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Information card for entry 4518091
Preview
| Coordinates | 4518091.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H34 Br2 O4 Si |
|---|---|
| Calculated formula | C21 H34 Br2 O4 Si |
| Title of publication | Direct Access to Monoprotected Homoallylic 1,2-Diols via Dual Chromium/Photoredox Catalysis |
| Authors of publication | Schäfers, Felix; Quach, Linda; Schwarz, J. Luca; Saladrigas, Mar; Daniliuc, Constantin G.; Glorius, Frank |
| Journal of publication | ACS Catalysis |
| Year of publication | 2020 |
| Pages of publication | 11841 - 11847 |
| a | 12.8335 ± 0.0002 Å |
| b | 14.5079 ± 0.0002 Å |
| c | 25.395 ± 0.0003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 4728.22 ± 0.11 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.0282 |
| Residual factor for significantly intense reflections | 0.0272 |
| Weighted residual factors for significantly intense reflections | 0.0669 |
| Weighted residual factors for all reflections included in the refinement | 0.0675 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.076 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 256806 (current) | 2020-09-29 | cif/ Adding structures of 4518091 via cif-deposit CGI script. |
4518091.cif |
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Users of the data should acknowledge the original authors of the
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