#------------------------------------------------------------------------------ #$Date: 2021-03-03 22:05:59 +0200 (Wed, 03 Mar 2021) $ #$Revision: 262403 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/85/4518518.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518518 loop_ _publ_author_name 'G\'omez, Paula' 'Georgakopoulos, Stamatis' 'M\'as-Montoya, Miriam' 'Cerd\'a, Jes\'us' 'P\'erez, Jos\'e' 'Ort\'i, Enrique' 'Arag\'o, Juan' 'Curiel, David' _publ_section_title ; Improving the Robustness of Organic Semiconductors through Hydrogen Bonding. ; _journal_issue 7 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 8620 _journal_page_last 8630 _journal_paper_doi 10.1021/acsami.0c18928 _journal_volume 13 _journal_year 2021 _chemical_formula_sum 'C26 H16 N2' _chemical_formula_weight 356.41 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 90 _cell_angle_beta 97.995(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 6.3982(3) _cell_length_b 7.4255(3) _cell_length_c 18.0900(8) _cell_measurement_reflns_used 8954 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 77.33 _cell_measurement_theta_min 4.38 _cell_volume 851.10(6) _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc.)' _computing_data_collection 'APEX3 2017.3 (Bruker AXS Inc.)' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc.)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.4167 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 QUEST' _diffrn_measurement_method '\w-scans and phi scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0702 _diffrn_reflns_av_unetI/netI 0.0252 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 22457 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 74.419 _diffrn_reflns_theta_min 4.937 _diffrn_source 'high brilliance microfocus sealed tube ' _exptl_absorpt_coefficient_mu 0.633 _exptl_absorpt_correction_T_max 0.754 _exptl_absorpt_correction_T_min 0.685 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS-2016/2 _exptl_crystal_colour brown _exptl_crystal_density_diffrn 1.391 _exptl_crystal_description lath _exptl_crystal_F_000 372 _exptl_crystal_size_max 0.140 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.232 _refine_diff_density_min -0.260 _refine_diff_density_rms 0.060 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.139 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 131 _refine_ls_number_reflns 1732 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.139 _refine_ls_R_factor_all 0.0604 _refine_ls_R_factor_gt 0.0493 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0665P)^2^+0.4741P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1283 _refine_ls_wR_factor_ref 0.1356 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1469 _reflns_number_total 1732 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file am0c18928_si_001.cif _cod_data_source_block pgp42_0msp_a _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 4518518 _shelx_shelxl_version_number 2018/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.917 _shelx_estimated_absorpt_t_max 0.981 _shelx_res_file ; TITL pgp42_0msp_a.res in P2(1)/n pgp42_0msp_a.res created by SHELXL-2018/1 at 10:24:48 on 11-Jul-2018 CELL 1.54178 6.3982 7.4255 18.0900 90.000 97.995 90.000 ZERR 2.000 0.0003 0.0003 0.0008 0.000 0.002 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N UNIT 52 32 4 omit -1 3 1 REM Old TITL pgp42_0msp in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.104, Rweak 0.005, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C13 N L.S. 10 ACTA BOND $H FMAP 2 PLAN 20 htab size 0.03 0.07 0.14 TEMP -173.150 WGHT 0.066500 0.474100 FVAR 0.76449 C1 1 0.829836 0.640652 0.607482 11.00000 0.01442 0.01941 = 0.02653 0.00136 0.00358 -0.00100 AFIX 43 H1 2 0.958095 0.679416 0.591731 11.00000 -1.20000 AFIX 0 C2 1 0.806676 0.654538 0.680723 11.00000 0.01522 0.01753 = 0.02564 -0.00137 -0.00065 -0.00098 AFIX 43 H2 2 0.916585 0.704425 0.715398 11.00000 -1.20000 AFIX 0 C2A 1 0.616713 0.593908 0.705286 11.00000 0.01781 0.01627 = 0.02203 0.00080 0.00206 0.00183 C2B 1 0.543275 0.590864 0.776946 11.00000 0.01884 0.01591 = 0.02556 0.00026 0.00160 0.00366 C3 1 0.630142 0.644668 0.848986 11.00000 0.02100 0.01987 = 0.02560 -0.00205 -0.00019 0.00227 AFIX 43 H3 2 0.766272 0.698050 0.857773 11.00000 -1.20000 AFIX 0 C4 1 0.513552 0.618434 0.907045 11.00000 0.02639 0.02463 = 0.02178 -0.00200 -0.00008 0.00485 AFIX 43 H4 2 0.571036 0.653837 0.956147 11.00000 -1.20000 AFIX 0 C5 1 0.310766 0.540016 0.894593 11.00000 0.02609 0.02465 = 0.02427 0.00254 0.00711 0.00403 AFIX 43 H5 2 0.234183 0.524057 0.935496 11.00000 -1.20000 AFIX 0 C6 1 0.221206 0.485922 0.824111 11.00000 0.02206 0.02044 = 0.02654 0.00170 0.00398 0.00244 AFIX 43 H6 2 0.084831 0.432903 0.815761 11.00000 -1.20000 AFIX 0 C6A 1 0.339729 0.512498 0.765600 11.00000 0.01931 0.01679 = 0.02448 -0.00012 0.00236 0.00220 N7 3 0.290178 0.470975 0.690830 11.00000 0.01529 0.02369 = 0.02216 -0.00119 0.00227 -0.00182 H0 2 0.179931 0.415209 0.670822 11.00000 0.03310 C7A 1 0.455680 0.520827 0.653812 11.00000 0.01566 0.01571 = 0.02511 0.00096 0.00284 0.00068 C7B 1 0.470196 0.508321 0.575947 11.00000 0.01469 0.01837 = 0.02146 0.00160 0.00325 0.00048 C8 1 0.310260 0.442738 0.522226 11.00000 0.01419 0.01863 = 0.02512 0.00209 0.00307 -0.00128 AFIX 43 H8 2 0.181035 0.404899 0.537503 11.00000 -1.20000 AFIX 0 C8A 1 0.334110 0.430999 0.446888 11.00000 0.01479 0.01655 = 0.02569 0.00159 0.00233 0.00037 HKLF 4 REM pgp42_0msp_a.res in P2(1)/n REM R1 = 0.0493 for 1469 Fo > 4sig(Fo) and 0.0604 for all 1732 data REM 131 parameters refined using 0 restraints END WGHT 0.0667 0.4735 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.232, deepest hole -0.260, 1-sigma level 0.060 Q1 1 0.2567 0.3841 0.4214 11.00000 0.05 0.23 Q2 1 0.7086 0.5612 0.9790 11.00000 0.05 0.22 Q3 1 0.4256 0.3867 0.5596 11.00000 0.05 0.22 Q4 1 0.7982 0.5212 0.5934 11.00000 0.05 0.21 Q5 1 0.4005 0.6224 0.7635 11.00000 0.05 0.18 Q6 1 0.3695 0.2620 0.5418 11.00000 0.05 0.17 Q7 1 0.3177 0.2802 0.4399 11.00000 0.05 0.17 Q8 1 0.4969 0.6117 0.6662 11.00000 0.05 0.17 Q9 1 0.3009 0.3033 0.6932 11.00000 0.05 0.16 Q10 1 0.3642 0.5432 0.5419 11.00000 0.05 0.16 Q11 1 0.4325 0.5359 0.8999 11.00000 0.05 0.16 Q12 1 0.5958 0.4799 0.9397 11.00000 0.05 0.16 Q13 1 0.2603 0.3142 0.6781 11.00000 0.05 0.16 Q14 1 0.2321 0.5787 0.8448 11.00000 0.05 0.16 Q15 1 0.3053 0.4561 0.8559 11.00000 0.05 0.15 Q16 1 0.6342 0.4283 0.8650 11.00000 0.05 0.15 Q17 1 0.3602 0.2833 0.7166 11.00000 0.05 0.15 Q18 1 0.3241 0.4776 0.9616 11.00000 0.05 0.15 Q19 1 0.4579 0.5184 0.6171 11.00000 0.05 0.15 Q20 1 0.6311 0.6285 0.8099 11.00000 0.05 0.15 ; _shelx_res_checksum 76446 _shelx_hkl_file ; 1 0 0 -0.60 1.00 1 0 0 2.00 0.80 -1 0 0 -0.40 1.00 -1 0 0 1.00 0.80 2 0 0 721.13 30.30 2 0 0 725.13 30.50 -2 0 0 715.23 30.80 2 0 0 761.62 30.50 -2 0 0 736.83 30.20 -2 0 0 727.03 30.30 -3 0 0 -0.20 2.70 3 0 0 -0.70 2.20 3 0 0 0.40 2.40 3 0 0 -0.90 2.30 -3 0 0 1.60 2.40 -3 0 0 0.20 2.60 4 0 0 23.40 5.10 4 0 0 28.40 5.10 4 0 0 19.40 4.10 4 0 0 25.00 5.40 -4 0 0 22.50 4.30 4 0 0 22.00 4.10 4 0 0 25.20 5.20 -4 0 0 21.70 3.70 -4 0 0 22.60 3.40 -4 0 0 26.00 5.30 -4 0 0 24.40 3.80 5 0 0 -5.20 5.50 5 0 0 -1.20 2.60 -5 0 0 5.10 2.70 -5 0 0 -1.40 4.00 -5 0 0 -2.70 2.70 5 0 0 -2.70 4.00 5 0 0 -1.50 2.40 5 0 0 -0.70 3.90 -5 0 0 1.70 2.80 -5 0 0 -6.40 8.20 6 0 0 421.16 19.20 6 0 0 432.36 20.00 -6 0 0 411.46 20.50 -6 0 0 328.37 33.10 -6 0 0 428.06 19.80 6 0 0 420.46 20.40 -6 0 0 416.66 19.20 6 0 0 399.96 18.00 -7 0 0 1.20 2.70 7 0 0 -1.90 3.00 -7 0 0 -1.00 3.00 7 0 0 -2.50 3.10 -7 0 0 -3.60 2.80 7 0 0 -2.30 2.30 0 -1 0 -0.70 0.50 0 1 0 -1.40 1.00 0 1 0 -0.30 0.60 0 1 0 1.20 1.00 1 -1 0 6354.56 270.97 1 -1 0 7006.20 271.77 -1 -1 0 7011.80 271.07 -1 -1 0 7001.20 272.17 -1 -1 0 6781.52 270.77 -1 1 0 6898.41 272.37 1 1 0 6497.15 269.27 1 1 0 6414.16 269.17 -1 1 0 6760.32 271.97 -2 -1 0 58.09 4.50 -2 -1 0 54.79 3.80 2 -1 0 57.59 4.10 -2 -1 0 57.69 4.00 2 -1 0 60.39 4.40 2 -1 0 52.99 3.90 -2 1 0 58.69 4.70 -2 1 0 58.49 4.60 2 1 0 57.19 4.60 -2 1 0 52.69 4.90 2 1 0 53.39 3.50 -3 -1 0 51.09 4.60 -3 -1 0 46.30 5.40 3 -1 0 45.60 4.80 -3 -1 0 47.90 4.10 3 -1 0 47.00 5.10 -3 -1 0 44.20 4.50 3 -1 0 48.10 5.20 3 -1 0 39.90 4.40 3 1 0 53.49 4.70 3 1 0 54.99 5.80 3 1 0 44.60 6.60 -3 1 0 44.00 8.40 -3 1 0 46.00 5.40 -4 -1 0 104.79 10.00 4 -1 0 92.99 6.80 -4 -1 0 97.09 6.90 -4 -1 0 100.29 7.80 4 -1 0 93.99 7.60 4 -1 0 95.69 11.90 -4 -1 0 88.29 6.20 -4 -1 0 103.59 8.40 4 -1 0 94.69 7.10 -4 -1 0 100.29 8.80 4 -1 0 82.39 6.60 4 -1 0 88.59 9.40 4 -1 0 83.89 6.90 -4 -1 0 95.59 6.40 -4 -1 0 97.89 7.30 4 1 0 91.79 6.60 4 1 0 94.59 7.00 -4 1 0 89.79 9.60 -4 1 0 83.29 6.90 -4 1 0 98.39 7.50 4 1 0 90.49 8.10 -4 1 0 96.19 7.70 -4 1 0 79.89 9.50 -4 1 0 103.19 9.60 4 1 0 77.69 8.40 5 -1 0 125.79 17.70 5 -1 0 124.59 8.60 5 -1 0 116.59 10.10 -5 -1 0 141.19 7.80 -5 -1 0 132.59 10.40 -5 -1 0 126.69 9.00 -5 -1 0 129.19 8.80 5 -1 0 137.99 9.20 -5 -1 0 139.49 9.10 5 -1 0 120.99 12.30 5 -1 0 136.39 12.00 5 -1 0 136.29 9.80 5 -1 0 143.59 8.00 5 1 0 150.38 9.90 5 1 0 132.99 8.90 -5 1 0 133.29 15.20 -5 1 0 138.19 9.30 -5 1 0 136.59 9.10 -5 1 0 144.49 10.20 -6 -1 0 25.90 5.00 6 -1 0 20.10 3.80 6 -1 0 20.50 3.10 6 -1 0 30.10 5.70 -6 -1 0 15.40 4.10 6 -1 0 18.80 4.40 -6 -1 0 18.20 3.50 -6 -1 0 14.90 3.20 6 1 0 20.60 3.70 -6 1 0 32.60 5.60 -6 1 0 23.00 12.60 6 1 0 24.50 5.50 6 1 0 20.20 3.70 7 -1 0 14.60 4.60 -7 -1 0 6.20 3.10 -7 -1 0 9.40 3.30 7 -1 0 7.40 2.90 -7 -1 0 9.30 2.70 7 -1 0 5.40 3.10 7 1 0 9.90 3.80 -7 1 0 8.70 2.40 7 1 0 13.10 3.00 7 1 0 12.00 2.70 0 -2 0 9717.53 384.66 0 2 0 9999.00 388.26 0 2 0 9375.66 388.06 0 2 0 9389.56 386.86 -1 -2 0 3744.13 154.28 1 -2 0 3900.91 153.88 -1 -2 0 3733.73 154.98 1 -2 0 3915.11 154.78 -1 -2 0 3758.02 154.78 -1 2 0 4008.00 155.28 -1 2 0 3890.31 155.08 -1 2 0 3942.01 154.78 -2 -2 0 208.08 10.30 2 -2 0 195.08 9.50 2 -2 0 196.68 9.30 -2 -2 0 208.58 9.40 -2 -2 0 211.38 9.40 -2 -2 0 193.58 9.50 2 -2 0 203.48 10.40 -2 2 0 192.48 10.50 -2 2 0 191.68 10.40 -2 2 0 193.78 10.10 -3 -2 0 84.49 5.90 -3 -2 0 76.99 6.20 3 -2 0 74.59 5.90 -3 -2 0 93.59 6.00 3 -2 0 80.79 5.70 -3 -2 0 76.39 6.70 3 -2 0 79.09 7.00 -3 2 0 72.29 6.30 -3 2 0 77.59 6.80 -3 2 0 85.59 7.10 4 -2 0 104.49 8.40 4 -2 0 114.09 7.60 4 -2 0 110.59 11.70 -4 -2 0 116.39 10.20 4 -2 0 104.19 8.00 -4 -2 0 103.69 8.50 -4 -2 0 107.69 7.20 4 -2 0 107.99 7.60 4 -2 0 111.29 8.10 -4 -2 0 104.99 7.50 -4 -2 0 113.89 10.30 -4 -2 0 146.49 18.00 -4 2 0 104.99 10.10 -4 2 0 111.99 9.30 -4 2 0 98.59 9.10 -4 2 0 118.69 9.90 4 2 0 81.29 9.40 -4 2 0 116.49 9.80 -4 2 0 89.79 7.80 -4 2 0 114.29 11.00 4 2 0 98.29 8.20 5 -2 0 62.19 6.70 5 -2 0 56.19 9.50 -5 -2 0 55.19 6.50 -5 -2 0 52.39 12.10 5 -2 0 56.79 6.70 5 -2 0 83.69 15.90 5 -2 0 59.09 5.50 5 -2 0 56.89 7.90 -5 -2 0 54.29 6.80 -5 -2 0 60.19 5.50 -5 -2 0 59.19 6.20 5 -2 0 56.99 7.60 -5 2 0 72.29 6.70 -5 2 0 61.59 9.40 5 2 0 63.49 6.90 -5 2 0 48.00 8.20 5 2 0 58.89 7.60 6 -2 0 65.39 7.70 -6 -2 0 49.30 7.10 -6 -2 0 56.19 4.80 6 -2 0 56.99 4.60 -6 -2 0 54.59 6.00 6 -2 0 62.09 6.10 -6 -2 0 58.09 9.00 6 -2 0 53.89 6.90 6 -2 0 62.89 11.50 -6 -2 0 62.39 5.90 6 2 0 56.99 5.90 -6 2 0 48.10 5.70 6 2 0 62.99 7.50 7 -2 0 67.69 4.20 -7 -2 0 46.40 7.80 -7 -2 0 61.29 6.10 7 -2 0 67.29 5.10 7 -2 0 64.99 6.00 -7 -2 0 65.19 5.10 -7 2 0 58.19 6.10 -7 2 0 70.99 5.10 7 2 0 58.59 5.00 -7 2 0 76.39 6.10 0 -3 0 1.00 1.70 0 -3 0 0.40 0.80 0 -3 0 -2.70 1.70 0 3 0 1.30 1.50 0 3 0 -1.90 1.90 0 3 0 0.00 2.10 -1 -3 0 524.85 22.60 1 -3 0 536.15 22.00 -1 -3 0 518.45 22.10 -1 -3 0 530.25 23.40 1 -3 0 564.24 23.40 -1 -3 0 499.35 22.00 -1 3 0 547.25 24.00 -1 3 0 532.75 23.30 -1 3 0 541.75 24.00 -2 -3 0 285.87 13.00 -2 -3 0 281.27 13.10 2 -3 0 276.97 13.20 2 -3 0 292.87 13.00 2 -3 0 288.47 14.40 -2 -3 0 274.77 14.20 -2 -3 0 271.47 12.80 -2 -3 0 264.37 13.60 -2 3 0 290.87 14.00 -2 3 0 282.37 14.50 -2 3 0 294.47 14.80 -3 -3 0 322.77 18.10 3 -3 0 286.77 13.80 -3 -3 0 277.67 15.40 -3 -3 0 286.77 15.20 3 -3 0 265.57 15.60 3 -3 0 283.97 13.50 3 -3 0 287.97 13.80 -3 -3 0 280.27 13.90 -3 -3 0 286.77 13.60 -3 -3 0 271.07 13.60 -3 3 0 276.47 14.80 -3 3 0 260.97 13.60 -3 3 0 268.97 15.50 -3 3 0 273.47 16.10 3 3 0 288.67 16.60 -3 3 0 264.17 14.50 -3 3 0 278.37 15.50 -3 3 0 270.07 14.50 -3 3 0 290.27 14.80 -4 -3 0 5.30 3.00 -4 -3 0 -1.80 3.40 -4 -3 0 -3.80 8.40 4 -3 0 1.00 3.40 4 -3 0 2.80 8.00 4 -3 0 2.30 3.30 4 -3 0 3.80 3.30 4 -3 0 11.00 3.80 -4 -3 0 3.50 2.70 -4 3 0 0.10 3.90 -4 3 0 1.70 3.90 4 3 0 0.50 5.70 -4 3 0 -10.20 7.00 -4 3 0 7.60 3.70 -4 3 0 3.30 6.30 -4 3 0 5.90 3.30 -5 -3 0 334.77 16.60 5 -3 0 343.47 19.00 -5 -3 0 328.37 15.80 -5 -3 0 283.37 23.70 5 -3 0 349.47 17.00 5 -3 0 341.87 16.00 -5 -3 0 327.57 17.60 -5 -3 0 338.47 16.70 -5 -3 0 342.87 19.80 5 -3 0 352.86 17.90 -5 -3 0 337.87 17.10 5 -3 0 358.56 17.80 5 -3 0 342.17 16.60 -5 3 0 383.36 22.70 -5 3 0 341.97 17.60 -5 3 0 313.27 17.40 -5 3 0 343.17 16.30 -5 3 0 313.97 24.10 6 -3 0 -3.00 3.40 6 -3 0 1.70 6.40 -6 -3 0 -4.70 2.60 6 -3 0 -1.20 2.90 -6 -3 0 1.80 3.40 -6 -3 0 3.20 3.90 -6 -3 0 1.60 2.80 6 -3 0 -2.20 13.00 6 -3 0 -1.90 3.70 -6 3 0 -2.30 4.20 -6 3 0 3.60 3.00 -6 3 0 -4.80 9.10 6 3 0 0.80 3.30 7 -3 0 20.40 3.50 -7 -3 0 17.00 3.60 7 -3 0 22.30 5.00 -7 -3 0 18.90 3.30 7 -3 0 16.10 2.60 7 3 0 23.10 3.50 -7 3 0 16.40 3.40 7 3 0 27.30 4.80 -7 3 0 22.20 3.90 -7 3 0 20.60 4.40 0 -4 0 5.80 2.80 0 -4 0 4.20 2.30 0 -4 0 3.10 1.40 0 -4 0 0.60 3.80 0 4 0 -1.40 2.80 0 4 0 1.20 2.10 0 4 0 0.80 2.60 -1 -4 0 63.19 6.00 -1 -4 0 54.69 4.30 -1 -4 0 49.30 5.40 1 -4 0 65.39 6.50 1 -4 0 67.39 5.50 1 -4 0 55.99 4.10 -1 4 0 63.59 6.10 -1 4 0 72.99 7.10 -1 4 0 46.80 8.90 -1 4 0 61.69 9.40 -1 4 0 75.99 7.10 -1 4 0 62.39 7.60 1 4 0 47.80 7.20 2 -4 0 83.39 5.40 -2 -4 0 84.69 7.10 -2 -4 0 71.19 5.40 -2 -4 0 79.39 7.40 2 -4 0 73.19 5.60 2 -4 0 86.39 8.30 -2 -4 0 57.69 5.30 -2 4 0 72.09 7.50 -2 4 0 60.69 13.20 2 4 0 63.99 8.10 -2 4 0 70.69 7.80 2 4 0 75.19 7.10 -2 4 0 76.19 6.60 -2 4 0 77.19 8.40 -2 4 0 75.89 8.50 -2 4 0 60.89 7.20 -2 4 0 75.79 7.00 2 4 0 64.69 6.90 2 4 0 66.49 7.40 -2 4 0 61.59 11.90 -2 4 0 58.49 10.60 -2 4 0 70.39 6.60 -2 4 0 74.39 7.10 -2 4 0 62.19 9.40 2 4 0 73.59 9.50 -3 -4 0 0.40 2.90 3 -4 0 0.50 3.60 -3 -4 0 4.20 4.40 -3 -4 0 1.40 4.80 3 -4 0 -1.40 9.00 3 -4 0 5.10 2.90 -3 -4 0 1.40 2.90 -3 -4 0 -5.50 5.60 -3 -4 0 3.40 2.60 3 -4 0 6.70 2.80 -3 4 0 -0.50 5.30 -3 4 0 1.50 3.40 -3 4 0 6.70 5.30 -3 4 0 1.90 4.90 -3 4 0 3.10 3.20 -3 4 0 -5.90 3.50 3 4 0 0.60 5.10 -3 4 0 2.60 3.80 -3 4 0 3.50 3.40 -3 4 0 -0.30 3.10 3 4 0 3.60 4.50 4 -4 0 143.09 12.30 -4 -4 0 148.79 11.10 -4 -4 0 158.88 10.00 -4 -4 0 170.08 9.40 4 -4 0 166.48 10.10 4 -4 0 142.79 10.40 -4 -4 0 150.08 9.60 -4 -4 0 157.38 10.10 4 -4 0 142.19 9.80 4 -4 0 140.59 11.10 4 -4 0 136.39 22.10 4 -4 0 152.28 9.90 -4 4 0 143.99 11.10 -4 4 0 127.69 14.40 -4 4 0 146.89 10.30 -4 4 0 144.79 10.40 -4 4 0 134.49 23.20 -4 4 0 168.88 10.10 -4 4 0 148.39 15.20 -4 4 0 154.18 9.90 4 4 0 175.28 11.50 -4 4 0 153.98 9.00 5 -4 0 0.50 3.30 -5 -4 0 1.30 3.20 -5 -4 0 2.90 4.50 5 -4 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3.60 -1 5 0 12.00 5.00 1 5 0 9.50 5.30 -1 5 0 9.60 3.40 1 5 0 18.00 5.20 -1 5 0 15.90 3.60 1 5 0 8.50 4.40 -1 5 0 9.80 3.90 -1 5 0 10.20 4.30 1 5 0 14.30 5.40 1 5 0 11.60 3.60 -1 5 0 18.50 6.60 -1 5 0 11.20 4.90 1 5 0 16.90 3.60 -1 5 0 9.30 4.20 1 5 0 -2.00 6.90 -1 5 0 9.60 6.10 -1 5 0 21.00 8.40 1 5 0 10.90 4.40 -1 5 0 15.30 5.20 1 5 0 9.90 5.60 -2 -5 0 12.10 4.50 2 -5 0 26.90 5.30 2 -5 0 18.80 3.40 2 -5 0 16.20 8.70 -2 -5 0 26.70 6.40 -2 -5 0 21.10 4.60 -2 -5 0 14.70 3.60 2 5 0 13.60 4.60 -2 5 0 33.40 6.70 -2 5 0 22.70 6.40 2 5 0 17.20 4.20 2 5 0 13.10 7.20 -2 5 0 25.00 7.60 -2 5 0 27.20 5.50 2 5 0 10.60 5.80 -2 5 0 20.70 4.40 -2 5 0 18.90 4.50 -2 5 0 19.50 5.00 -2 5 0 17.60 4.90 -2 5 0 10.20 4.30 -2 5 0 20.70 5.30 -3 -5 0 -2.30 5.20 3 -5 0 3.30 3.50 3 -5 0 -0.30 3.40 3 -5 0 28.90 13.00 -3 -5 0 0.90 3.50 3 -5 0 -0.80 4.40 -3 -5 0 5.40 4.40 -3 -5 0 0.60 3.30 -3 -5 0 -4.80 8.80 -3 -5 0 0.60 3.40 -3 5 0 -0.90 3.50 -3 5 0 8.80 5.50 -3 5 0 1.60 3.70 -3 5 0 -0.30 5.40 -3 5 0 2.10 5.60 -3 5 0 -4.80 3.50 -3 5 0 -6.80 8.00 -3 5 0 0.20 3.50 3 5 0 4.40 4.20 -3 5 0 -2.50 4.60 3 5 0 -2.70 5.10 3 5 0 10.20 5.40 -3 5 0 13.60 8.90 -3 5 0 -4.70 4.30 4 -5 0 205.08 12.20 -4 -5 0 223.08 12.50 4 -5 0 208.38 12.30 -4 -5 0 219.48 11.60 -4 -5 0 224.28 15.70 4 -5 0 223.78 16.00 -4 -5 0 219.98 12.40 4 -5 0 217.48 13.90 -4 -5 0 237.28 14.40 4 -5 0 202.68 14.00 -4 5 0 220.28 12.70 -4 5 0 205.98 11.90 -4 5 0 247.78 21.90 -4 5 0 190.38 15.00 -4 5 0 204.18 12.80 -4 5 0 208.18 12.20 4 5 0 204.48 11.10 4 5 0 218.08 12.90 -4 5 0 196.78 22.80 4 5 0 226.98 13.40 -4 5 0 194.28 12.60 5 -5 0 15.60 4.00 5 -5 0 17.80 5.00 -5 -5 0 10.10 3.50 5 -5 0 12.00 4.80 -5 -5 0 12.10 3.40 -5 -5 0 11.10 8.10 -5 -5 0 12.90 2.70 -5 -5 0 20.90 3.90 5 -5 0 19.30 7.60 -5 -5 0 9.70 5.40 5 5 0 14.60 4.10 5 5 0 13.20 2.60 -5 5 0 9.00 3.40 -5 5 0 12.70 3.30 -5 5 0 22.10 4.40 5 5 0 8.50 5.30 -5 5 0 17.40 3.80 6 -5 0 19.70 2.90 6 -5 0 25.50 7.30 6 -5 0 26.60 4.40 -6 -5 0 25.30 4.80 -6 -5 0 26.70 4.20 -6 -5 0 30.80 6.40 -6 -5 0 20.20 2.80 6 -5 0 28.60 3.70 -6 5 0 30.10 4.40 6 5 0 24.40 3.60 6 5 0 16.50 3.40 -6 5 0 22.90 3.90 0 -6 0 116.99 14.90 0 -6 0 155.38 15.20 0 -6 0 143.99 9.00 0 -6 0 147.59 9.00 0 6 0 144.69 10.10 0 6 0 144.09 9.90 0 6 0 137.29 10.10 0 6 0 146.09 9.50 0 6 0 159.88 10.30 0 6 0 169.28 11.00 1 -6 0 17.40 4.00 -1 -6 0 21.80 8.40 1 -6 0 13.10 3.90 1 -6 0 11.30 6.80 -1 -6 0 15.50 3.70 -1 6 0 17.00 4.40 1 6 0 18.20 4.40 1 6 0 30.90 8.90 -1 6 0 13.10 4.00 -1 6 0 11.90 4.40 -1 6 0 15.50 4.30 -1 6 0 12.70 7.70 -1 6 0 11.70 7.70 -1 6 0 15.40 5.90 -1 6 0 15.10 5.90 1 6 0 28.20 6.10 1 6 0 12.30 4.00 1 6 0 17.10 4.60 -1 6 0 18.00 5.10 -1 6 0 23.50 6.40 -1 6 0 15.30 4.80 -1 6 0 3.20 5.70 1 6 0 18.00 5.00 -1 6 0 26.30 5.70 1 6 0 2.60 7.60 2 -6 0 50.09 7.00 -2 -6 0 43.30 7.40 -2 -6 0 44.80 6.40 -2 -6 0 51.79 13.00 2 -6 0 46.30 7.10 -2 -6 0 37.90 5.90 2 -6 0 38.60 9.60 -2 6 0 50.39 8.30 -2 6 0 41.70 6.90 2 6 0 47.60 7.40 -2 6 0 35.10 5.50 -2 6 0 31.90 7.00 2 6 0 45.10 6.50 -2 6 0 40.00 11.10 -2 6 0 50.29 6.70 -2 6 0 45.00 6.70 -2 6 0 59.49 8.40 2 6 0 56.39 9.10 -2 6 0 37.10 5.90 -2 6 0 29.20 6.60 2 6 0 51.29 7.60 -3 -6 0 132.29 9.60 3 -6 0 108.59 9.00 -3 -6 0 133.99 10.70 3 -6 0 126.29 10.50 -3 -6 0 111.89 9.70 -3 -6 0 131.19 9.50 3 -6 0 107.69 17.80 3 -6 0 104.79 10.90 -3 6 0 141.99 9.50 -3 6 0 127.89 9.50 -3 6 0 128.19 10.90 -3 6 0 109.19 20.50 3 6 0 125.49 9.70 3 6 0 115.29 10.50 -3 6 0 117.29 8.80 -3 6 0 118.39 9.20 -3 6 0 126.79 10.00 3 6 0 131.19 9.90 -4 -6 0 36.10 6.00 4 -6 0 31.90 7.40 -4 -6 0 30.50 4.10 4 -6 0 40.70 7.10 -4 -6 0 26.00 5.00 4 -6 0 25.10 4.60 4 -6 0 32.90 5.50 -4 -6 0 37.70 7.00 4 6 0 25.00 5.10 -4 6 0 18.00 6.20 -4 6 0 31.30 6.20 -4 6 0 31.30 6.20 -4 6 0 38.60 7.60 -5 -6 0 2.10 3.20 -5 -6 0 0.10 1.80 5 -6 0 8.40 3.60 5 -6 0 0.60 4.80 -5 -6 0 -0.60 5.90 5 -6 0 -3.90 3.10 -5 -6 0 3.90 3.60 -5 -6 0 -1.20 3.10 5 6 0 1.20 4.50 5 6 0 2.40 3.30 -5 6 0 1.20 2.50 -5 6 0 2.10 2.30 -5 6 0 -2.60 3.40 -5 6 0 -0.40 3.20 -6 -6 0 1.90 2.50 6 -6 0 8.70 1.80 6 6 0 1.30 3.30 -6 6 0 5.90 2.10 -6 6 0 3.80 2.20 0 -7 0 0.00 4.60 0 -7 0 1.40 4.90 0 -7 0 9.60 16.10 0 7 0 1.80 3.70 0 7 0 -2.30 3.50 0 7 0 -1.90 5.00 0 7 0 -3.00 3.60 0 7 0 0.00 3.80 0 7 0 -5.20 7.00 0 7 0 8.80 4.60 1 -7 0 -14.50 15.80 1 -7 0 8.20 5.20 -1 7 0 18.20 11.70 -1 7 0 9.50 3.50 -1 7 0 7.30 4.80 1 7 0 -0.10 3.90 -1 7 0 8.40 3.50 1 7 0 0.40 4.00 -1 7 0 1.20 3.40 1 7 0 2.70 6.10 -1 7 0 6.90 4.00 1 7 0 4.90 3.90 -2 -7 0 90.89 8.60 2 -7 0 86.39 11.70 2 -7 0 73.69 12.00 -2 -7 0 84.49 10.30 -2 -7 0 78.29 10.50 -2 7 0 88.19 7.90 -2 7 0 80.59 7.90 2 7 0 83.89 8.40 -2 7 0 90.19 7.60 -2 7 0 79.89 7.20 2 7 0 84.99 7.40 -2 7 0 97.29 9.50 -2 7 0 71.79 7.30 -3 -7 0 153.18 10.90 -3 -7 0 165.58 13.20 3 -7 0 126.19 14.50 3 -7 0 175.68 12.50 -3 -7 0 174.38 10.60 -3 -7 0 161.68 14.00 -3 7 0 165.18 10.10 3 7 0 158.58 11.10 -3 7 0 182.78 10.70 3 7 0 185.58 11.20 -3 7 0 152.48 9.70 -3 7 0 164.08 9.90 3 7 0 159.28 10.00 4 -7 0 12.50 7.10 -4 -7 0 27.60 5.70 -4 -7 0 27.10 4.40 4 -7 0 25.70 4.30 -4 -7 0 22.60 4.70 4 -7 0 27.20 4.80 -4 -7 0 34.00 4.60 -4 7 0 31.10 5.20 -4 7 0 23.90 4.70 4 7 0 34.20 6.00 4 7 0 21.00 3.80 -4 7 0 30.80 4.50 5 -7 0 36.10 4.10 -5 -7 0 38.40 3.20 -5 -7 0 44.60 6.20 -5 7 0 30.40 3.60 0 8 0 86.19 7.80 0 8 0 69.99 6.30 0 8 0 68.59 7.10 0 8 0 53.69 7.20 0 8 0 75.09 6.60 -1 -8 0 11.10 7.20 -1 8 0 5.40 4.70 -1 8 0 13.00 3.10 1 8 0 11.80 3.40 -1 8 0 9.30 3.20 -1 8 0 12.50 3.10 -1 8 0 16.10 3.90 1 8 0 8.90 3.20 -2 -8 0 31.30 6.70 -2 -8 0 37.00 7.40 -2 8 0 28.70 4.70 -2 8 0 25.30 5.50 -2 8 0 33.10 4.90 -2 8 0 33.90 5.00 2 8 0 33.20 5.50 -3 -8 0 112.09 7.70 -3 -8 0 136.19 12.10 -3 8 0 118.19 7.00 -3 8 0 118.89 6.90 3 8 0 118.49 7.20 -3 8 0 106.59 7.40 -4 8 0 5.30 2.60 4 8 0 7.60 3.30 -4 8 0 8.00 2.40 0 9 0 7.20 4.40 1 9 0 43.60 4.60 1 9 0 43.60 5.10 -1 9 0 37.40 4.10 -1 9 0 38.60 4.60 7 0 -1 56.89 5.20 7 0 -1 61.19 6.50 -7 0 1 45.40 5.60 -7 0 1 63.19 5.40 7 0 -1 55.59 6.60 -7 0 1 59.89 7.10 6 0 -1 1.60 4.00 -6 0 1 -7.00 14.50 6 0 -1 3.20 2.30 6 0 -1 3.30 2.90 -6 0 1 7.40 3.60 -6 0 1 8.90 3.00 6 0 -1 0.00 3.50 -6 0 1 -2.30 3.90 -5 0 1 27.50 4.80 -5 0 1 49.10 10.50 -5 0 1 39.10 6.50 -5 0 1 24.90 4.90 5 0 -1 14.80 10.80 5 0 -1 36.10 4.50 5 0 -1 29.60 6.60 5 0 -1 29.50 6.40 -5 0 1 37.50 10.50 -5 0 1 30.20 5.70 5 0 -1 42.40 5.20 -5 0 1 37.20 5.40 4 0 -1 2.70 2.70 -4 0 1 2.50 3.60 -4 0 1 8.10 3.70 -4 0 1 -3.50 3.50 -4 0 1 7.80 3.90 -4 0 1 6.30 3.10 4 0 -1 4.60 2.90 -4 0 1 6.80 3.00 -4 0 1 -3.30 4.90 4 0 -1 1.60 3.50 -4 0 1 2.30 2.70 4 0 -1 6.70 4.60 4 0 -1 3.90 2.90 3 0 -1 627.04 27.00 -3 0 1 662.53 28.00 -3 0 1 614.84 26.70 -3 0 1 637.84 26.50 -3 0 1 616.14 26.80 3 0 -1 612.34 26.60 3 0 -1 603.34 26.50 3 0 -1 611.64 27.20 -2 0 1 -2.20 1.60 2 0 -1 2.80 1.50 -2 0 1 3.30 1.80 2 0 -1 1.10 1.40 2 0 -1 1.60 1.60 -2 0 1 -1.20 1.60 -1 0 1 71.69 4.00 -1 0 1 68.99 3.80 1 0 -1 81.39 3.90 0 0 1 1.10 0.30 0 0 -1 1.30 0.30 0 0 -1 0.90 0.30 -1 0 -1 120.69 5.80 -1 0 -1 120.99 5.60 -1 0 -1 120.49 5.80 1 0 1 125.99 5.70 1 0 1 115.49 5.60 2 0 1 1.30 1.80 2 0 1 1.20 1.50 -2 0 -1 -1.30 1.70 2 0 1 3.50 1.90 -2 0 -1 -1.30 1.60 -3 0 -1 510.75 22.90 -3 0 -1 508.25 23.30 3 0 1 543.45 23.10 3 0 1 557.04 23.90 3 0 1 543.15 23.70 3 0 1 508.85 23.40 -3 0 -1 567.54 24.30 4 0 1 7.10 3.10 4 0 1 2.40 2.70 -4 0 -1 5.70 4.40 4 0 1 -2.10 3.90 -4 0 -1 3.10 2.90 -4 0 -1 1.90 3.00 -4 0 -1 4.10 2.60 4 0 1 1.90 2.50 4 0 1 -2.30 4.60 -4 0 -1 -2.80 5.10 -4 0 -1 -0.90 4.50 -4 0 -1 -5.80 3.60 5 0 1 116.19 9.10 5 0 1 126.39 7.40 -5 0 -1 127.89 8.30 5 0 1 115.79 9.50 -5 0 -1 126.79 8.90 5 0 1 120.29 18.40 5 0 1 117.49 8.30 -5 0 -1 126.59 15.90 -5 0 -1 116.39 7.20 -5 0 -1 122.19 10.20 -5 0 -1 137.69 9.40 6 0 1 2.00 3.30 -6 0 -1 -17.00 12.80 -6 0 -1 -4.10 2.60 6 0 1 2.90 2.80 6 0 1 -3.30 3.10 6 0 1 1.60 2.80 -6 0 -1 -4.30 3.70 -6 0 -1 0.30 3.10 -7 0 -1 5.90 3.00 -7 0 -1 4.50 2.60 7 0 1 6.20 2.40 7 0 1 4.00 2.90 7 0 1 3.00 2.80 -7 -1 1 2.40 2.70 7 -1 -1 2.50 3.00 7 -1 -1 2.50 2.60 -7 -1 1 -0.30 2.60 -7 -1 1 0.00 3.00 7 1 -1 -3.90 3.20 -7 1 1 1.10 2.20 7 1 -1 -2.60 2.30 7 1 -1 -0.90 2.60 -6 -1 1 5.50 4.30 -6 -1 1 26.50 15.30 -6 -1 1 14.20 3.30 -6 -1 1 12.30 4.00 6 -1 -1 -1.10 8.10 6 -1 -1 18.30 4.60 6 -1 -1 2.60 5.00 6 -1 -1 12.20 4.60 -6 -1 1 14.40 3.10 6 -1 -1 20.70 3.70 6 -1 -1 10.40 2.50 -6 1 1 -9.90 11.10 -6 1 1 14.90 4.60 6 1 -1 18.40 4.20 6 1 -1 10.20 4.10 6 1 -1 14.20 3.40 -6 1 1 2.80 12.20 -6 1 1 17.40 3.70 5 -1 -1 -2.80 3.70 5 -1 -1 -1.10 3.00 5 -1 -1 -5.40 11.20 5 -1 -1 -1.00 2.60 5 -1 -1 3.60 5.30 -5 -1 1 1.50 3.90 -5 -1 1 4.40 2.40 5 -1 -1 8.80 8.00 -5 -1 1 0.00 2.80 -5 -1 1 -4.70 5.70 5 -1 -1 -0.30 2.30 -5 -1 1 -0.30 6.10 -5 -1 1 -6.20 9.30 -5 -1 1 -0.90 3.60 5 -1 -1 6.30 4.50 -5 -1 1 3.20 2.60 5 1 -1 -1.10 2.70 -5 1 1 -2.50 2.70 5 1 -1 0.80 2.90 -5 1 1 -2.60 4.00 -5 1 1 0.90 3.40 -5 1 1 -13.00 11.00 5 1 -1 -6.30 4.20 -5 1 1 -2.20 7.90 -4 -1 1 183.38 11.90 4 -1 -1 169.58 9.50 4 -1 -1 169.68 9.80 -4 -1 1 159.78 9.80 4 -1 -1 180.68 10.40 -4 -1 1 181.58 10.20 -4 -1 1 174.08 10.90 4 -1 -1 188.68 12.40 -4 -1 1 153.28 9.20 -4 -1 1 150.68 12.20 -4 -1 1 171.48 9.00 -4 -1 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17.50 4.80 -4 -3 -4 33.60 6.00 4 -3 4 30.90 6.10 4 -3 4 27.50 6.10 -4 -3 -4 22.50 3.90 -4 -3 -4 26.50 4.00 4 3 4 26.70 4.90 -4 3 -4 22.60 7.70 4 3 4 29.10 5.40 -4 3 -4 24.00 8.50 -4 3 -4 38.90 7.90 -4 3 -4 27.30 6.60 -4 3 -4 21.50 4.80 -4 3 -4 25.40 4.00 -5 -3 -4 0.40 4.70 5 -3 4 7.10 3.30 5 -3 4 14.40 4.10 -5 -3 -4 11.90 3.70 -5 -3 -4 10.60 2.90 -5 -3 -4 25.40 7.20 5 -3 4 7.80 5.30 -5 -3 -4 10.60 3.70 5 -3 4 13.80 8.30 5 -3 4 29.50 14.10 5 -3 4 12.80 4.60 5 -3 4 6.90 2.70 -5 3 -4 25.00 14.90 5 3 4 9.30 2.80 5 3 4 0.50 4.50 -5 3 -4 14.20 3.70 -5 3 -4 9.80 4.40 5 3 4 2.20 5.30 5 3 4 4.60 5.20 -6 -3 -4 69.59 7.70 6 -3 4 77.49 5.80 6 -3 4 74.49 8.80 -6 -3 -4 83.09 5.90 6 -3 4 72.19 5.00 -6 -3 -4 89.49 8.00 -6 -3 -4 75.09 5.20 -6 3 -4 74.39 5.90 -6 3 -4 77.39 6.60 6 3 4 76.89 7.60 6 3 4 72.39 5.80 6 3 4 80.69 7.80 7 -3 4 -2.20 2.40 -7 -3 -4 -0.20 2.00 7 3 4 2.70 2.00 -7 3 -4 -3.00 2.10 7 3 4 3.40 3.10 -7 -4 4 33.10 4.40 -7 -4 4 51.59 5.10 -7 -4 4 42.40 6.10 7 -4 -4 47.00 6.40 7 -4 -4 45.00 5.00 -7 4 4 40.60 6.10 -7 4 4 55.69 4.50 7 4 -4 41.90 5.00 6 -4 -4 89.69 7.80 6 -4 -4 106.99 8.70 -6 -4 4 95.59 7.10 -6 -4 4 97.79 5.90 -6 -4 4 120.09 9.60 6 -4 -4 104.89 10.70 6 -4 -4 91.79 7.80 6 -4 -4 92.79 6.20 -6 -4 4 100.69 6.90 6 4 -4 107.09 8.60 -6 4 4 106.99 8.80 -6 4 4 94.39 7.60 -6 4 4 98.59 7.00 6 4 -4 95.39 6.70 -6 4 4 100.69 7.20 5 -4 -4 21.80 4.70 -5 -4 4 17.10 3.70 -5 -4 4 16.20 3.60 -5 -4 4 14.10 3.70 -5 -4 4 13.50 2.80 5 -4 -4 2.50 6.10 -5 -4 4 26.10 6.20 -5 -4 4 15.80 13.60 5 -4 -4 19.30 3.80 5 -4 -4 19.60 4.20 5 -4 -4 16.00 4.40 -5 -4 4 19.40 5.30 -5 4 4 12.20 4.20 -5 4 4 15.70 3.60 -5 4 4 15.80 3.30 -5 4 4 12.30 3.30 -5 4 4 10.50 5.20 -5 4 4 -25.00 20.70 -5 4 4 21.30 4.60 -5 4 4 10.10 4.10 -5 4 4 14.20 9.40 -5 4 4 -0.30 15.70 4 -4 -4 99.09 9.40 -4 -4 4 89.39 9.40 -4 -4 4 104.69 8.00 -4 -4 4 115.69 10.60 4 -4 -4 101.09 8.10 4 -4 -4 76.39 10.60 4 -4 -4 130.29 21.90 4 -4 -4 120.49 9.00 -4 -4 4 110.59 8.80 -4 -4 4 109.19 8.60 -4 -4 4 103.69 7.70 -4 4 4 116.89 9.40 -4 4 4 102.29 13.10 -4 4 4 109.19 18.50 -4 4 4 83.79 10.70 -4 4 4 106.89 10.50 -4 4 4 84.49 8.80 4 4 -4 113.19 12.00 -4 4 4 105.89 8.30 -4 4 4 101.99 8.60 -4 4 4 100.29 8.60 -3 -4 4 -2.90 2.80 3 -4 -4 0.80 3.20 -3 -4 4 0.10 2.80 -3 -4 4 -0.60 3.40 3 -4 -4 2.50 3.00 -3 -4 4 4.10 5.50 3 -4 -4 -5.40 7.00 3 -4 -4 5.20 4.70 -3 -4 4 4.80 3.30 -3 -4 4 -0.30 3.80 -3 -4 4 -2.10 5.00 -3 4 4 2.70 3.60 -3 4 4 -0.10 5.20 -3 4 4 10.30 5.10 -3 4 4 3.10 4.20 -3 4 4 3.40 5.50 -3 4 4 3.00 4.20 -3 4 4 3.70 3.80 -3 4 4 0.50 3.40 3 4 -4 -3.90 4.20 -3 4 4 1.70 4.40 -3 4 4 -4.40 6.20 -2 -4 4 27.40 5.60 -2 -4 4 38.10 6.20 2 -4 -4 26.50 4.00 -2 -4 4 29.20 4.20 2 -4 -4 30.90 5.90 2 -4 -4 30.20 4.20 -2 -4 4 39.80 6.60 -2 -4 4 37.90 6.60 -2 -4 4 34.90 4.90 -2 4 4 17.30 5.90 -2 4 4 26.90 6.40 -2 4 4 39.90 5.90 -2 4 4 34.80 6.00 -2 4 4 21.60 4.20 2 4 -4 23.50 4.20 -2 4 4 31.20 6.70 -2 4 4 21.00 5.20 -2 4 4 37.30 6.60 -2 4 4 29.70 5.50 2 4 -4 36.80 6.80 -2 4 4 31.10 5.30 -2 4 4 38.90 6.10 -2 4 4 40.90 8.80 2 4 -4 29.00 5.50 -1 -4 4 302.67 15.30 1 -4 -4 311.47 15.80 -1 -4 4 300.47 14.10 -1 -4 4 305.37 13.90 -1 -4 4 312.17 15.90 -1 4 4 281.07 15.80 -1 4 4 282.17 16.90 -1 4 4 298.27 16.30 1 4 -4 285.77 14.60 -1 4 4 311.77 15.00 -1 4 4 286.27 15.30 -1 4 4 303.97 16.30 -1 4 4 284.77 15.00 -1 4 4 317.07 16.30 1 4 -4 303.67 14.70 -1 4 4 314.57 16.60 -1 4 4 298.67 17.80 -1 4 4 302.57 16.30 -1 4 4 317.87 18.90 1 4 -4 285.37 15.20 -1 4 4 300.67 16.40 1 4 -4 275.57 14.80 -1 4 4 281.27 15.40 0 -4 -4 30.50 5.40 0 -4 -4 21.90 4.90 0 -4 4 26.70 4.80 0 -4 4 21.80 3.40 0 -4 4 30.20 3.80 0 -4 4 25.80 4.50 0 -4 4 24.60 4.00 0 4 4 24.80 5.20 0 4 4 35.80 8.10 0 4 4 16.30 6.90 0 4 4 24.10 5.10 0 4 4 32.90 5.20 0 4 4 19.00 4.40 0 4 -4 15.70 4.20 0 4 4 24.00 4.10 0 4 4 24.90 7.40 0 4 4 17.80 4.00 0 4 -4 28.50 5.10 0 4 -4 30.70 5.10 0 4 -4 38.60 7.80 0 4 -4 29.60 4.60 0 4 -4 25.30 4.90 1 -4 4 304.97 14.10 -1 -4 -4 288.27 13.60 -1 -4 -4 320.07 13.30 1 -4 4 301.57 13.80 1 -4 4 308.97 15.70 1 -4 4 310.87 14.30 1 -4 4 318.87 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8 15.80 3.70 6 5 -8 18.50 3.20 -6 5 8 16.00 3.30 -6 5 8 12.80 2.90 5 -5 -8 10.60 3.90 -5 -5 8 9.70 8.70 -5 -5 8 15.50 3.20 -5 -5 8 19.70 4.40 5 -5 -8 14.60 4.50 5 -5 -8 14.40 5.60 -5 -5 8 17.90 5.50 -5 -5 8 20.30 3.60 -5 5 8 12.00 4.30 -5 5 8 17.00 4.50 -5 5 8 14.00 3.50 -5 5 8 20.30 4.10 -5 5 8 24.70 7.10 -5 5 8 15.90 3.90 -4 -5 8 142.19 10.60 -4 -5 8 146.69 9.60 -4 -5 8 140.29 11.00 4 -5 -8 129.89 11.60 4 -5 -8 121.09 10.60 -4 -5 8 94.59 17.80 -4 -5 8 139.39 8.20 -4 -5 8 122.79 9.20 4 -5 -8 117.09 12.50 -4 5 8 137.29 9.60 -4 5 8 137.49 9.60 -4 5 8 145.69 10.80 4 5 -8 154.88 12.00 -4 5 8 143.19 10.00 -4 5 8 123.29 12.00 -4 5 8 128.49 9.10 -4 5 8 148.09 9.60 -4 5 8 115.69 11.00 -3 -5 8 183.68 10.30 3 -5 -8 193.78 12.50 -3 -5 8 185.38 20.70 -3 -5 8 168.38 14.20 -3 -5 8 195.38 11.70 -3 -5 8 162.88 14.30 -3 -5 8 171.18 23.70 3 -5 -8 174.28 12.30 -3 -5 8 182.88 12.20 -3 -5 8 176.88 11.40 -3 5 8 187.08 12.00 -3 5 8 183.98 11.80 -3 5 8 190.28 12.10 -3 5 8 188.88 11.20 -3 5 8 169.48 22.30 -3 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4.40 4 -5 -9 48.50 6.80 -4 -5 9 46.60 6.50 -4 -5 9 59.79 7.80 -4 -5 9 40.60 5.20 -4 -5 9 38.00 6.70 -4 -5 9 33.70 12.70 -4 -5 9 57.89 6.50 -4 5 9 46.70 6.70 -4 5 9 50.99 7.10 -4 5 9 54.09 6.80 -4 5 9 60.69 8.00 -4 5 9 43.50 8.20 4 5 -9 56.39 8.40 -4 5 9 59.49 9.30 -4 5 9 62.69 10.30 3 -5 -9 145.69 11.00 -3 -5 9 134.99 10.10 -3 -5 9 129.79 10.70 3 -5 -9 136.29 11.70 -3 -5 9 132.59 12.00 -3 -5 9 102.99 16.40 -3 -5 9 129.29 9.30 -3 -5 9 163.98 22.00 -3 -5 9 109.59 13.60 -3 -5 9 140.09 8.20 -3 5 9 118.59 24.90 -3 5 9 128.19 10.80 -3 5 9 123.29 11.10 -3 5 9 110.49 9.80 3 5 -9 142.29 10.10 -3 5 9 125.09 9.70 -3 5 9 151.28 11.40 -3 5 9 116.89 10.70 -3 5 9 118.59 9.50 -3 5 9 131.19 9.50 -2 -5 9 13.30 4.30 -2 -5 9 7.70 3.20 2 -5 -9 12.90 5.30 -2 -5 9 11.90 5.10 -2 -5 9 10.20 4.30 -2 -5 9 12.00 4.10 -2 -5 9 -1.00 8.70 2 -5 -9 21.30 6.20 -2 -5 9 9.50 5.50 2 -5 -9 57.99 23.30 -2 -5 9 3.90 8.50 -2 5 9 5.20 10.70 -2 5 9 21.20 8.30 -2 5 9 10.60 4.10 -2 5 9 11.50 5.20 -2 5 9 12.90 4.80 2 5 -9 11.20 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8.10 1 -5 9 -0.60 3.90 1 -5 9 3.10 3.60 1 -5 9 0.40 3.80 -1 -5 -9 4.10 4.00 -1 -5 -9 -0.60 4.70 -1 5 -9 -0.80 4.10 1 5 9 2.60 2.90 1 5 9 9.90 5.10 -1 5 -9 5.10 5.00 1 5 9 -7.60 5.80 1 5 9 1.50 4.70 1 5 9 2.30 5.10 1 5 9 2.30 4.00 -1 5 -9 5.90 3.50 1 5 9 -0.70 3.40 2 -5 9 3.80 3.50 2 -5 9 -0.20 2.60 2 -5 9 0.40 10.20 -2 -5 -9 0.50 4.30 2 -5 9 8.00 6.80 -2 -5 -9 -1.70 4.10 2 -5 9 -5.30 4.10 2 -5 9 2.30 6.70 -2 5 -9 -0.40 3.10 -2 5 -9 4.30 4.80 2 5 9 13.70 5.70 -2 5 -9 4.90 5.20 -2 5 -9 1.30 3.80 -2 5 -9 38.00 22.60 2 5 9 8.00 4.30 2 5 9 4.10 3.80 -3 -5 -9 17.50 4.20 3 -5 9 24.40 4.00 -3 -5 -9 27.10 5.10 -3 -5 -9 29.10 6.50 3 -5 9 12.10 5.50 3 -5 9 33.70 6.60 3 -5 9 20.30 3.90 3 -5 9 15.50 9.40 -3 5 -9 20.70 4.70 -3 5 -9 6.50 6.70 -3 5 -9 18.50 6.70 3 5 9 19.10 5.30 3 5 9 24.50 5.30 3 5 9 35.20 9.20 3 5 9 16.10 4.20 -3 5 -9 22.00 7.00 -3 5 -9 26.40 5.20 4 -5 9 14.70 3.00 4 -5 9 3.50 8.20 -4 -5 -9 15.90 5.10 -4 -5 -9 14.90 2.90 4 -5 9 14.50 3.50 4 -5 9 17.20 3.40 4 -5 9 17.70 4.50 -4 -5 -9 21.10 5.70 4 5 9 12.70 3.20 -4 5 -9 17.70 5.00 -4 5 -9 10.20 2.90 4 5 9 8.20 3.50 4 5 9 14.10 3.90 5 -5 9 21.70 2.70 -5 -5 -9 16.90 2.80 5 -5 9 19.20 3.30 5 -5 9 17.30 3.60 -5 -5 -9 17.60 3.80 5 5 9 15.90 3.80 -5 5 -9 15.00 3.40 5 -6 -9 8.20 6.20 -5 -6 9 3.60 2.10 -5 -6 9 4.00 2.40 5 -6 -9 -3.70 5.40 -5 6 9 7.30 2.60 -5 6 9 2.20 2.30 -5 6 9 2.50 3.90 -5 6 9 1.00 2.90 -4 -6 9 9.60 2.40 -4 -6 9 8.20 6.50 -4 -6 9 14.90 3.70 -4 -6 9 13.80 3.00 -4 -6 9 16.60 4.30 4 -6 -9 11.40 9.70 -4 6 9 15.70 5.90 -4 6 9 21.80 5.10 -4 6 9 16.00 3.80 4 6 -9 11.30 5.00 -4 6 9 13.70 4.20 -4 6 9 9.90 3.20 -4 6 9 16.80 3.50 -4 6 9 10.40 3.70 3 -6 -9 9.20 12.60 3 -6 -9 13.50 8.70 -3 -6 9 2.60 3.90 -3 -6 9 15.60 8.70 -3 -6 9 8.10 7.90 -3 -6 9 6.00 4.00 -3 -6 9 -0.60 5.10 -3 -6 9 13.70 3.80 -3 6 9 13.20 4.00 -3 6 9 8.40 3.40 -3 6 9 11.70 5.50 -3 6 9 9.50 3.70 -3 6 9 9.40 4.20 -3 6 9 12.20 5.60 3 6 -9 11.10 4.10 -2 -6 9 22.90 20.30 -2 -6 9 1.30 5.50 -2 -6 9 7.60 4.10 -2 -6 9 11.80 6.60 -2 -6 9 5.80 3.80 -2 -6 9 6.40 4.70 -2 -6 9 7.00 3.10 -2 6 9 4.60 4.30 -2 6 9 10.60 4.80 -2 6 9 0.80 4.10 -2 6 9 8.50 4.00 -2 6 9 5.40 3.70 -2 6 9 5.30 4.00 -2 6 9 10.60 4.60 -2 6 9 7.60 5.30 2 6 -9 6.20 3.40 -2 6 9 4.20 4.90 2 6 -9 -2.00 4.40 -2 6 9 11.10 5.10 -1 -6 9 8.20 6.60 -1 -6 9 21.90 11.90 -1 -6 9 10.70 3.00 -1 -6 9 9.60 5.30 -1 -6 9 6.90 4.30 -1 -6 9 7.00 3.80 -1 -6 9 -1.60 12.70 -1 -6 9 8.10 4.00 1 6 -9 6.00 3.90 -1 6 9 11.30 4.20 -1 6 9 13.50 4.20 -1 6 9 31.90 17.90 -1 6 9 10.40 5.30 1 6 -9 10.20 3.80 -1 6 9 6.60 5.10 -1 6 9 -2.60 6.80 -1 6 9 9.30 4.90 -1 6 9 10.10 4.80 -1 6 9 5.50 4.10 1 6 -9 2.30 4.60 -1 6 9 0.50 4.50 0 -6 9 34.60 7.40 0 -6 9 27.70 10.70 0 -6 9 56.29 7.90 0 -6 9 51.19 7.50 0 -6 9 49.80 6.90 0 -6 9 49.20 5.60 0 -6 9 42.30 13.00 0 6 9 41.80 10.10 0 6 -9 58.69 6.40 0 6 9 35.60 8.00 0 6 9 60.59 9.50 0 6 9 33.40 7.60 0 6 9 49.50 6.60 0 6 9 37.80 7.50 0 6 9 39.70 6.80 0 6 -9 48.80 6.30 0 6 -9 44.60 8.00 0 6 9 39.90 6.30 1 -6 9 5.00 13.00 1 -6 9 10.40 4.00 1 -6 9 24.70 5.30 -1 -6 -9 22.50 6.70 1 -6 9 -9.60 13.20 1 -6 9 14.50 3.20 -1 -6 -9 13.80 6.60 1 -6 9 12.00 7.00 1 -6 9 15.30 4.50 -1 6 -9 17.80 3.90 1 6 9 7.10 4.40 1 6 9 14.40 4.10 -1 6 -9 12.00 5.00 -1 6 -9 15.80 3.80 2 -6 9 6.60 5.10 -2 -6 -9 5.90 6.50 -2 -6 -9 0.30 6.90 2 -6 9 11.30 4.30 2 -6 9 -6.20 7.90 2 -6 9 7.60 4.30 2 6 9 1.40 6.60 -2 6 -9 9.00 3.10 2 6 9 8.70 4.20 -2 6 -9 10.20 4.50 -3 -6 -9 0.80 4.10 3 -6 9 4.00 2.20 3 -6 9 15.50 6.40 -3 -6 -9 -7.00 5.20 3 -6 9 5.30 3.10 3 -6 9 -2.80 3.60 -3 6 -9 0.10 2.80 3 6 9 0.80 3.20 -3 6 -9 3.10 6.20 3 6 9 2.10 3.70 -3 6 -9 2.40 3.80 3 6 9 3.90 2.70 4 -6 9 17.50 2.80 4 -6 9 11.20 2.90 -4 -6 -9 18.20 3.90 4 -6 9 17.60 4.20 -4 -6 -9 13.90 4.50 4 -6 9 20.30 3.40 4 6 9 16.30 3.50 4 6 9 13.70 3.00 -4 -7 9 19.20 4.80 -4 -7 9 21.10 2.90 -4 -7 9 38.00 7.80 -4 7 9 27.70 5.90 -4 7 9 33.40 6.00 -4 7 9 24.70 5.40 -4 7 9 26.90 4.30 -4 7 9 26.70 4.70 -3 -7 9 2.60 2.10 -3 -7 9 8.30 3.50 -3 -7 9 3.10 5.90 -3 -7 9 5.80 4.30 -3 -7 9 -0.40 3.40 -3 7 9 -0.10 2.90 -3 7 9 6.70 3.20 -3 7 9 -1.10 3.00 3 7 -9 5.20 3.60 -3 7 9 7.70 3.40 -3 7 9 -4.00 4.30 -3 7 9 6.50 3.10 -2 -7 9 2.90 3.90 -2 -7 9 -0.80 2.40 -2 -7 9 -2.10 3.60 -2 -7 9 0.50 5.30 -2 7 9 2.80 3.40 -2 7 9 3.20 3.50 2 7 -9 -0.90 3.00 -2 7 9 -2.30 3.70 -2 7 9 5.30 4.70 2 7 -9 4.70 4.20 -2 7 9 0.20 5.30 -2 7 9 2.60 3.30 -2 7 9 -2.50 3.60 -1 -7 9 -3.20 5.70 -1 -7 9 22.90 9.40 -1 -7 9 -2.00 6.10 -1 -7 9 -3.00 4.10 -1 -7 9 3.00 2.60 -1 -7 9 -1.10 3.60 -1 7 9 0.30 4.80 -1 7 9 4.60 5.60 -1 7 9 0.00 3.00 -1 7 9 0.50 3.80 -1 7 9 4.40 3.90 1 7 -9 -0.70 2.90 -1 7 9 6.90 3.90 -1 7 9 7.30 3.70 0 -7 9 8.80 4.40 0 -7 9 10.30 3.90 0 -7 9 9.90 2.80 0 -7 9 13.00 9.10 0 7 9 14.10 3.90 0 7 -9 11.80 3.50 0 7 9 4.20 4.30 0 7 9 13.70 4.70 0 7 9 13.20 6.90 0 7 9 5.70 4.00 0 7 -9 7.00 4.10 0 7 9 12.00 4.40 0 7 -9 14.90 4.00 1 -7 9 69.99 9.20 1 -7 9 99.89 7.90 1 -7 9 88.89 6.20 -1 7 -9 99.69 7.20 -1 7 -9 80.09 7.10 -1 7 -9 84.79 8.20 1 7 9 82.69 8.10 1 7 9 95.99 7.80 1 7 9 83.09 7.10 2 -7 9 74.99 7.10 2 -7 9 80.39 5.30 2 -7 9 93.09 10.60 2 -7 9 65.99 7.00 2 -7 9 85.29 7.40 2 7 9 71.19 6.80 2 7 9 74.49 6.20 -2 7 -9 94.99 9.00 2 7 9 71.79 6.70 -2 7 -9 74.59 6.10 3 -7 9 1.60 3.00 3 -7 9 -5.60 3.60 3 -7 9 4.20 1.70 3 -7 9 0.80 4.00 3 7 9 1.50 2.60 3 7 9 -0.60 3.50 3 7 9 0.00 2.30 -3 7 -9 10.20 3.90 -2 -8 9 39.70 7.50 -2 -8 9 27.10 3.70 -2 -8 9 26.00 4.40 2 8 -9 18.80 4.10 -1 -8 9 2.30 2.20 -1 -8 9 2.80 3.80 1 8 -9 3.80 3.10 0 -8 9 31.50 3.90 0 -8 9 48.90 7.30 0 8 -9 44.20 4.30 0 8 9 33.20 5.40 0 8 9 25.80 5.50 0 8 -9 36.00 4.80 1 -8 9 25.80 4.80 1 -8 9 23.80 4.20 1 -8 9 11.50 5.40 1 8 9 15.50 3.10 1 8 9 24.60 5.10 -1 8 -9 20.10 3.80 1 8 9 12.50 3.60 2 -8 9 19.00 2.90 2 8 9 25.90 3.80 -2 8 -9 20.40 3.60 7 0 -10 -1.40 4.50 -7 0 10 6.50 2.20 -7 0 10 3.70 3.20 7 0 -10 0.20 1.90 -6 0 10 40.90 8.70 6 0 -10 40.30 4.50 -6 0 10 34.20 5.80 6 0 -10 41.70 8.80 -5 0 10 -6.10 11.10 5 0 -10 8.40 8.80 5 0 -10 2.00 3.90 -5 0 10 0.10 3.10 5 0 -10 6.60 5.90 -5 0 10 6.50 4.50 5 0 -10 1.60 2.60 -5 0 10 -0.30 4.10 -5 0 10 -6.60 5.50 4 0 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-3 10 16.00 3.30 1 -3 10 17.60 4.60 1 -3 10 21.30 5.00 1 -3 10 22.50 3.90 1 -3 10 27.50 4.30 1 3 10 22.80 5.30 1 3 10 22.70 4.20 -1 3 -10 31.30 4.80 1 3 10 22.20 4.60 -1 3 -10 37.90 6.90 -1 3 -10 22.00 5.70 1 3 10 38.10 8.80 2 -3 10 6.10 3.10 2 -3 10 5.10 4.60 2 -3 10 -12.50 9.50 2 -3 10 4.10 5.40 -2 -3 -10 1.90 3.30 2 -3 10 0.30 3.50 2 -3 10 3.90 2.40 -2 -3 -10 5.10 3.30 -2 -3 -10 8.40 7.50 -2 -3 -10 2.30 6.80 -2 -3 -10 -2.50 3.00 2 3 10 5.50 5.00 -2 3 -10 1.30 3.20 2 3 10 -2.50 2.70 2 3 10 -2.60 2.80 -2 3 -10 4.10 3.80 -2 3 -10 6.50 8.00 2 3 10 1.40 3.70 3 -3 10 244.48 14.80 -3 -3 -10 232.18 14.90 -3 -3 -10 226.48 12.80 3 -3 10 232.38 14.60 3 -3 10 229.98 11.30 -3 -3 -10 239.28 12.90 3 -3 10 244.58 19.30 -3 -3 -10 246.38 12.20 3 -3 10 213.18 12.80 3 -3 10 227.78 12.10 -3 -3 -10 214.68 14.10 3 3 10 232.38 13.40 3 3 10 228.38 13.20 -3 3 -10 228.58 12.70 -3 3 -10 226.68 12.60 3 3 10 230.78 11.70 3 3 10 217.28 14.10 -4 -3 -10 32.40 8.20 4 -3 10 -5.50 13.20 4 -3 10 30.50 6.10 -4 -3 -10 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19 3.40 5.20 -1 -2 -19 8.60 3.70 -1 -2 -19 8.00 2.90 -1 -2 -19 4.10 2.00 1 -2 19 7.20 2.80 -1 -2 -19 12.40 4.10 -1 -2 -19 -0.30 7.00 1 2 19 2.80 2.70 1 2 19 4.00 2.90 -1 2 -19 4.70 2.90 1 2 19 0.50 4.00 -1 2 -19 2.60 2.90 -1 2 -19 9.40 4.50 -2 -2 -19 2.30 4.30 -2 -2 -19 4.50 1.80 -2 -2 -19 7.40 2.50 2 -2 19 4.90 2.30 2 2 19 0.10 2.90 -2 2 -19 8.90 6.20 2 2 19 1.80 3.70 -2 2 -19 9.70 3.00 -3 -2 -19 0.90 2.00 -4 -3 19 31.90 4.30 4 -3 -19 25.80 3.30 -4 3 19 31.50 4.40 -3 -3 19 3.90 3.00 -3 -3 19 -5.60 4.40 3 -3 -19 -0.80 4.10 3 -3 -19 4.10 2.30 -3 3 19 7.70 8.40 -3 3 19 0.30 2.90 -3 3 19 -2.30 3.00 -3 3 19 1.90 2.80 -2 -3 19 29.80 5.50 2 -3 -19 26.00 4.80 -2 -3 19 14.90 3.20 2 -3 -19 28.00 7.50 -2 3 19 31.90 6.50 -2 3 19 25.00 4.50 -2 3 19 18.80 3.80 -2 3 19 23.00 4.40 -1 -3 19 14.10 3.00 1 -3 -19 7.90 6.20 1 -3 -19 4.60 7.80 1 -3 -19 11.20 2.50 -1 -3 19 7.30 4.10 -1 3 19 19.10 4.30 1 3 -19 12.00 3.50 -1 3 19 5.80 4.20 1 3 -19 16.40 3.90 -1 3 19 -0.90 5.40 -1 3 19 9.70 2.70 0 -3 -19 2.60 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-3.50 2.80 0 4 -19 -0.80 2.70 0 4 19 -14.00 9.30 0 4 -19 3.00 3.00 1 -4 19 0.70 2.20 -1 -4 -19 -0.10 3.00 1 -4 19 10.00 7.70 -1 -4 -19 12.20 4.70 -1 -4 -19 2.30 2.20 1 -4 19 -1.30 4.60 -1 4 -19 0.10 3.00 1 4 19 -3.50 3.70 -1 -5 19 3.60 2.20 -1 5 19 9.40 2.70 -4 0 20 143.39 9.00 -4 0 20 151.18 8.90 4 0 -20 114.59 6.40 -4 0 20 134.29 8.10 -4 0 20 123.39 7.40 3 0 -20 0.00 2.00 -3 0 20 5.40 2.70 -3 0 20 2.40 3.20 2 0 -20 4.10 3.00 -2 0 20 2.90 3.50 2 0 -20 0.60 2.50 2 0 -20 -6.70 5.60 -2 0 20 -5.70 4.10 -2 0 20 0.80 2.60 2 0 -20 2.10 2.20 1 0 -20 1.60 2.80 1 0 -20 -7.40 4.60 1 0 -20 -9.70 15.70 -1 0 20 0.90 3.50 -1 0 20 -1.80 3.40 -1 0 20 1.20 2.50 1 0 -20 -2.80 2.10 1 0 -20 1.30 2.40 0 0 -20 7.70 2.30 0 0 20 9.00 3.00 0 0 -20 10.60 2.80 0 0 20 12.80 2.90 0 0 20 7.60 4.80 0 0 -20 6.70 10.10 -1 0 -20 -1.50 1.90 -1 0 -20 0.80 2.70 1 0 20 3.70 2.30 1 0 20 2.50 2.60 -1 0 -20 -0.60 2.30 -2 0 -20 1.90 2.70 -2 0 -20 -0.80 2.30 2 0 20 0.00 2.10 2 0 20 -4.10 2.50 -4 -1 20 1.00 2.20 4 -1 -20 0.10 2.10 -4 -1 20 -5.30 4.80 -4 1 20 -0.20 3.40 -4 1 20 -1.50 2.60 -4 1 20 5.20 4.40 3 -1 -20 68.69 8.60 3 -1 -20 83.29 5.10 -3 -1 20 81.09 7.00 -3 -1 20 83.59 5.70 -3 1 20 77.09 5.40 -3 1 20 90.49 6.40 -3 1 20 77.99 7.10 -3 1 20 62.09 9.70 -3 1 20 82.79 10.40 2 -1 -20 -0.80 3.30 2 -1 -20 3.50 3.40 2 -1 -20 1.40 2.00 2 -1 -20 1.60 10.60 -2 -1 20 1.00 2.60 -2 -1 20 -2.10 3.10 2 -1 -20 -2.10 4.40 -2 1 20 3.50 3.30 2 1 -20 -0.30 2.80 -2 1 20 8.40 2.70 2 1 -20 2.80 2.60 -2 1 20 -0.40 3.40 -2 1 20 5.80 3.70 2 1 -20 2.80 2.40 -1 -1 20 24.50 4.60 1 -1 -20 29.30 4.90 1 -1 -20 29.50 4.30 1 -1 -20 26.70 4.90 -1 -1 20 27.70 4.00 -1 -1 20 20.60 4.40 1 -1 -20 24.50 3.90 -1 1 20 21.40 4.10 1 1 -20 30.10 3.80 1 1 -20 27.60 4.70 1 1 -20 32.10 4.50 -1 1 20 25.20 5.90 -1 1 20 27.10 4.90 -1 1 20 21.00 3.70 0 -1 20 6.40 4.20 0 -1 20 4.80 2.50 0 -1 -20 5.40 2.70 0 -1 20 10.10 3.60 0 -1 -20 7.50 3.20 0 -1 -20 13.80 4.60 0 -1 -20 1.60 10.50 0 -1 -20 5.80 2.10 0 1 20 10.20 2.70 0 1 -20 7.90 2.40 0 1 -20 11.30 2.50 0 1 20 1.70 3.00 0 1 -20 5.70 2.70 0 1 20 3.80 8.10 0 1 20 11.50 5.50 -1 -1 -20 -4.50 2.70 -1 -1 -20 0.00 2.30 1 -1 20 -9.30 10.10 -1 -1 -20 0.40 1.80 1 -1 20 -0.20 2.30 -1 -1 -20 -7.60 5.00 1 1 20 -3.60 2.30 1 1 20 4.70 2.50 1 1 20 5.10 6.80 -1 1 -20 -2.80 2.20 -1 1 -20 3.30 2.50 2 -1 20 19.60 3.50 -2 -1 -20 25.90 4.10 -2 -1 -20 21.00 3.10 -2 -1 -20 15.10 2.70 2 1 20 23.90 3.60 2 1 20 14.40 2.90 -2 1 -20 21.90 3.60 -2 1 -20 26.30 5.00 4 -2 -20 27.40 3.10 -4 -2 20 38.50 3.80 -4 2 20 40.40 6.10 3 -2 -20 7.00 2.10 -3 -2 20 8.90 2.60 -3 -2 20 4.90 3.10 3 -2 -20 2.90 4.30 -3 2 20 12.20 3.30 -3 2 20 8.20 3.20 -3 2 20 18.00 6.00 2 -2 -20 13.90 9.20 2 -2 -20 0.70 1.90 2 -2 -20 -5.10 4.10 -2 -2 20 2.30 2.50 -2 2 20 -1.20 3.20 -2 2 20 0.50 3.50 -2 2 20 2.00 2.80 1 -2 -20 11.40 7.80 -1 -2 20 4.50 2.80 1 -2 -20 5.60 3.90 1 -2 -20 -1.30 4.10 1 -2 -20 4.40 2.10 -1 2 20 2.90 2.50 -1 2 20 6.30 4.30 -1 2 20 11.90 5.10 1 2 -20 3.10 2.50 -1 2 20 -3.40 4.90 1 2 -20 -1.70 2.60 0 -2 20 1.20 2.40 0 -2 20 4.30 3.80 0 -2 -20 4.10 4.50 0 -2 -20 12.40 8.40 0 -2 -20 8.40 4.50 0 -2 -20 5.90 2.10 0 -2 -20 6.90 2.90 0 2 20 2.40 2.40 0 2 -20 9.30 3.00 0 2 -20 18.20 5.20 0 2 20 5.50 4.50 0 2 -20 6.70 2.30 1 -2 20 28.90 3.90 -1 -2 -20 17.30 2.50 -1 -2 -20 32.50 6.40 -1 -2 -20 20.10 4.10 -1 -2 -20 20.00 3.60 1 2 20 24.90 3.90 -1 2 -20 25.30 4.40 1 2 20 20.30 7.20 2 -2 20 2.30 2.20 -2 -2 -20 1.80 1.60 -2 -2 -20 6.10 2.30 -2 -2 -20 5.50 3.80 2 2 20 -1.00 2.50 2 2 20 2.80 4.30 3 -3 -20 21.80 3.10 3 -3 -20 14.40 5.10 -3 3 20 20.20 4.10 -3 3 20 15.30 3.10 2 -3 -20 -6.70 4.10 2 -3 -20 2.20 2.00 -2 -3 20 0.30 2.80 -2 3 20 -0.60 2.40 -2 3 20 8.70 4.50 -2 3 20 -3.70 4.00 -1 -3 20 -3.60 2.60 1 -3 -20 6.20 4.00 1 -3 -20 0.20 2.00 -1 -3 20 1.20 4.50 -1 3 20 5.30 2.40 -1 3 20 4.40 4.10 0 -3 -20 21.80 4.60 0 -3 -20 31.30 6.70 0 -3 20 22.70 4.40 0 -3 -20 23.20 3.20 0 3 20 24.60 5.90 0 3 -20 27.10 4.40 0 3 20 24.10 3.90 -1 -3 -20 4.70 2.70 1 -3 20 13.20 2.90 -1 -3 -20 8.60 4.80 -1 -3 -20 9.10 2.90 1 3 20 3.70 3.60 -1 3 -20 18.30 3.50 2 -4 -20 6.60 2.50 -2 -4 20 0.10 5.10 -2 4 20 2.40 2.60 -2 4 20 -3.20 2.70 -1 4 20 11.10 2.80 -1 4 20 8.50 3.60 -1 4 20 9.20 5.60 1 4 -20 12.40 3.80 0 -4 -20 25.60 4.10 0 4 20 31.40 4.30 0 4 20 37.40 5.30 0 4 -20 40.60 3.90 -3 0 21 8.20 2.80 -3 0 21 7.00 2.80 -2 0 21 2.50 5.20 -2 0 21 -3.30 2.40 -2 0 21 4.00 3.00 2 0 -21 2.10 2.70 2 0 -21 1.30 2.00 1 0 -21 5.00 2.40 1 0 -21 2.20 2.70 1 0 -21 4.70 2.10 -1 0 21 13.00 4.10 0 0 21 1.00 2.30 0 0 -21 4.40 2.10 0 0 -21 -0.30 2.20 0 0 -21 1.90 2.80 0 0 21 1.70 2.80 0 0 21 2.80 5.60 1 0 21 120.89 6.50 -1 0 -21 132.49 7.00 -1 0 -21 113.89 6.70 1 0 21 123.19 6.90 -3 -1 21 4.40 3.50 3 -1 -21 2.70 1.80 -3 -1 21 4.20 3.10 -3 -1 21 4.60 2.30 -3 1 21 4.50 2.90 2 -1 -21 21.70 3.20 -2 -1 21 18.00 3.30 -2 -1 21 14.30 3.60 2 1 -21 16.20 2.90 -2 1 21 22.60 5.20 -2 1 21 12.30 3.80 -2 1 21 20.70 3.70 -2 1 21 22.00 3.70 1 -1 -21 -1.80 2.50 1 -1 -21 -0.40 1.80 -1 -1 21 2.70 3.70 -1 -1 21 -0.90 4.70 -1 -1 21 -1.60 2.10 1 -1 -21 2.70 3.00 1 1 -21 -2.80 2.20 -1 1 21 2.10 2.50 -1 1 21 1.80 2.60 1 1 -21 0.90 2.40 -1 1 21 1.40 5.40 0 -1 -21 19.20 3.10 0 -1 -21 11.20 2.90 0 -1 21 15.80 3.60 0 -1 21 17.10 3.70 0 -1 -21 26.20 4.60 0 -1 -21 17.20 5.60 0 1 -21 16.80 3.40 0 1 21 19.40 3.40 0 1 21 21.90 7.30 0 1 -21 19.20 3.90 0 1 21 17.80 3.20 -1 -1 -21 0.60 2.30 -1 -1 -21 -1.70 2.10 1 -1 21 -1.40 2.10 1 -1 21 4.30 3.10 -1 1 -21 1.90 2.20 -1 1 -21 3.70 2.50 1 1 21 0.70 2.20 -3 -2 21 4.50 2.40 3 -2 -21 4.70 1.80 -3 2 21 9.70 3.00 -3 2 21 0.00 3.00 2 -2 -21 8.00 2.00 2 -2 -21 -2.00 4.50 -2 -2 21 8.40 3.00 -2 -2 21 6.30 2.60 -2 2 21 3.10 3.00 -2 2 21 5.90 3.30 1 -2 -21 3.30 4.40 1 -2 -21 7.50 4.20 1 -2 -21 7.50 3.90 1 -2 -21 0.40 1.80 -1 2 21 -1.40 2.40 1 2 -21 -1.50 2.60 -1 2 21 5.20 4.80 0 -2 -21 17.70 4.50 0 -2 -21 14.40 3.40 0 -2 21 13.00 2.60 0 -2 21 8.40 5.20 0 -2 -21 23.40 2.90 0 2 21 25.00 3.80 0 2 21 -1.00 13.50 0 2 -21 18.40 3.50 0 2 -21 18.90 3.60 1 -2 21 17.50 4.10 -1 -2 -21 27.10 3.70 1 -2 21 24.00 3.80 -1 -2 -21 24.60 2.80 -1 2 -21 24.50 3.60 1 2 21 27.30 3.80 2 -3 -21 15.10 3.00 -2 -3 21 8.50 2.70 -2 -3 21 15.40 3.50 -2 3 21 17.10 3.90 -2 3 21 12.20 2.80 -1 -3 21 2.20 3.70 1 -3 -21 -5.40 4.90 -1 -3 21 1.30 2.80 -1 3 21 1.60 2.50 0 -3 -21 -2.20 1.70 0 3 21 3.30 2.40 0 3 -21 -2.60 2.90 -2 0 22 6.70 2.50 -2 0 22 2.90 3.10 -2 0 22 -2.90 4.30 1 0 -22 -0.10 3.10 -1 0 22 13.30 4.40 -1 0 22 6.90 4.60 -1 0 22 1.30 4.70 -1 0 22 4.20 2.30 0 0 -22 7.10 2.40 0 0 22 2.00 2.20 0 0 -22 -1.00 2.30 0 0 22 0.70 2.60 -2 -1 22 11.40 3.50 -2 -1 22 5.40 3.00 -2 -1 22 7.50 2.30 2 -1 -22 4.40 1.90 -2 1 22 0.20 3.80 -2 1 22 2.40 3.50 1 -1 -22 -0.20 2.90 -1 -1 22 0.70 2.50 1 -1 -22 4.30 1.90 1 -1 -22 7.00 3.00 1 1 -22 0.50 2.60 -1 1 22 -0.40 2.50 -1 1 22 -4.20 4.40 0 -1 -22 5.70 1.90 0 -1 -22 4.80 2.30 0 1 22 3.00 2.30 0 1 -22 -0.10 2.00 0 1 -22 1.10 2.10 1 -2 -22 5.90 1.80 -1 -2 22 -2.90 4.00 -1 -2 22 3.40 2.30 -1 2 22 6.70 2.70 -1 2 22 -3.30 7.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 52294 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.8298(3) 0.6407(2) 0.60748(10) 0.0200(4) Uani 1 1 d . . . . . H1 H 0.958095 0.679416 0.591731 0.024 Uiso 1 1 calc R U . . . C2 C 0.8067(3) 0.6545(2) 0.68072(10) 0.0198(4) Uani 1 1 d . . . . . H2 H 0.916585 0.704425 0.715398 0.024 Uiso 1 1 calc R U . . . C2A C 0.6167(3) 0.5939(2) 0.70529(10) 0.0188(4) Uani 1 1 d . . . . . C2B C 0.5433(3) 0.5909(2) 0.77695(10) 0.0202(4) Uani 1 1 d . . . . . C3 C 0.6301(3) 0.6447(2) 0.84899(10) 0.0225(4) Uani 1 1 d . . . . . H3 H 0.766272 0.698050 0.857773 0.027 Uiso 1 1 calc R U . . . C4 C 0.5136(3) 0.6184(3) 0.90705(11) 0.0246(4) Uani 1 1 d . . . . . H4 H 0.571036 0.653837 0.956147 0.030 Uiso 1 1 calc R U . . . C5 C 0.3108(3) 0.5400(3) 0.89459(11) 0.0247(4) Uani 1 1 d . . . . . H5 H 0.234183 0.524057 0.935496 0.030 Uiso 1 1 calc R U . . . C6 C 0.2212(3) 0.4859(2) 0.82411(11) 0.0230(4) Uani 1 1 d . . . . . H6 H 0.084831 0.432903 0.815761 0.028 Uiso 1 1 calc R U . . . C6A C 0.3397(3) 0.5125(2) 0.76560(10) 0.0203(4) Uani 1 1 d . . . . . N7 N 0.2902(2) 0.4710(2) 0.69083(9) 0.0204(4) Uani 1 1 d . . . . . H0 H 0.180(4) 0.415(3) 0.6708(13) 0.033(6) Uiso 1 1 d . . . . . C7A C 0.4557(3) 0.5208(2) 0.65381(10) 0.0188(4) Uani 1 1 d . . . . . C7B C 0.4702(3) 0.5083(2) 0.57595(10) 0.0181(4) Uani 1 1 d . . . . . C8 C 0.3103(3) 0.4427(2) 0.52223(10) 0.0193(4) Uani 1 1 d . . . . . H8 H 0.181035 0.404899 0.537503 0.023 Uiso 1 1 calc R U . . . C8A C 0.3341(3) 0.4310(2) 0.44689(10) 0.0191(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0144(8) 0.0194(9) 0.0265(10) 0.0014(7) 0.0036(7) -0.0010(6) C2 0.0152(8) 0.0175(8) 0.0256(9) -0.0014(7) -0.0006(7) -0.0010(6) C2A 0.0178(8) 0.0163(8) 0.0220(9) 0.0008(7) 0.0021(7) 0.0018(6) C2B 0.0188(8) 0.0159(8) 0.0256(10) 0.0003(7) 0.0016(7) 0.0037(6) C3 0.0210(9) 0.0199(9) 0.0256(9) -0.0021(7) -0.0002(7) 0.0023(7) C4 0.0264(10) 0.0246(9) 0.0218(9) -0.0020(7) -0.0001(7) 0.0048(7) C5 0.0261(10) 0.0246(9) 0.0243(10) 0.0025(7) 0.0071(7) 0.0040(7) C6 0.0221(9) 0.0204(9) 0.0265(10) 0.0017(7) 0.0040(7) 0.0024(7) C6A 0.0193(9) 0.0168(9) 0.0245(10) -0.0001(7) 0.0024(7) 0.0022(6) N7 0.0153(7) 0.0237(8) 0.0222(8) -0.0012(6) 0.0023(6) -0.0018(6) C7A 0.0157(8) 0.0157(8) 0.0251(10) 0.0010(7) 0.0028(7) 0.0007(6) C7B 0.0147(8) 0.0184(9) 0.0215(9) 0.0016(7) 0.0033(7) 0.0005(6) C8 0.0142(8) 0.0186(8) 0.0251(10) 0.0021(7) 0.0031(7) -0.0013(6) C8A 0.0148(8) 0.0166(8) 0.0257(10) 0.0016(7) 0.0023(7) 0.0004(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C8A 121.86(16) . 3_666 ? C2 C1 H1 119.1 . . ? C8A C1 H1 119.1 3_666 . ? C1 C2 C2A 119.63(16) . . ? C1 C2 H2 120.2 . . ? C2A C2 H2 120.2 . . ? C7A C2A C2 119.78(16) . . ? C7A C2A C2B 106.92(15) . . ? C2 C2A C2B 133.30(16) . . ? C3 C2B C6A 119.33(17) . . ? C3 C2B C2A 134.10(17) . . ? C6A C2B C2A 106.56(16) . . ? C4 C3 C2B 118.65(17) . . ? C4 C3 H3 120.7 . . ? C2B C3 H3 120.7 . . ? C3 C4 C5 121.17(18) . . ? C3 C4 H4 119.4 . . ? C5 C4 H4 119.4 . . ? C6 C5 C4 121.39(18) . . ? C6 C5 H5 119.3 . . ? C4 C5 H5 119.3 . . ? C5 C6 C6A 117.25(18) . . ? C5 C6 H6 121.4 . . ? C6A C6 H6 121.4 . . ? N7 C6A C6 129.41(17) . . ? N7 C6A C2B 108.38(16) . . ? C6 C6A C2B 122.21(17) . . ? C7A N7 C6A 109.17(15) . . ? C7A N7 H0 124.7(16) . . ? C6A N7 H0 126.0(16) . . ? N7 C7A C2A 108.96(15) . . ? N7 C7A C7B 128.39(16) . . ? C2A C7A C7B 122.63(16) . . ? C8 C7B C7A 124.55(16) . . ? C8 C7B C8A 119.35(17) . 3_666 ? C7A C7B C8A 116.10(16) . 3_666 ? C8A C8 C7B 122.16(16) . . ? C8A C8 H8 118.9 . . ? C7B C8 H8 118.9 . . ? C8 C8A C1 121.56(16) . 3_666 ? C8 C8A C7B 118.49(16) . 3_666 ? C1 C8A C7B 119.96(16) 3_666 3_666 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.357(3) . ? C1 C8A 1.437(2) 3_666 ? C1 H1 0.9500 . ? C2 C2A 1.424(2) . ? C2 H2 0.9500 . ? C2A C7A 1.399(2) . ? C2A C2B 1.439(3) . ? C2B C3 1.402(3) . ? C2B C6A 1.415(2) . ? C3 C4 1.384(3) . ? C3 H3 0.9500 . ? C4 C5 1.411(3) . ? C4 H4 0.9500 . ? C5 C6 1.383(3) . ? C5 H5 0.9500 . ? C6 C6A 1.399(3) . ? C6 H6 0.9500 . ? C6A N7 1.381(2) . ? N7 C7A 1.380(2) . ? N7 H0 0.85(3) . ? C7A C7B 1.427(3) . ? C7B C8 1.397(2) . ? C7B C8A 1.444(2) 3_666 ? C8 C8A 1.395(3) . ? C8 H8 0.9500 . ?