88 18.10 17.39 o 12 3 1 89.73 87.96 15.22 o 13 3 1 34.15 20.29 14.49 o 14 3 1 226.58 183.95 24.16 o 15 3 1 0.68 69.38 40.44 o 16 3 1 70.80 35.84 22.35 o 17 3 1 1.47 38.43 53.12 o 18 3 1 167.84 182.47 48.38 o 19 3 1 3.05 -28.33 28.33 o -19 4 1 338.43 298.61 85.00 o -18 4 1 143.73 72.45 60.22 o -17 4 1 249.23 285.08 38.95 o -16 4 1 10.48 68.71 27.46 o -15 4 1 91.22 137.32 20.97 o -14 4 1 1713.83 1631.61 37.53 o -13 4 1 89.81 117.33 18.20 o -12 4 1 631.77 651.26 24.44 o -11 4 1 6270.01 6118.06 66.29 o -10 4 1 429.42 433.22 17.78 o -9 4 1 726.55 627.20 20.13 o -8 4 1 828.04 978.78 23.27 o -7 4 1 2037.60 2333.39 30.16 o -6 4 1 168.29 136.52 9.98 o -5 4 1 3477.54 2761.20 32.40 o -4 4 1 9.43 9.56 5.49 o -3 4 1 17272.97 17624.26 193.43 o -2 4 1 11.06 18.65 4.41 o -1 4 1 102374.24 107588.81 1212.96 o 0 4 1 66.94 87.91 4.83 o 1 4 1 68939.38 73253.19 863.82 o 2 4 1 2189.81 2189.17 30.13 o 3 4 1 7883.34 7740.29 99.53 o 4 4 1 124.92 100.66 7.11 o 5 4 1 8848.74 8226.21 104.35 o 6 4 1 5333.92 5217.16 54.77 o 7 4 1 1674.52 1613.00 23.27 o 8 4 1 759.66 675.44 15.69 o 9 4 1 1621.86 1692.00 25.84 o 10 4 1 6.99 21.78 15.18 o 11 4 1 1448.15 1462.94 29.79 o 12 4 1 283.55 323.15 21.20 o 13 4 1 10.91 17.21 15.99 o 14 4 1 1450.40 1383.83 34.57 o 15 4 1 1342.62 1336.62 37.69 o 16 4 1 436.27 462.21 31.43 o 17 4 1 3.66 49.31 34.81 o 18 4 1 0.22 -17.61 33.07 o -18 5 1 290.93 353.62 50.85 o -17 5 1 146.42 153.16 28.15 o -16 5 1 997.99 1103.44 42.17 o -15 5 1 855.56 842.92 33.51 o -14 5 1 600.16 550.22 33.16 o -13 5 1 4208.58 4033.79 61.32 o -12 5 1 0.49 -2.63 26.20 o -11 5 1 897.13 835.92 26.73 o -10 5 1 20.88 11.77 11.73 o -9 5 1 6386.93 6230.97 65.16 o -8 5 1 1549.85 1441.89 22.76 o -7 5 1 5354.49 4703.55 54.45 o -6 5 1 1627.51 1617.84 24.27 o -5 5 1 4121.92 3671.54 41.21 o -4 5 1 406.01 488.50 12.22 o -3 5 1 2526.21 2513.64 29.42 o -2 5 1 36.34 65.63 5.29 o -1 5 1 24497.87 25856.21 282.82 o 0 5 1 533.83 540.36 11.29 o 1 5 1 43524.71 44476.15 450.46 o 2 5 1 943.66 910.46 15.50 o 3 5 1 3864.31 3480.80 45.97 o 4 5 1 23.51 11.34 5.92 o 5 5 1 2579.37 2747.29 32.02 o 6 5 1 3683.70 4118.63 44.27 o 7 5 1 6977.38 6965.02 62.13 o 8 5 1 1608.39 1490.53 23.24 o 9 5 1 6198.50 5980.68 60.62 o 10 5 1 5022.10 4782.71 54.74 o 11 5 1 1706.81 1732.78 33.68 o 12 5 1 1608.70 1579.10 39.13 o 13 5 1 436.97 440.09 21.25 o 14 5 1 110.03 133.92 20.59 o 15 5 1 144.26 150.54 20.77 o 16 5 1 1079.02 1061.25 54.15 o 17 5 1 459.21 515.06 35.21 o 18 5 1 35.04 55.58 70.99 o 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