#------------------------------------------------------------------------------ #$Date: 2021-05-30 00:25:04 +0300 (Sun, 30 May 2021) $ #$Revision: 265617 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/87/4518757.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4518757 loop_ _publ_author_name 'Ao, Yu-Fei' 'Hu, Hui-Juan' 'Zhao, Cheng-Xin' 'Chen, Peng' 'Huang, Tingting' 'Chen, Hui' 'Wang, Qi-Qiang' 'Wang, De-Xian' 'Wang, Mei-Xiang' _publ_section_title ; Reversal and Amplification of the Enantioselectivity of Biocatalytic Desymmetrization toward Meso Heterocyclic Dicarboxamides Enabled by Rational Engineering of Amidase ; _journal_name_full 'ACS Catalysis' _journal_page_first 6900 _journal_page_last 6907 _journal_paper_doi 10.1021/acscatal.1c01220 _journal_year 2021 _chemical_absolute_configuration ad _chemical_formula_moiety '2(C14 H17 N O4)' _chemical_formula_sum 'C28 H34 N2 O8' _chemical_formula_weight 526.57 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-12-03 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 90 _cell_angle_beta 95.829(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 7.9990(2) _cell_length_b 14.9431(3) _cell_length_c 11.0324(2) _cell_measurement_reflns_used 20074 _cell_measurement_temperature 170.01(10) _cell_measurement_theta_max 30.6680 _cell_measurement_theta_min 1.8500 _cell_volume 1311.88(5) _computing_cell_refinement 'CrysAlisPro 1.171.39.45i (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.45i (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.45i (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 170.01(10) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.905 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -100.00 78.00 0.50 5.00 -- -11.40 45.00 -12.34 356 2 \w -100.00 78.00 0.50 5.00 -- -11.40 45.00 120.00 356 3 \w -100.00 78.00 0.50 5.00 -- -11.40 45.00 60.00 356 4 \w -100.00 78.00 0.50 5.00 -- -11.40 45.00 178.51 356 5 \w -84.00 27.00 0.50 5.00 -- 5.00 45.00 90.00 222 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC10 (RCD3): fixed-chi single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0528080000 _diffrn_orient_matrix_UB_12 0.0365523000 _diffrn_orient_matrix_UB_13 0.0192049000 _diffrn_orient_matrix_UB_21 -0.0713701000 _diffrn_orient_matrix_UB_22 0.0282788000 _diffrn_orient_matrix_UB_23 -0.0009765000 _diffrn_orient_matrix_UB_31 -0.0080603000 _diffrn_orient_matrix_UB_32 -0.0108229000 _diffrn_orient_matrix_UB_33 0.0616939000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0227 _diffrn_reflns_av_unetI/netI 0.0186 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.905 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 32333 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.860 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.046 _diffrn_reflns_theta_min 1.855 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.098 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.65407 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.45i (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.333 _exptl_crystal_description block _exptl_crystal_F_000 560 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.14 _refine_diff_density_max 0.199 _refine_diff_density_min -0.168 _refine_diff_density_rms 0.033 _refine_ls_abs_structure_details ; Flack x determined using 2932 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.01(16) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 343 _refine_ls_number_reflns 7224 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.077 _refine_ls_R_factor_all 0.0335 _refine_ls_R_factor_gt 0.0301 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0428P)^2^+0.0935P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0763 _refine_ls_wR_factor_ref 0.0779 _reflns_Friedel_coverage 0.839 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.813 _reflns_number_gt 6730 _reflns_number_total 7224 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c01220_si_002.cif _cod_data_source_block mx8954 _cod_database_code 4518757 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula CHON _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.986 _shelx_estimated_absorpt_t_min 0.973 _reflns_odcompleteness_completeness 99.97 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 27.42 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H,H) groups 2.a Ternary CH refined with riding coordinates: C2(H2), C6(H6), C16(H16), C20(H20) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C4(H4A,H4B), C5(H5A,H5B), C8(H8A,H8B), C17(H17A,H17B), C18(H18A, H18B), C19(H19A,H19B), C22(H22A,H22B) 2.c Aromatic/amide H refined with riding coordinates: C10(H10), C11(H11), C12(H12), C13(H13), C14(H14), C24(H24), C25(H25), C26(H26), C27(H27), C28(H28) 2.d X=CH2 refined with riding coordinates: N1(H1A,H1B), N2(H2A,H2B) ; _shelx_res_file ; TITL mx8954_a.res in P2(1) mx8954.res created by SHELXL-2018/3 at 09:04:37 on 03-Dec-2020 REM Old TITL MX8954 in P2(1)/m REM SHELXT solution in P2(1): R1 0.094, Rweak 0.027, Alpha 0.001 REM 0.335 for 8 systematic absences, Orientation as input REM Flack x = 0.002 ( 0.157 ) from 2420 Parsons' quotients REM Formula found by SHELXT: C22 N2 O4 CELL 0.71073 7.999 14.9431 11.0324 90 95.829 90 ZERR 2 0.0002 0.0003 0.0002 0 0.002 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 56 68 4 16 L.S. 4 PLAN 1 SIZE 0.14 0.18 0.28 CONF BOND LIST 6 fmap 2 MORE -1 BOND $H ACTA REM REM REM WGHT 0.042800 0.093500 FVAR 0.68530 O1 4 0.404660 0.412265 0.629929 11.00000 0.05117 0.04256 = 0.02709 -0.00033 0.01452 -0.01359 O2 4 0.613513 0.459299 0.367886 11.00000 0.03053 0.02427 = 0.01993 -0.00023 0.00714 0.00062 O3 4 0.795632 0.547129 0.211572 11.00000 0.04453 0.02815 = 0.02838 -0.00180 0.00712 -0.00377 O4 4 0.710880 0.449309 0.063007 11.00000 0.03167 0.04071 = 0.02443 -0.00591 0.01194 -0.00371 N1 3 0.558340 0.530764 0.579758 11.00000 0.04653 0.03611 = 0.02706 -0.00494 0.01607 -0.00918 AFIX 93 H1A 2 0.541898 0.559435 0.645089 11.00000 -1.20000 H1B 2 0.618096 0.554305 0.527571 11.00000 -1.20000 AFIX 0 C1 1 0.491779 0.450528 0.559558 11.00000 0.02893 0.03220 = 0.02043 0.00176 0.00280 0.00068 C2 1 0.525456 0.402173 0.443793 11.00000 0.02598 0.02603 = 0.02160 0.00375 0.00321 0.00094 AFIX 13 H2 2 0.417297 0.386133 0.399328 11.00000 -1.20000 AFIX 0 C3 1 0.623661 0.316760 0.473985 11.00000 0.03994 0.03157 = 0.03181 0.00960 0.00125 0.00688 AFIX 23 H3A 2 0.561954 0.278768 0.525131 11.00000 -1.20000 H3B 2 0.731142 0.331139 0.518517 11.00000 -1.20000 AFIX 0 C4 1 0.651634 0.267572 0.357353 11.00000 0.04662 0.02348 = 0.04528 0.00306 0.00891 0.01052 AFIX 23 H4A 2 0.545103 0.245607 0.318835 11.00000 -1.20000 H4B 2 0.724771 0.216594 0.376152 11.00000 -1.20000 AFIX 0 C5 1 0.730917 0.330209 0.270713 11.00000 0.03393 0.02503 = 0.03601 -0.00224 0.00757 0.00735 AFIX 23 H5A 2 0.734231 0.301105 0.192403 11.00000 -1.20000 H5B 2 0.845453 0.343664 0.303086 11.00000 -1.20000 AFIX 0 C6 1 0.630344 0.417038 0.253943 11.00000 0.02491 0.02502 = 0.02218 -0.00199 0.00382 0.00362 AFIX 13 H6 2 0.518559 0.404050 0.212850 11.00000 -1.20000 AFIX 0 C7 1 0.721006 0.480801 0.176898 11.00000 0.02442 0.02582 = 0.02265 -0.00130 0.00366 0.00626 C8 1 0.819770 0.488144 -0.021178 11.00000 0.03834 0.03320 = 0.02903 -0.00025 0.01571 0.00237 AFIX 23 H8A 2 0.896775 0.530568 0.021145 11.00000 -1.20000 H8B 2 0.753128 0.519352 -0.086360 11.00000 -1.20000 AFIX 0 C9 1 0.915795 0.413030 -0.072201 11.00000 0.02369 0.02867 = 0.02265 -0.00160 0.00715 -0.00256 C10 1 0.901496 0.396016 -0.196674 11.00000 0.02875 0.03374 = 0.02289 0.00144 0.00410 0.00014 AFIX 43 H10 2 0.830891 0.431010 -0.249473 11.00000 -1.20000 AFIX 0 C11 1 0.992592 0.326785 -0.242229 11.00000 0.03614 0.04060 = 0.02216 -0.00803 0.00536 -0.00101 AFIX 43 H11 2 0.984643 0.316420 -0.325736 11.00000 -1.20000 AFIX 0 C12 1 1.094453 0.273480 -0.164626 11.00000 0.03118 0.03265 = 0.03702 -0.00661 0.00872 0.00133 AFIX 43 H12 2 1.154117 0.226733 -0.195516 11.00000 -1.20000 AFIX 0 C13 1 1.108095 0.289506 -0.040301 11.00000 0.02828 0.03857 = 0.03233 0.00411 0.00392 0.00427 AFIX 43 H13 2 1.176431 0.253272 0.012353 11.00000 -1.20000 AFIX 0 C14 1 1.020078 0.359400 0.005526 11.00000 0.02933 0.04151 = 0.02118 -0.00227 0.00361 0.00067 AFIX 43 H14 2 1.030827 0.370527 0.088894 11.00000 -1.20000 AFIX 0 O5 4 0.485773 0.601230 0.812027 11.00000 0.05873 0.03796 = 0.03051 -0.00069 0.01957 -0.01054 O6 4 0.311403 0.554873 1.085114 11.00000 0.02980 0.02421 = 0.01994 -0.00207 0.00756 0.00002 O7 4 0.186544 0.453622 1.259163 11.00000 0.03977 0.02734 = 0.02727 -0.00182 0.00653 0.00287 O8 4 0.143164 0.576871 1.368157 11.00000 0.03872 0.02998 = 0.02901 -0.00673 0.01777 -0.00545 N2 3 0.346968 0.480238 0.871492 11.00000 0.03619 0.03335 = 0.02265 -0.00371 0.00929 -0.00499 AFIX 93 H2A 2 0.369986 0.449056 0.809807 11.00000 -1.20000 H2B 2 0.288471 0.457223 0.924842 11.00000 -1.20000 AFIX 0 C15 1 0.401637 0.563750 0.884334 11.00000 0.02802 0.03167 = 0.02099 0.00252 0.00289 0.00123 C16 1 0.352345 0.616335 0.993240 11.00000 0.02479 0.02687 = 0.02355 0.00222 0.00375 0.00225 AFIX 13 H16 2 0.250757 0.650581 0.966531 11.00000 -1.20000 AFIX 0 C17 1 0.487359 0.682053 1.040554 11.00000 0.02829 0.02460 = 0.03226 0.00000 0.00735 -0.00123 AFIX 23 H17A 2 0.506828 0.724508 0.976976 11.00000 -1.20000 H17B 2 0.591534 0.650281 1.063463 11.00000 -1.20000 AFIX 0 C18 1 0.433485 0.731790 1.150572 11.00000 0.03702 0.02510 = 0.04139 -0.00787 0.01208 -0.00352 AFIX 23 H18A 2 0.525918 0.768092 1.186836 11.00000 -1.20000 H18B 2 0.340227 0.771239 1.124982 11.00000 -1.20000 AFIX 0 C19 1 0.380898 0.665410 1.244193 11.00000 0.03354 0.02995 = 0.02989 -0.00999 0.00784 -0.00375 AFIX 23 H19A 2 0.478205 0.631949 1.278745 11.00000 -1.20000 H19B 2 0.334796 0.697401 1.309697 11.00000 -1.20000 AFIX 0 C20 1 0.249806 0.601332 1.184276 11.00000 0.02497 0.02608 = 0.02500 -0.00434 0.00657 0.00243 AFIX 13 H20 2 0.151967 0.636611 1.152034 11.00000 -1.20000 AFIX 0 C21 1 0.191708 0.533199 1.272252 11.00000 0.02159 0.03006 = 0.02230 -0.00368 0.00267 0.00253 C22 1 0.060928 0.525469 1.456678 11.00000 0.03291 0.02716 = 0.02763 0.00064 0.01049 0.00034 AFIX 23 H22A 2 0.141389 0.487683 1.504349 11.00000 -1.20000 H22B 2 -0.026628 0.487932 1.416217 11.00000 -1.20000 AFIX 0 C23 1 -0.012662 0.593049 1.536578 11.00000 0.02331 0.02614 = 0.02329 -0.00040 0.00650 -0.00361 C24 1 0.017762 0.588894 1.662381 11.00000 0.02879 0.03609 = 0.02449 0.00384 0.00280 -0.00388 AFIX 43 H24 2 0.085191 0.543629 1.698677 11.00000 -1.20000 AFIX 0 C25 1 -0.052075 0.652044 1.734201 11.00000 0.03977 0.05248 = 0.02126 -0.00666 0.00679 -0.01114 AFIX 43 H25 2 -0.033638 0.647851 1.818606 11.00000 -1.20000 AFIX 0 C26 1 -0.148179 0.720727 1.682127 11.00000 0.03849 0.04037 = 0.04052 -0.01492 0.01663 -0.00574 AFIX 43 H26 2 -0.193560 0.763245 1.730918 11.00000 -1.20000 AFIX 0 C27 1 -0.177046 0.726255 1.556610 11.00000 0.03779 0.03268 = 0.04455 0.00202 0.01222 0.00677 AFIX 43 H27 2 -0.240323 0.773211 1.520679 11.00000 -1.20000 AFIX 0 C28 1 -0.111807 0.661957 1.484565 11.00000 0.03461 0.03492 = 0.02443 0.00324 0.00739 0.00336 AFIX 43 H28 2 -0.134617 0.664914 1.400307 11.00000 -1.20000 AFIX 0 HKLF 4 REM mx8954_a.res in P2(1) REM wR2 = 0.0779, GooF = S = 1.077, Restrained GooF = 1.077 for all data REM R1 = 0.0301 for 6730 Fo > 4sig(Fo) and 0.0335 for all 7224 data REM 343 parameters refined using 1 restraints END WGHT 0.0428 0.0935 REM Highest difference peak 0.199, deepest hole -0.168, 1-sigma level 0.033 Q1 1 0.0216 0.5648 1.4931 11.00000 0.05 0.20 ; _shelx_res_checksum 60827 _shelx_hkl_file ; 0 0 -1 11.45 0.43 0 0 1 9.79 0.42 0 0 -1 11.08 0.37 0 0 -1 11.00 0.36 0 0 -2 10.37 0.48 0 0 -2 10.65 0.44 0 0 -2 9.97 0.45 0 0 -2 9.86 0.56 0 0 -2 9.71 0.59 0 0 -3 18.54 0.72 0 0 -3 19.66 0.92 0 0 -3 19.24 0.78 0 0 -3 18.50 0.73 0 0 -3 17.84 0.92 0 0 4 416.30 9.51 0 0 -4 411.93 9.74 0 0 4 433.28 9.90 0 0 -4 440.72 9.55 0 0 -4 424.95 9.50 0 0 -4 424.36 9.81 0 0 -4 410.00 9.84 0 0 -4 413.28 9.59 0 0 -5 265.18 6.60 0 0 5 281.97 6.97 0 0 -5 286.33 6.56 0 0 -5 264.13 6.83 0 0 -5 272.29 6.79 0 0 -5 274.33 6.93 0 0 5 280.30 7.02 0 0 -5 278.73 6.50 0 0 -6 2.10 0.49 0 0 -6 1.43 0.58 0 0 -6 1.95 0.52 0 0 -6 1.42 0.36 0 0 -6 2.30 0.38 0 0 6 2.28 0.63 0 0 6 0.80 0.56 0 0 -6 2.14 0.59 0 0 -7 67.18 2.52 0 0 -7 67.58 2.35 0 0 -7 68.06 2.13 0 0 -7 68.07 2.21 0 0 7 74.03 2.77 0 0 7 67.88 2.75 0 0 -7 64.94 2.62 0 0 -7 66.42 2.23 0 0 -7 63.79 2.51 0 0 8 11.97 1.24 0 0 -8 12.60 0.86 0 0 -8 11.60 1.15 0 0 -8 11.50 0.87 0 0 -8 11.83 0.96 0 0 -8 13.69 0.87 0 0 -8 12.45 1.11 0 0 -8 11.96 1.12 0 0 8 10.73 1.16 0 0 -9 3.03 0.56 0 0 9 1.62 0.90 0 0 -9 2.31 0.90 0 0 -9 2.35 0.83 0 0 -9 4.12 0.79 0 0 -9 1.87 0.54 0 0 -9 2.67 0.77 0 0 -9 2.26 0.53 0 0 -10 113.79 4.21 0 0 -10 123.68 3.76 0 0 -10 131.77 3.75 0 0 -10 122.02 4.19 0 0 -10 132.41 4.24 0 0 10 122.59 4.49 0 0 -10 128.50 3.90 0 0 -11 297.72 7.53 0 0 -11 324.16 8.34 0 0 -11 299.43 7.66 0 0 11 300.09 8.64 0 0 -11 304.59 8.22 0 0 -11 275.19 8.24 0 0 -11 294.09 7.76 0 0 -12 -0.85 0.96 0 0 -12 0.11 0.79 0 0 -12 0.07 0.55 0 0 -12 -0.26 0.63 0 0 -13 8.45 1.00 0 0 -13 8.86 1.09 0 0 -13 8.53 1.38 0 0 -13 8.21 1.33 0 0 -14 0.10 0.78 0 0 -14 1.34 1.05 0 0 -15 10.13 1.34 0 0 -15 10.85 1.61 0 -1 -1 530.62 11.37 0 1 1 530.92 11.38 0 1 -1 521.48 11.34 0 1 -1 524.95 11.54 0 -1 -1 536.92 11.40 0 1 1 523.83 11.44 0 -1 -1 501.60 11.43 0 -1 -1 530.15 11.48 0 1 1 524.40 11.40 0 1 1 521.32 11.49 0 -1 -2 2002.31 42.14 0 1 -2 1889.12 42.15 0 1 -2 2015.32 41.81 0 -1 -2 1942.90 41.94 0 -1 -2 1958.11 41.97 0 -1 -2 1999.00 42.00 0 1 -2 1953.21 41.92 0 1 -2 1911.95 42.05 0 1 2 1953.13 42.06 0 1 2 1801.79 42.15 0 1 -2 1978.45 41.83 0 -1 -2 1931.67 42.07 0 1 -3 483.21 10.16 0 1 -3 447.22 10.16 0 -1 -3 456.93 10.38 0 1 -3 464.28 10.49 0 -1 -3 470.48 10.30 0 1 -3 468.72 10.23 0 -1 -3 472.26 10.37 0 -1 -3 458.93 10.32 0 1 -3 464.97 10.31 0 1 -3 467.26 10.19 0 1 -3 448.79 10.55 0 -1 -3 469.25 10.56 0 1 3 445.34 10.40 0 -1 -3 434.37 10.46 0 -1 -4 88.06 2.57 0 -1 -4 93.94 2.76 0 1 -4 88.58 2.67 0 1 -4 89.22 2.35 0 -1 -4 86.08 2.44 0 1 -4 90.96 2.33 0 1 -4 89.03 2.40 0 -1 4 84.89 2.75 0 -1 -4 89.43 2.43 0 1 4 87.58 2.62 0 1 -4 83.22 2.68 0 1 4 87.29 2.44 0 -1 -4 86.78 2.63 0 -1 -4 84.83 2.50 0 1 -4 93.72 2.32 0 1 5 349.55 8.50 0 -1 -5 352.09 8.22 0 -1 -5 346.02 8.28 0 -1 -5 347.45 8.40 0 1 -5 351.17 8.17 0 1 -5 357.34 8.09 0 1 5 361.69 8.21 0 1 -5 365.19 8.04 0 1 -5 336.64 8.05 0 -1 -5 349.81 8.48 0 -1 5 355.88 8.73 0 1 -5 354.62 8.54 0 1 -5 337.60 8.52 0 -1 -5 349.10 8.59 0 -1 -5 346.06 8.17 0 -1 6 421.98 10.31 0 1 -6 419.09 9.60 0 1 -6 443.80 9.57 0 -1 -6 429.26 10.20 0 1 6 411.52 9.69 0 -1 -6 406.97 10.04 0 -1 -6 417.58 9.73 0 1 -6 411.58 9.55 0 -1 -6 411.54 9.96 0 1 6 402.87 10.26 0 -1 -6 416.26 9.68 0 1 -6 399.89 10.09 0 -1 -6 414.27 9.83 0 1 -6 411.65 9.92 0 1 -6 394.17 10.07 0 1 -6 418.69 9.71 0 1 6 414.91 10.09 0 -1 -7 53.54 2.23 0 -1 -7 52.56 1.91 0 1 -7 53.08 1.95 0 -1 7 53.98 2.42 0 1 -7 54.46 1.83 0 1 -7 51.86 2.02 0 1 7 54.02 2.26 0 1 7 52.94 2.40 0 1 -7 50.83 1.84 0 1 -7 52.83 2.25 0 -1 -7 50.97 2.28 0 -1 -7 50.46 2.01 0 1 -7 49.03 2.21 0 1 -7 56.99 1.86 0 -1 -7 53.81 1.97 0 1 -7 52.68 2.12 0 -1 -7 55.41 2.20 0 -1 -8 20.81 1.20 0 1 -8 21.18 1.36 0 1 -8 21.40 1.10 0 -1 -8 19.54 1.48 0 1 -8 17.72 1.37 0 1 8 22.64 1.64 0 -1 -8 20.66 1.37 0 1 -8 18.79 1.16 0 1 8 19.26 1.43 0 1 -8 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0.78 0 2 -2 19.13 1.00 0 2 -2 19.39 0.57 0 2 2 20.29 0.91 0 -2 2 19.13 0.56 0 -2 -2 20.46 0.75 0 -2 -2 19.92 0.80 0 2 -2 20.56 0.56 0 2 2 19.55 0.79 0 -2 -2 18.75 0.85 0 -2 -2 18.59 0.72 0 -2 -3 138.57 3.54 0 -2 -3 141.49 3.55 0 2 3 146.73 3.74 0 -2 -3 144.53 3.82 0 2 -3 140.11 3.30 0 2 -3 146.56 3.34 0 2 -3 142.41 3.50 0 -2 3 147.31 3.32 0 2 3 149.81 3.64 0 -2 -3 144.23 3.77 0 -2 -3 139.46 3.61 0 2 -3 138.50 3.88 0 -2 -4 245.83 6.13 0 2 -4 247.90 5.64 0 -2 -4 245.07 5.91 0 -2 -4 250.06 5.96 0 2 4 250.40 6.01 0 2 -4 250.04 5.72 0 -2 -4 250.93 5.88 0 -2 -4 243.18 5.90 0 2 -4 245.42 6.09 0 2 -4 234.53 6.25 0 2 -4 236.06 5.62 0 -2 4 243.04 6.33 0 2 -4 244.64 5.83 0 -2 -4 251.51 6.21 0 2 -4 247.31 5.59 0 2 -5 60.10 1.73 0 2 5 61.25 1.98 0 2 -5 61.35 2.21 0 2 5 59.00 2.12 0 2 -5 59.90 1.95 0 2 -5 55.60 2.26 0 -2 -5 59.09 1.97 0 2 -5 60.93 1.87 0 -2 -5 60.74 2.20 0 -2 -5 62.49 2.28 0 -2 -5 61.21 2.05 0 -2 5 57.46 2.35 0 -2 -5 63.41 1.97 0 -2 -5 62.21 2.07 0 2 -5 59.67 1.77 0 2 -5 62.47 1.79 0 -2 6 581.86 13.78 0 -2 -6 564.49 13.53 0 2 -6 572.98 12.81 0 2 -6 535.50 13.48 0 2 -6 569.79 12.94 0 2 6 580.11 13.09 0 2 -6 591.75 12.79 0 2 6 552.75 13.31 0 -2 -6 585.79 13.49 0 2 -6 557.24 13.40 0 -2 -6 579.15 13.21 0 2 -6 560.73 13.07 0 -2 -6 573.30 13.11 0 2 -6 577.43 12.84 0 -2 -6 588.71 13.21 0 2 6 528.86 13.60 0 -2 -6 565.11 13.05 0 2 -7 51.72 2.35 0 2 -7 55.81 1.86 0 2 -7 56.38 1.85 0 2 -7 59.28 1.85 0 2 7 55.85 2.05 0 -2 -7 55.01 2.33 0 2 7 50.21 2.41 0 2 7 56.47 2.30 0 -2 -7 55.54 2.15 0 2 -7 54.64 2.32 0 -2 -7 53.98 2.01 0 -2 -7 54.05 2.03 0 -2 -7 58.87 2.43 0 2 -7 56.01 2.07 0 -2 -7 58.12 2.20 0 2 -7 54.37 1.96 0 -2 7 49.08 2.42 0 2 8 14.87 1.25 0 2 -8 14.57 1.01 0 -2 -8 15.61 1.07 0 2 -8 14.63 0.90 0 -2 -8 15.93 1.16 0 2 -8 12.46 1.30 0 -2 8 16.33 1.47 0 -2 -8 15.53 1.05 0 2 -8 15.80 1.31 0 -2 -8 16.07 1.29 0 2 8 14.01 1.36 0 2 -8 16.32 0.93 0 -2 -8 13.13 1.27 0 2 -8 14.55 0.89 0 -2 -8 15.82 1.16 0 2 -8 14.64 1.13 0 2 -8 14.49 1.06 0 2 -9 15.41 1.25 0 2 -9 18.85 1.05 0 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12.44 1.02 0 -3 -7 13.25 0.92 0 -3 -7 13.57 1.23 0 3 7 12.96 1.27 0 3 7 10.15 1.00 0 3 -7 13.06 0.86 0 -3 -7 14.67 1.02 0 3 -7 13.35 0.76 0 -3 -7 14.65 1.04 0 3 -7 12.85 1.24 0 -3 -7 13.87 1.18 0 3 -7 12.17 1.09 0 3 -8 160.47 3.98 0 3 8 152.45 4.37 0 -3 -8 145.10 4.32 0 -3 -8 145.33 4.44 0 -3 -8 158.13 4.45 0 3 8 156.21 4.65 0 3 8 142.23 4.97 0 -3 -8 154.16 4.84 0 3 -8 151.38 4.02 0 3 -8 154.01 4.20 0 3 -8 152.59 4.71 0 3 -8 157.41 4.07 0 3 -8 142.43 4.83 0 3 -8 145.03 4.30 0 -3 -8 149.63 4.39 0 -3 -8 145.46 4.78 0 3 -9 64.37 2.59 0 3 -9 65.16 2.38 0 3 -9 65.16 2.51 0 -3 -9 68.79 2.60 0 -3 -9 70.71 3.00 0 3 9 61.25 3.07 0 3 -9 63.19 2.80 0 -3 -9 71.42 2.64 0 3 -9 70.56 2.27 0 3 -9 63.64 2.92 0 -3 -9 67.01 2.52 0 3 -9 69.38 2.21 0 3 9 68.14 2.54 0 3 9 77.84 2.95 0 3 -9 66.12 2.28 0 -3 -10 109.89 4.15 0 3 -10 123.05 3.32 0 3 -10 113.26 3.53 0 3 -10 112.22 3.38 0 3 -10 111.01 3.69 0 3 -10 108.12 3.66 0 3 -10 106.89 3.76 0 3 -10 111.98 3.30 0 3 -10 103.67 4.05 0 -3 -10 105.94 3.67 0 3 10 110.76 4.47 0 -3 -10 111.78 3.66 0 -3 -10 112.46 3.70 0 3 10 106.45 3.97 0 -3 -11 44.72 2.16 0 -3 -11 42.16 2.02 0 3 -11 41.85 2.06 0 3 -11 40.39 1.75 0 -3 -11 43.35 2.11 0 3 -11 42.60 1.88 0 3 -11 50.18 1.86 0 -3 -11 39.51 2.44 0 3 11 45.10 2.81 0 3 11 41.87 2.34 0 3 -11 45.18 2.17 0 3 -11 38.87 2.12 0 3 -12 3.71 0.67 0 3 -12 4.92 0.92 0 -3 -12 3.40 1.09 0 3 12 2.19 1.04 0 3 -12 5.56 1.06 0 -3 -12 3.63 0.89 0 3 -12 4.73 0.97 0 -3 -12 4.90 0.88 0 3 12 4.42 1.36 0 3 -12 5.20 0.81 0 3 -13 40.49 1.91 0 3 13 38.82 2.42 0 3 -13 38.94 2.21 0 -3 -13 37.84 2.12 0 3 -13 30.43 2.10 0 3 -13 33.28 1.92 0 -3 -13 38.58 2.00 0 -3 -14 13.67 1.72 0 -3 -14 12.45 1.29 0 -3 -14 12.37 1.44 0 3 -14 8.51 1.36 0 3 -14 10.27 1.20 0 3 -14 13.98 1.52 0 3 -14 13.95 1.25 0 3 -15 15.46 1.67 0 -4 0 63.56 1.65 0 4 0 63.98 1.64 0 -4 0 64.35 1.86 0 4 0 64.30 1.78 0 4 0 62.73 1.89 0 4 0 65.33 1.71 0 4 -1 3.83 0.43 0 4 1 3.58 0.47 0 -4 1 3.02 0.19 0 4 1 3.72 0.51 0 4 1 3.65 0.36 0 -4 1 2.97 0.27 0 4 -1 3.12 0.40 0 -4 -1 3.32 0.41 0 4 1 3.83 0.37 0 -4 1 3.54 0.31 0 4 -1 3.60 0.22 0 4 -1 3.20 0.33 0 -4 1 3.38 0.45 0 4 -1 3.59 0.27 0 -4 -2 52.34 1.62 0 -4 2 54.75 1.36 0 4 2 56.30 1.80 0 4 -2 56.02 1.63 0 4 2 52.75 1.65 0 4 -2 53.02 1.73 0 -4 -2 52.69 1.61 0 -4 2 53.93 1.58 0 4 2 52.28 1.86 0 4 2 47.01 1.63 0 4 -2 54.01 1.36 0 -4 -2 52.41 1.81 0 4 2 56.49 1.66 0 -4 2 48.44 1.69 0 4 -2 53.91 1.44 0 4 -3 185.69 4.11 0 -4 -3 188.24 4.59 0 -4 3 188.21 4.21 0 4 3 186.09 4.94 0 4 3 181.50 4.64 0 4 -3 186.21 4.17 0 4 3 187.94 4.60 0 4 3 183.23 4.59 0 -4 -3 188.53 4.87 0 -4 -3 183.11 4.52 0 4 -3 182.12 4.51 0 4 3 190.80 4.81 0 -4 3 175.84 4.48 0 -4 -3 177.13 4.78 0 4 -3 197.88 5.19 0 4 -3 172.58 4.65 0 4 -4 407.56 9.76 0 4 4 405.87 10.12 0 -4 -4 428.29 10.04 0 4 4 405.48 9.89 0 -4 4 417.31 9.53 0 4 4 424.31 9.72 0 4 -4 427.87 10.32 0 -4 4 423.93 9.23 0 -4 -4 414.62 9.96 0 4 -4 425.86 9.26 0 4 -4 416.29 9.17 0 4 -4 420.31 9.18 0 4 -4 412.57 9.56 0 -4 -4 397.76 9.65 0 -4 -4 410.54 9.58 0 -4 -4 406.37 9.74 0 -4 -4 430.77 9.69 0 -4 -5 52.20 2.10 0 4 5 47.60 1.84 0 -4 -5 45.94 1.74 0 4 -5 47.62 1.68 0 4 -5 46.57 1.36 0 -4 -5 47.11 1.78 0 -4 -5 48.89 2.00 0 -4 -5 48.74 1.86 0 4 -5 47.31 1.84 0 4 -5 45.62 2.20 0 4 -5 49.53 1.40 0 -4 -5 47.25 1.70 0 4 -5 51.34 1.52 0 -4 -6 91.78 2.95 0 -4 -6 91.95 2.84 0 4 6 89.94 2.84 0 4 -6 90.09 3.34 0 -4 -6 89.75 2.88 0 4 -6 96.38 2.44 0 4 -6 86.47 2.99 0 -4 -6 88.94 3.15 0 4 6 88.67 2.92 0 4 -6 90.41 2.55 0 4 -6 89.34 2.92 0 4 -6 86.02 2.71 0 -4 -6 86.06 3.14 0 -4 -6 91.28 2.78 0 4 -6 90.38 2.36 0 4 -6 87.28 2.43 0 -4 -7 71.20 2.45 0 4 7 65.14 2.89 0 4 7 71.76 2.51 0 -4 -7 68.39 2.77 0 -4 -7 64.72 2.74 0 4 -7 69.79 1.98 0 -4 -7 65.83 2.50 0 4 -7 63.45 2.87 0 -4 -7 69.48 2.48 0 4 -7 71.07 2.09 0 4 -7 68.18 2.51 0 4 -7 69.85 2.07 0 4 7 73.02 2.61 0 4 -7 65.01 2.32 0 4 -7 71.85 2.22 0 -4 -7 70.06 2.40 0 4 -7 68.75 2.64 0 -4 -8 15.46 1.13 0 4 -8 17.19 0.84 0 4 8 14.90 1.12 0 4 8 17.22 1.31 0 -4 -8 17.42 1.15 0 -4 -8 17.76 1.46 0 -4 -8 15.14 1.12 0 4 -8 15.43 1.28 0 4 8 17.65 1.54 0 -4 -8 16.28 1.42 0 4 -8 17.67 1.03 0 4 -8 15.61 1.08 0 4 -8 17.17 1.22 0 4 -8 14.95 0.87 0 4 -8 17.50 0.90 0 4 -8 13.03 1.45 0 4 -9 65.88 2.02 0 -4 -9 61.26 2.86 0 -4 -9 58.17 2.41 0 -4 -9 62.58 2.52 0 4 -9 59.94 2.43 0 4 -9 63.10 2.13 0 4 9 60.07 3.06 0 4 -9 59.84 2.65 0 4 9 60.38 2.64 0 4 -9 68.23 2.14 0 4 -9 69.10 2.63 0 4 -9 63.70 2.97 0 4 -9 60.64 2.41 0 4 -9 66.73 2.31 0 -4 -9 64.92 2.46 0 4 -10 108.72 3.71 0 -4 -10 116.92 3.74 0 4 10 115.02 4.62 0 -4 -10 115.44 3.78 0 4 -10 116.67 3.42 0 -4 -10 116.08 4.33 0 4 10 115.04 4.05 0 4 -10 118.10 3.35 0 4 -10 120.67 3.27 0 4 -10 119.66 3.92 0 -4 -10 112.88 3.85 0 4 -10 117.52 3.58 0 4 -10 108.35 3.78 0 4 -11 51.27 2.38 0 4 11 50.68 3.02 0 -4 -11 49.37 2.72 0 -4 -11 50.45 2.27 0 4 -11 50.14 1.91 0 4 -11 53.83 2.05 0 4 11 47.63 2.51 0 -4 -11 50.58 2.36 0 4 -11 47.23 2.27 0 4 -11 48.41 2.29 0 4 -12 10.07 1.18 0 4 12 14.75 1.92 0 4 -12 11.72 0.92 0 4 -12 11.82 1.21 0 4 -12 13.27 1.04 0 -4 -12 12.77 1.26 0 -4 -12 9.47 1.47 0 4 -12 11.35 1.25 0 4 12 13.26 1.47 0 -4 -12 12.29 1.17 0 4 -13 0.33 0.79 0 4 13 0.38 1.33 0 -4 -13 0.10 0.67 0 4 -13 0.11 0.82 0 4 -13 0.49 0.76 0 4 -13 -0.08 0.61 0 4 13 0.25 0.89 0 -4 -13 0.33 0.82 0 -4 -14 3.24 1.01 0 -4 -14 2.82 0.90 0 4 -14 2.51 0.87 0 4 -14 2.99 1.04 0 4 -14 1.67 0.92 0 -4 -15 17.87 1.54 0 4 -15 18.84 1.85 0 -5 0 0.04 0.23 0 -5 0 0.14 0.35 0 5 0 -0.34 0.26 0 5 0 -0.04 0.32 0 5 0 0.05 0.23 0 -5 0 0.03 0.26 0 5 0 0.04 0.21 0 5 1 149.77 3.61 0 -5 1 135.10 3.67 0 5 -1 145.97 3.33 0 5 1 142.65 3.75 0 -5 -1 142.40 3.60 0 5 -1 144.64 3.55 0 5 1 148.38 3.92 0 5 -1 143.27 3.83 0 5 1 149.50 3.66 0 -5 1 144.28 3.45 0 5 -1 148.11 3.47 0 -5 -1 143.35 3.70 0 -5 1 148.26 3.80 0 -5 1 154.61 3.53 0 -5 1 149.08 3.33 0 5 -1 143.26 3.74 0 -5 2 515.88 11.53 0 5 2 510.61 11.39 0 5 2 508.37 11.44 0 5 -2 512.25 11.03 0 -5 -2 490.33 11.33 0 -5 2 507.65 11.02 0 -5 -2 504.80 11.37 0 -5 -2 471.90 11.37 0 5 2 499.28 11.55 0 5 -2 499.12 11.55 0 -5 -2 512.29 11.64 0 5 2 495.75 11.38 0 5 -2 495.70 11.38 0 5 2 493.90 11.71 0 5 -2 495.60 11.13 0 -5 2 517.05 11.32 0 -5 2 516.29 11.08 0 -5 -3 15.12 0.84 0 5 3 17.15 0.95 0 5 -3 16.52 0.51 0 5 -3 16.39 0.95 0 -5 -3 16.41 0.85 0 5 -3 17.23 1.31 0 -5 3 16.02 0.81 0 5 3 17.81 1.06 0 5 -3 17.63 0.60 0 5 -3 16.69 0.70 0 5 3 15.66 0.87 0 5 3 15.49 1.07 0 5 3 18.50 0.93 0 -5 3 17.26 0.62 0 5 -3 18.90 0.89 0 -5 -3 16.25 1.08 0 5 -4 58.66 1.54 0 -5 4 60.44 1.88 0 5 -4 59.02 1.50 0 -5 -4 59.16 2.00 0 5 4 61.35 2.21 0 5 -4 62.02 2.57 0 -5 -4 57.08 1.90 0 5 4 62.95 2.04 0 5 -4 60.66 1.94 0 -5 4 58.28 1.58 0 5 4 58.40 2.33 0 5 4 57.65 2.00 0 5 -4 60.18 2.13 0 -5 -4 62.95 2.31 0 -5 -4 56.05 2.17 0 -5 -5 16.78 1.01 0 5 5 16.97 1.18 0 5 -5 17.60 0.66 0 5 -5 17.91 1.42 0 5 -5 19.82 0.77 0 5 -5 17.57 0.66 0 -5 5 16.93 0.70 0 -5 -5 17.11 1.08 0 -5 -5 17.30 1.22 0 -5 -5 17.44 0.97 0 5 5 15.65 1.01 0 -5 -5 16.41 1.17 0 5 -5 17.52 0.95 0 5 -5 16.96 1.10 0 -5 -5 18.06 1.04 0 -5 5 18.12 0.94 0 -5 -6 57.20 2.12 0 -5 -6 56.41 2.01 0 -5 -6 56.22 2.20 0 5 -6 56.67 1.76 0 5 6 59.53 2.15 0 -5 -6 60.85 2.48 0 5 6 55.42 2.18 0 5 -6 56.50 2.21 0 5 -6 58.03 1.65 0 5 -6 56.12 2.02 0 5 -6 57.89 1.61 0 5 -6 61.71 2.72 0 -5 -6 55.20 2.13 0 -5 -6 57.91 2.43 0 5 7 61.02 2.29 0 -5 -7 57.79 2.57 0 5 -7 59.60 2.76 0 5 -7 59.87 1.91 0 5 -7 61.84 1.80 0 5 -7 58.96 2.41 0 -5 -7 59.09 2.29 0 -5 -7 58.50 2.33 0 5 -7 58.69 1.70 0 -5 -7 58.56 2.13 0 5 -7 57.02 1.81 0 -5 -7 57.47 2.54 0 -5 -7 56.63 2.20 0 5 -7 61.37 2.38 0 5 -7 54.50 2.09 0 5 7 56.27 2.31 0 5 8 74.58 2.70 0 5 -8 70.49 3.16 0 5 -8 68.55 2.77 0 5 -8 67.20 2.49 0 5 8 70.57 3.22 0 5 -8 74.22 2.19 0 5 -8 69.80 2.16 0 -5 -8 73.55 2.65 0 -5 -8 74.18 3.05 0 5 -8 73.00 2.32 0 5 -8 72.28 2.05 0 -5 -8 70.99 2.50 0 -5 -8 71.54 2.68 0 5 -8 69.43 2.72 0 5 8 70.89 2.74 0 5 -9 17.91 0.94 0 5 -9 17.51 0.96 0 5 -9 20.94 1.13 0 -5 -9 18.14 1.60 0 -5 -9 18.31 1.29 0 -5 -9 18.89 1.24 0 5 -9 16.07 1.18 0 5 9 16.55 1.36 0 5 9 16.75 1.72 0 5 -9 16.75 1.39 0 5 -9 17.03 0.84 0 -5 -9 15.71 1.27 0 5 -9 19.65 1.40 0 -5 -10 125.54 3.86 0 5 10 124.51 4.22 0 -5 -10 130.40 4.13 0 -5 -10 120.24 3.96 0 5 -10 122.03 3.26 0 5 -10 118.82 3.88 0 -5 -10 118.88 4.51 0 5 10 124.94 4.86 0 5 -10 124.56 3.65 0 5 -10 114.51 3.89 0 5 -10 116.60 4.05 0 5 -10 125.44 3.50 0 5 -10 117.88 3.39 0 5 -11 36.42 1.61 0 5 -11 39.62 1.77 0 -5 -11 35.17 1.98 0 5 -11 37.64 1.53 0 5 -11 34.65 2.01 0 5 11 41.38 2.23 0 -5 -11 35.41 1.96 0 5 -11 36.47 1.94 0 5 11 35.69 2.63 0 5 -11 33.18 1.90 0 -5 -11 38.22 2.40 0 5 -12 6.99 1.09 0 5 12 10.46 1.79 0 -5 -12 6.73 1.38 0 5 -12 9.30 1.11 0 5 -12 6.73 1.02 0 5 12 7.07 1.22 0 5 -12 10.46 0.91 0 -5 -12 7.65 1.10 0 -5 -12 8.71 1.09 0 -5 -13 10.16 1.17 0 5 -13 8.93 1.24 0 5 13 7.95 1.88 0 5 -13 7.96 1.20 0 5 13 9.88 1.36 0 5 -13 8.61 1.24 0 -5 -13 8.14 1.22 0 5 -13 9.82 0.96 0 5 14 24.70 2.60 0 -5 -14 23.39 1.74 0 -5 -14 28.57 1.97 0 5 -14 30.53 2.06 0 5 -14 25.33 1.81 0 -5 -15 32.23 2.06 0 6 0 886.13 20.13 0 6 0 932.45 19.79 0 -6 0 917.44 19.68 0 6 0 893.09 19.89 0 -6 0 917.12 20.03 0 -6 0 866.55 19.74 0 -6 0 914.67 19.88 0 6 0 900.62 19.66 0 6 1 85.70 2.63 0 -6 1 92.80 2.19 0 -6 1 92.25 2.32 0 -6 1 89.08 2.38 0 -6 1 90.91 2.67 0 -6 -1 84.44 2.55 0 6 1 89.05 2.81 0 -6 -1 90.79 2.46 0 -6 1 87.36 2.56 0 6 -1 87.01 2.63 0 6 1 88.68 2.62 0 6 1 90.15 2.46 0 6 -1 89.41 2.44 0 6 -1 90.65 2.19 0 6 1 95.67 2.53 0 -6 -1 87.85 2.61 0 6 -1 89.48 2.34 0 6 -2 61.56 2.15 0 -6 2 63.93 1.67 0 -6 -2 62.87 1.98 0 -6 -2 60.20 1.94 0 6 -2 60.33 1.66 0 -6 2 58.80 1.91 0 6 -2 61.52 1.48 0 6 -2 61.77 2.00 0 -6 2 63.75 1.71 0 6 2 60.97 2.02 0 6 2 64.32 1.97 0 6 2 63.21 1.97 0 6 2 65.26 2.29 0 6 2 61.19 2.11 0 -6 2 62.87 2.10 0 6 -2 60.82 1.77 0 6 3 0.80 0.40 0 6 -3 0.76 0.28 0 6 3 1.97 0.64 0 -6 3 0.55 0.20 0 -6 3 0.41 0.38 0 -6 -3 1.47 0.62 0 -6 -3 0.76 0.42 0 6 3 1.42 0.56 0 6 -3 0.51 0.47 0 -6 -3 1.18 0.44 0 6 3 1.50 0.43 0 -6 -3 0.87 0.36 0 6 -3 1.00 0.21 0 6 -3 0.81 0.39 0 -6 -4 945.57 21.82 0 6 -4 998.93 21.14 0 6 -4 959.82 22.05 0 -6 -4 980.44 22.23 0 -6 4 999.62 21.68 0 -6 -4 985.56 21.74 0 6 -4 982.15 21.22 0 6 4 977.65 22.16 0 6 -4 975.05 21.42 0 6 -4 983.17 21.77 0 6 4 940.59 22.38 0 6 4 987.35 21.90 0 6 4 999.29 21.89 0 6 -4 973.57 21.10 0 6 -4 1019.32 22.83 0 -6 4 983.26 21.28 0 6 -5 73.74 2.09 0 -6 5 71.92 1.93 0 6 -5 69.25 2.57 0 -6 -5 76.66 2.36 0 -6 -5 72.19 2.43 0 6 -5 72.82 1.90 0 6 -5 68.86 3.03 0 6 5 70.01 2.46 0 -6 5 68.81 2.25 0 6 -5 68.05 2.31 0 6 5 75.35 2.92 0 -6 -5 76.22 2.78 0 6 -5 74.09 1.84 0 6 -5 72.77 1.88 0 6 5 70.37 2.66 0 6 -6 98.98 2.61 0 6 -6 98.83 2.50 0 6 -6 99.37 3.31 0 -6 -6 100.67 3.50 0 6 -6 98.76 3.83 0 -6 6 101.12 2.56 0 -6 -6 93.70 3.15 0 6 6 97.26 3.19 0 -6 -6 102.76 3.53 0 6 -6 97.72 3.02 0 6 -6 100.02 2.51 0 -6 -6 101.99 3.16 0 -6 -6 99.11 2.99 0 -6 6 98.26 2.95 0 6 -7 180.24 5.52 0 6 -7 201.81 5.66 0 -6 -7 196.52 5.24 0 -6 -7 203.92 5.59 0 -6 -7 195.18 5.49 0 6 -7 208.50 6.31 0 6 -7 201.81 4.90 0 6 -7 201.93 4.69 0 -6 -7 191.69 5.84 0 6 -7 189.08 5.27 0 6 -7 193.32 4.82 0 6 -7 201.31 4.76 0 -6 -7 205.78 5.50 0 -6 -7 203.01 5.91 0 6 7 199.90 5.56 0 6 7 203.87 5.52 0 6 -8 123.01 4.09 0 6 8 122.82 4.04 0 -6 -8 135.63 3.80 0 -6 -8 122.83 4.00 0 6 -8 124.77 4.12 0 6 -8 126.95 3.36 0 -6 -8 127.05 4.44 0 6 -8 116.26 3.76 0 6 -8 130.18 3.34 0 6 -8 129.13 3.47 0 6 -8 130.06 4.71 0 6 -8 128.74 3.20 0 -6 -8 125.62 3.95 0 6 -9 106.33 2.90 0 6 -9 97.16 3.62 0 6 -9 105.02 3.05 0 6 -9 104.76 3.70 0 -6 -9 105.53 4.04 0 -6 -9 100.96 3.55 0 6 -9 101.20 3.38 0 -6 -9 107.35 3.32 0 6 9 103.39 4.26 0 6 -9 101.37 2.72 0 6 9 100.73 3.61 0 6 -9 105.38 2.93 0 -6 -9 94.79 3.43 0 6 -10 66.76 2.14 0 -6 -10 62.98 3.14 0 -6 -10 66.48 2.51 0 -6 -10 67.04 2.79 0 6 -10 68.70 2.35 0 6 10 69.81 3.50 0 6 -10 65.57 2.86 0 -6 -10 66.09 2.73 0 6 10 70.17 2.90 0 6 -10 59.75 2.53 0 6 -10 71.42 2.70 0 6 -10 64.99 1.98 0 6 -10 70.87 2.25 0 6 -11 67.22 2.78 0 6 -11 68.26 2.99 0 6 -11 77.10 2.46 0 -6 -11 67.55 2.85 0 6 -11 64.80 2.74 0 6 11 74.85 3.10 0 -6 -11 69.70 2.96 0 -6 -11 72.36 3.42 0 6 11 68.06 3.65 0 6 -11 74.59 2.30 0 -6 -12 4.85 0.96 0 -6 -12 6.20 0.99 0 6 12 6.54 1.14 0 6 12 8.19 1.62 0 6 -12 5.58 0.74 0 6 -12 3.44 0.88 0 6 -12 5.58 1.01 0 6 -12 4.38 1.07 0 6 13 6.57 1.68 0 6 -13 6.74 1.14 0 -6 -13 7.13 1.16 0 -6 -13 6.80 1.19 0 6 -13 6.48 1.20 0 -6 -14 15.25 1.48 0 6 -14 14.25 1.53 0 -7 0 0.21 0.27 0 7 0 -0.15 0.23 0 7 0 0.33 0.41 0 7 0 -0.08 0.37 0 -7 0 -0.03 0.23 0 -7 0 0.33 0.41 0 7 0 0.19 0.29 0 -7 0 0.11 0.34 0 -7 0 -0.14 0.41 0 -7 1 6.81 0.47 0 -7 -1 6.38 0.52 0 7 1 6.31 0.57 0 -7 1 6.38 0.39 0 7 -1 6.05 0.37 0 7 -1 5.31 0.46 0 -7 -1 5.98 0.64 0 -7 1 6.27 0.64 0 -7 -1 7.40 0.67 0 -7 -1 6.19 0.56 0 7 -1 5.78 0.53 0 7 1 6.72 0.54 0 7 1 7.21 0.68 0 -7 1 5.87 0.66 0 7 1 7.06 0.67 0 -7 1 6.31 0.50 0 7 -1 6.61 0.68 0 7 1 7.26 0.79 0 7 2 25.32 1.17 0 7 2 26.93 1.44 0 -7 2 26.16 0.69 0 7 2 26.68 1.27 0 -7 2 26.50 1.17 0 7 2 26.94 1.17 0 7 -2 26.47 0.95 0 7 -2 25.90 1.04 0 7 -2 24.58 1.30 0 -7 -2 27.85 1.31 0 7 -2 24.61 0.74 0 -7 2 27.33 0.98 0 7 2 25.44 1.29 0 -7 2 26.32 0.93 0 -7 2 29.43 1.35 0 -7 -2 25.81 1.19 0 -7 -2 25.32 1.16 0 7 -2 28.08 1.28 0 7 3 46.48 2.06 0 7 -3 41.02 1.81 0 7 3 44.41 1.69 0 7 -3 44.12 1.31 0 -7 -3 43.12 1.63 0 7 -3 43.81 1.44 0 -7 -3 46.11 1.71 0 7 3 45.04 1.87 0 -7 3 42.69 1.59 0 -7 -3 45.50 1.86 0 -7 3 43.77 1.30 0 7 3 44.61 1.75 0 7 -3 43.36 1.68 0 -7 4 37.02 1.46 0 7 -4 35.47 1.52 0 7 -4 39.03 1.30 0 7 4 35.31 1.72 0 7 -4 34.41 0.93 0 7 -4 33.88 1.67 0 7 -4 38.62 0.94 0 7 4 39.70 1.64 0 7 4 37.98 1.60 0 -7 -4 37.89 1.52 0 7 -4 35.40 1.11 0 -7 -4 37.26 1.62 0 -7 -4 39.30 1.86 0 7 -4 40.07 2.23 0 -7 -4 37.13 1.55 0 7 4 37.62 1.96 0 -7 4 38.53 1.16 0 -7 -4 35.79 1.54 0 -7 5 300.26 7.30 0 -7 5 299.69 6.86 0 7 -5 319.31 8.58 0 7 -5 305.37 7.05 0 7 -5 307.60 6.72 0 -7 -5 314.68 7.98 0 7 -5 296.43 6.80 0 7 5 299.96 7.58 0 7 -5 294.63 7.42 0 -7 -5 279.70 7.57 0 7 5 306.50 7.86 0 -7 -5 298.98 7.55 0 7 -5 305.90 6.68 0 7 5 301.55 7.58 0 -7 -5 297.04 7.36 0 7 5 304.46 8.21 0 7 -5 300.92 7.78 0 -7 -6 87.11 2.76 0 7 -6 90.00 2.21 0 -7 6 87.59 2.31 0 -7 -6 82.95 2.88 0 7 -6 89.35 2.28 0 7 6 79.39 3.39 0 7 -6 83.39 2.47 0 7 6 91.47 3.25 0 7 -6 84.61 2.23 0 7 -6 91.01 3.72 0 -7 6 92.59 2.77 0 -7 -6 86.38 3.26 0 7 6 86.18 2.97 0 7 -6 84.79 2.81 0 7 -6 89.58 3.14 0 -7 -7 187.11 5.07 0 7 -7 202.92 6.31 0 7 -7 191.74 4.61 0 7 -7 185.44 5.54 0 7 7 184.28 5.36 0 7 -7 190.94 4.51 0 7 -7 190.34 4.47 0 -7 -7 189.71 5.77 0 7 -7 182.41 5.15 0 -7 -7 189.34 5.32 0 7 -8 81.45 2.25 0 7 -8 80.76 2.16 0 -7 -8 90.29 3.50 0 7 -8 78.81 2.34 0 -7 -8 81.68 2.71 0 7 -8 79.16 2.30 0 7 -8 80.39 2.83 0 7 8 78.74 2.98 0 -7 -8 77.79 2.96 0 7 -8 77.04 3.11 0 7 -8 70.66 2.93 0 -7 -8 80.36 2.95 0 -7 -9 20.69 1.72 0 -7 -9 22.99 1.33 0 7 -9 19.98 0.96 0 7 -9 18.26 1.30 0 7 9 21.69 1.54 0 -7 -9 18.91 1.42 0 7 -9 20.36 0.85 0 7 -9 22.45 1.01 0 7 9 27.92 2.16 0 -7 -9 19.16 1.40 0 7 -9 20.70 1.51 0 7 -9 20.12 1.08 0 7 -9 20.55 1.54 0 7 -10 127.96 4.43 0 7 10 116.90 4.96 0 -7 -10 127.18 4.77 0 -7 -10 131.56 4.26 0 -7 -10 127.48 3.88 0 7 -10 132.24 3.51 0 7 10 124.14 4.28 0 7 -10 127.37 3.41 0 -7 -10 126.20 4.28 0 7 -10 122.58 4.04 0 -7 -11 3.30 0.90 0 7 -11 2.82 0.91 0 7 -11 3.02 0.55 0 7 11 2.08 0.87 0 7 11 3.22 1.40 0 7 -11 2.68 0.81 0 -7 -11 1.75 1.12 0 7 -11 1.72 0.76 0 -7 -11 2.66 0.83 0 7 -12 0.79 0.81 0 7 -12 1.66 0.81 0 -7 -12 1.71 0.86 0 -7 -12 -0.42 0.83 0 7 12 1.63 0.88 0 7 12 1.72 1.28 0 7 -12 1.75 0.93 0 7 -13 4.20 1.07 0 7 -13 2.85 0.97 0 7 13 4.30 1.63 0 -7 -13 4.23 1.07 0 -7 -13 4.67 1.01 0 -7 -14 8.35 1.25 0 7 -14 8.10 1.30 0 -8 0 501.25 11.71 0 -8 0 510.87 11.51 0 8 0 502.49 11.24 0 -8 0 507.28 11.73 0 -8 0 505.97 11.38 0 8 0 495.06 11.88 0 8 0 502.94 11.42 0 -8 0 496.58 11.25 0 8 0 498.27 11.56 0 8 -1 66.53 1.79 0 8 1 70.26 2.16 0 -8 -1 64.04 2.22 0 -8 -1 64.50 2.06 0 -8 1 67.66 1.95 0 8 1 60.83 2.28 0 -8 1 66.71 2.31 0 8 1 67.45 2.27 0 -8 -1 66.14 2.24 0 -8 -1 64.13 2.33 0 8 -1 67.36 1.99 0 -8 1 64.79 2.23 0 -8 1 68.40 2.03 0 -8 1 64.64 1.78 0 -8 -1 68.17 2.06 0 8 -1 67.37 2.37 0 8 -1 69.09 2.12 0 8 1 67.38 2.48 0 8 1 64.66 2.02 0 -8 2 21.70 0.92 0 -8 -2 23.05 1.17 0 8 -2 21.90 1.02 0 -8 2 21.52 1.23 0 -8 2 22.31 0.65 0 8 2 25.44 1.19 0 8 -2 21.65 0.91 0 8 -2 21.80 0.70 0 8 2 22.71 1.40 0 8 -2 20.84 1.25 0 8 -2 20.69 1.19 0 -8 2 23.99 1.17 0 8 2 21.67 1.24 0 -8 -2 23.02 1.13 0 -8 2 21.95 0.88 0 8 2 23.19 1.24 0 -8 -2 23.18 1.25 0 8 2 20.55 1.06 0 -8 3 43.13 1.33 0 -8 -3 40.16 1.67 0 8 3 41.05 1.85 0 -8 3 44.00 1.65 0 8 -3 40.26 1.86 0 8 3 40.53 2.00 0 -8 3 45.34 1.87 0 8 -3 43.60 1.34 0 -8 -3 43.74 1.89 0 8 -3 42.47 1.46 0 -8 -3 42.96 1.70 0 8 3 44.21 1.82 0 8 3 43.92 1.73 0 -8 -3 39.56 1.59 0 8 -3 39.66 1.72 0 -8 -4 59.22 2.12 0 8 -4 61.79 2.93 0 8 -4 60.94 2.38 0 -8 4 57.94 1.68 0 -8 4 59.55 2.03 0 8 4 54.35 2.33 0 -8 -4 57.67 2.08 0 8 4 56.19 2.53 0 8 -4 59.91 1.65 0 8 -4 61.53 2.19 0 -8 -4 57.51 2.12 0 8 -4 58.27 1.83 0 8 4 60.43 2.23 0 -8 -4 61.38 2.23 0 -8 -4 58.85 2.37 0 8 4 59.67 2.19 0 -8 -4 55.65 2.39 0 8 5 145.01 4.85 0 -8 -5 154.69 4.28 0 -8 5 153.94 4.07 0 8 -5 152.33 3.57 0 8 -5 158.01 5.26 0 8 -5 151.15 3.81 0 -8 -5 146.60 4.27 0 8 5 149.14 4.32 0 8 -5 148.75 4.52 0 -8 -5 151.03 4.66 0 8 5 155.14 4.35 0 8 -5 152.31 4.23 0 -8 -5 150.68 4.13 0 8 -5 148.78 3.30 0 8 5 152.54 4.58 0 -8 -5 161.89 4.40 0 8 -5 137.39 3.30 0 -8 5 150.35 3.61 0 8 6 570.46 13.86 0 -8 6 600.91 12.98 0 8 6 590.50 14.21 0 -8 -6 596.43 13.59 0 -8 -6 576.24 13.90 0 8 -6 594.39 13.23 0 -8 -6 582.86 14.28 0 8 -6 587.15 12.80 0 8 -6 585.07 13.71 0 8 -6 580.19 12.76 0 -8 6 598.52 13.55 0 8 -6 580.18 12.89 0 8 -6 597.83 15.03 0 -8 -6 588.54 13.84 0 8 -6 583.76 14.13 0 8 6 570.54 14.63 0 8 -7 239.04 5.45 0 -8 7 239.89 6.15 0 8 -7 230.09 6.25 0 -8 -7 231.28 6.40 0 8 -7 233.55 5.42 0 8 -7 239.35 5.50 0 -8 -7 240.06 6.15 0 8 7 233.39 6.47 0 8 -7 235.58 5.81 0 8 -7 240.11 6.71 0 8 -8 4.93 0.80 0 8 -8 5.16 0.61 0 8 -8 6.65 0.48 0 -8 -8 6.95 0.81 0 8 -8 7.94 1.08 0 -8 -8 6.93 0.93 0 8 -8 6.32 0.45 0 8 -8 5.71 0.53 0 8 8 5.48 0.97 0 -8 -8 6.98 1.15 0 8 -8 5.22 0.51 0 8 -9 22.64 0.96 0 8 -9 18.80 1.61 0 8 -9 20.38 1.12 0 8 -9 20.73 1.40 0 8 -9 21.57 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0 -9 -4 188.02 5.04 0 -9 4 189.21 4.96 0 9 -4 190.22 4.72 0 9 -4 192.00 4.51 0 -9 -4 186.52 5.14 0 -9 -5 143.95 4.31 0 9 -5 155.93 5.42 0 9 -5 143.07 4.29 0 -9 5 151.31 4.14 0 -9 5 150.53 3.66 0 -9 -5 155.83 4.75 0 9 -5 144.05 3.60 0 9 -5 145.43 4.60 0 9 5 145.39 4.41 0 -9 -5 147.58 4.39 0 -9 -5 150.59 4.71 0 -9 -5 144.95 4.29 0 9 5 148.72 4.97 0 -9 -5 148.49 4.20 0 9 5 146.99 4.37 0 9 -5 153.02 3.88 0 9 5 152.90 4.66 0 -9 6 523.56 11.79 0 9 6 516.26 13.56 0 9 6 540.57 12.81 0 -9 -6 522.16 12.69 0 9 -6 523.53 12.61 0 9 6 529.05 13.09 0 9 -6 530.64 11.73 0 9 -6 538.16 13.09 0 -9 6 532.18 12.40 0 -9 -6 539.56 12.73 0 9 -6 541.63 12.08 0 -9 -6 528.64 12.46 0 9 -7 36.28 1.16 0 9 -7 35.91 1.44 0 9 -7 36.59 1.03 0 9 7 39.15 2.45 0 9 7 35.22 1.88 0 -9 7 38.29 1.70 0 -9 -7 35.19 1.85 0 9 -7 36.14 1.06 0 9 -7 42.12 2.17 0 -9 7 36.18 1.20 0 -9 -7 34.80 1.66 0 -9 -7 37.55 1.89 0 9 -7 39.27 1.85 0 9 -8 24.97 0.89 0 9 -8 22.33 1.46 0 9 -8 22.36 1.70 0 -9 -8 25.57 1.60 0 -9 -8 26.96 1.42 0 9 8 25.14 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1.01 0 11 5 25.50 1.64 0 11 -5 24.62 1.20 0 -11 -5 24.96 1.45 0 -11 -5 23.86 1.73 0 11 -5 26.64 1.77 0 11 5 24.19 1.69 0 11 -5 23.83 1.52 0 -11 6 129.53 3.33 0 -11 -6 134.31 4.16 0 11 -6 125.68 3.58 0 11 -6 132.12 3.31 0 -11 6 138.20 3.96 0 -11 -6 136.27 4.01 0 -11 -6 132.64 4.58 0 11 6 132.41 4.52 0 11 6 128.66 4.26 0 11 6 128.29 4.92 0 11 -6 126.37 4.51 0 11 -6 129.43 4.19 0 11 -7 24.80 1.22 0 -11 -7 25.39 1.90 0 11 7 28.20 2.24 0 -11 -7 26.49 1.46 0 -11 -7 23.75 1.58 0 11 7 23.20 1.63 0 -11 -7 25.18 1.62 0 11 -7 25.68 1.62 0 11 -7 26.46 1.90 0 11 -7 23.96 0.92 0 -11 7 25.07 0.97 0 -11 -8 44.41 2.28 0 -11 -8 52.01 2.13 0 -11 -8 48.16 2.35 0 11 -8 50.11 2.34 0 11 8 54.46 3.16 0 11 -8 50.08 1.85 0 11 8 50.99 2.47 0 11 -8 51.72 2.68 0 -11 -8 48.03 2.66 0 -11 -9 7.82 1.09 0 11 -9 7.55 1.09 0 -11 -9 9.16 1.14 0 11 9 8.78 1.20 0 11 -9 9.44 1.34 0 -11 -10 28.52 1.90 0 11 10 27.28 1.90 0 11 -10 29.29 2.16 0 11 -10 27.09 1.79 0 -11 -10 27.55 1.85 0 11 11 11.24 1.96 0 11 11 8.50 1.29 0 11 -11 8.43 1.42 0 -11 -11 6.73 1.11 0 11 -11 7.49 1.15 0 11 -12 12.60 1.66 0 -12 0 25.70 1.06 0 -12 0 28.33 1.60 0 -12 0 27.05 1.37 0 -12 0 26.78 1.29 0 -12 0 26.21 1.57 0 -12 0 26.91 1.17 0 12 0 24.48 1.43 0 12 0 24.46 1.63 0 12 0 27.68 1.36 0 12 0 28.83 1.81 0 12 -1 37.09 2.03 0 -12 -1 41.90 1.98 0 12 1 35.83 1.65 0 -12 1 34.99 1.48 0 -12 1 33.88 1.78 0 12 -1 33.88 1.93 0 -12 -1 39.43 1.81 0 -12 1 37.80 1.28 0 12 1 38.91 2.15 0 -12 1 38.31 1.58 0 12 -1 37.37 1.56 0 12 1 37.27 1.82 0 -12 1 34.21 1.17 0 12 -1 38.13 1.69 0 -12 -1 37.22 1.54 0 -12 -1 38.67 1.63 0 12 1 35.36 1.94 0 -12 -1 35.54 1.41 0 -12 -1 38.45 1.87 0 12 2 16.38 1.51 0 -12 2 15.63 0.90 0 12 2 20.04 1.42 0 -12 2 17.45 0.61 0 -12 -2 17.07 1.12 0 12 -2 16.50 0.96 0 -12 -2 17.03 1.00 0 12 2 16.39 1.15 0 -12 -2 15.47 1.06 0 12 -2 16.60 1.36 0 -12 -2 17.55 1.32 0 12 -2 17.43 1.11 0 -12 -2 17.43 1.29 0 -12 2 17.29 0.97 0 -12 2 16.16 0.58 0 12 2 17.42 1.31 0 -12 2 19.29 1.26 0 -12 -3 36.91 1.82 0 -12 3 37.24 1.42 0 -12 -3 36.44 1.72 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17.57 1.91 0 -12 -7 19.12 1.74 0 12 -7 18.04 1.47 0 12 -7 20.45 1.71 0 -12 -7 17.46 1.39 0 -12 -8 45.63 2.29 0 12 8 45.86 2.37 0 12 -8 47.93 2.67 0 -12 -8 47.87 2.31 0 -12 -8 46.62 2.69 0 12 -8 45.47 2.28 0 12 8 43.75 2.90 0 -12 -9 9.08 1.16 0 -12 -9 6.52 1.06 0 -12 -9 5.74 1.32 0 12 9 8.56 1.28 0 12 -9 10.47 1.25 0 12 -9 9.58 1.40 0 -12 -10 17.16 1.55 0 12 -10 16.85 1.78 0 -12 -10 18.35 1.58 0 12 -10 15.27 1.51 0 12 10 16.73 1.63 0 12 -11 3.69 1.08 0 -12 -11 5.00 1.11 0 12 11 5.51 1.72 0 -12 -11 4.58 1.09 0 12 -11 0.60 1.15 0 13 0 -0.37 0.67 0 -13 0 0.07 0.30 0 -13 0 -0.04 0.41 0 -13 0 -0.26 0.55 0 13 0 -0.33 0.75 0 -13 0 -0.06 0.44 0 13 0 0.31 0.51 0 13 0 -0.52 0.73 0 -13 1 32.23 1.20 0 13 1 36.06 1.68 0 13 1 33.41 1.96 0 -13 1 34.99 1.56 0 -13 1 33.10 1.13 0 -13 -1 36.78 1.77 0 13 1 32.18 1.75 0 13 1 36.15 2.17 0 -13 -1 36.07 1.52 0 -13 -1 33.00 1.56 0 -13 -1 31.12 1.35 0 -13 1 33.34 1.47 0 13 -1 31.33 1.96 0 13 -1 35.47 1.70 0 13 -1 35.00 1.55 0 13 -1 31.58 1.95 0 13 -2 10.90 0.95 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1356.66 28.84 2 2 -1 1359.45 28.70 2 2 -1 1301.68 28.76 -2 2 1 1364.01 28.83 2 2 -1 1331.57 29.00 2 -2 -1 1356.07 28.91 2 -2 -1 1318.30 28.88 -2 2 1 1335.97 28.83 -2 2 1 1263.83 28.93 -2 2 1 1301.81 28.92 2 -2 -1 1339.51 28.92 2 -2 0 334.05 7.88 2 2 0 337.25 7.54 -2 2 0 332.55 7.65 2 2 0 334.81 7.50 -2 2 0 327.39 7.66 2 -2 0 328.84 7.45 -2 2 0 337.02 7.48 2 2 0 342.60 7.60 -2 -2 0 332.61 7.57 2 -2 0 333.35 7.62 -2 -2 0 339.40 7.57 2 -2 0 337.11 7.66 2 2 0 328.27 7.86 -2 2 -1 6199.53 126.89 2 2 1 6056.58 126.77 2 2 1 6071.87 127.05 2 -2 1 5984.37 126.55 2 -2 1 6039.79 127.36 -2 2 -1 5927.72 126.58 -2 -2 -1 5903.57 126.75 -2 2 -1 5870.57 126.83 2 2 1 5380.83 127.14 -2 -2 -1 5569.71 126.95 2 -2 1 5936.19 126.88 -2 -2 -1 6164.51 127.17 -2 2 -2 78.57 2.18 -2 2 -2 77.89 1.89 -2 -2 -2 80.57 2.54 2 2 2 82.00 2.55 2 2 2 81.44 2.65 -2 2 -2 75.30 2.30 2 -2 2 81.42 1.87 -2 -2 -2 77.60 2.19 2 -2 2 81.49 2.74 -2 -2 -2 83.51 2.15 -2 2 -2 78.33 2.65 2 2 2 79.07 2.19 2 -2 2 77.05 2.28 2 2 3 28.98 1.11 -2 2 -3 27.72 1.19 -2 2 -3 26.78 0.75 2 -2 3 22.16 1.11 2 -2 3 28.22 0.76 2 2 3 24.76 1.04 -2 -2 -3 25.73 0.99 -2 -2 -3 26.64 1.38 -2 -2 -3 26.55 1.07 -2 2 -3 26.15 1.03 2 -2 3 27.55 1.02 2 2 3 27.01 1.41 2 -2 3 27.13 1.56 -2 2 -3 27.54 1.49 -2 -2 -4 123.31 3.72 -2 2 -4 124.22 2.81 2 2 4 124.26 3.28 2 -2 4 121.37 2.84 2 -2 4 118.58 3.14 -2 -2 -4 112.37 3.24 -2 -2 -4 115.33 3.71 -2 -2 -4 119.82 3.13 2 2 4 116.23 3.79 2 2 4 120.07 3.17 -2 2 -4 120.39 3.45 -2 2 -4 125.20 3.90 -2 2 -4 122.91 3.19 2 2 5 13.22 1.21 -2 2 -5 9.48 1.03 -2 -2 -5 11.19 1.12 -2 -2 -5 12.79 0.72 2 2 5 11.08 0.74 -2 2 -5 11.58 0.71 -2 -2 -5 12.32 0.80 2 -2 5 12.33 0.73 2 2 5 13.95 1.19 -2 2 -5 9.84 1.12 -2 -2 -5 11.00 1.04 -2 2 -5 11.27 0.88 2 -2 5 11.48 0.54 -2 2 -5 12.13 0.49 -2 -2 -6 65.13 2.27 -2 -2 -6 68.03 2.76 2 -2 6 66.41 2.14 2 2 6 68.54 2.93 2 2 6 70.06 2.20 -2 2 -6 68.19 1.81 2 -2 6 66.52 1.88 -2 -2 -6 69.92 2.13 -2 2 -6 69.02 2.49 2 -2 6 67.92 3.05 -2 2 -6 66.41 2.16 -2 2 -6 57.61 2.72 -2 -2 -6 71.72 2.75 2 2 6 67.07 2.88 -2 2 -6 64.97 2.73 2 2 7 85.95 3.55 -2 2 -7 86.41 3.35 -2 -2 -7 90.25 2.89 -2 2 -7 85.40 3.06 -2 -2 -7 89.35 3.34 2 2 7 88.56 2.86 -2 -2 -7 86.84 2.64 -2 -2 -7 89.94 3.44 2 -2 7 89.93 2.72 -2 2 -7 79.39 3.35 2 -2 7 86.24 3.70 -2 2 -7 82.31 2.68 -2 2 -7 90.18 2.34 2 2 7 90.06 2.74 2 -2 8 153.79 4.45 -2 2 -8 170.66 4.09 2 2 8 162.46 5.54 -2 -2 -8 165.00 5.22 2 2 8 162.54 4.49 -2 2 -8 171.42 5.00 -2 2 -8 146.96 5.21 -2 -2 -8 170.71 4.74 -2 -2 -8 162.68 4.40 -2 2 -8 163.89 4.52 -2 -2 -8 165.25 5.24 2 -2 8 166.82 5.78 -2 -2 -9 37.70 2.28 -2 2 -9 44.58 1.87 -2 2 -9 49.13 1.63 -2 2 -9 43.22 1.50 2 2 9 39.58 2.55 -2 -2 -9 46.20 2.02 -2 -2 -9 43.38 1.77 2 2 9 43.10 1.86 -2 2 -9 44.25 2.21 -2 -2 -9 43.34 2.38 2 -2 9 39.46 2.69 -2 2 -10 89.77 2.59 2 -2 10 90.17 4.25 -2 2 -10 87.31 3.02 2 2 10 82.69 2.95 -2 -2 -10 85.17 2.88 -2 -2 -10 80.92 3.58 2 2 10 84.81 3.92 -2 -2 -10 92.14 3.65 -2 2 -10 86.58 3.46 -2 -2 -10 88.90 3.19 -2 -2 -11 26.35 2.01 -2 2 -11 22.37 1.43 -2 -2 -11 25.13 1.61 -2 -2 -11 22.47 1.34 -2 -2 -11 24.23 1.91 -2 2 -11 27.53 1.89 -2 2 -11 24.12 1.14 2 -2 11 22.44 2.27 2 2 11 23.04 2.15 2 -2 12 30.20 2.69 -2 -2 -12 27.50 2.16 -2 -2 -12 35.44 2.34 -2 -2 -12 28.51 1.55 -2 -2 -12 25.28 1.71 -2 2 -12 30.09 2.06 2 2 12 29.46 2.45 -2 2 -12 27.06 1.99 -2 2 -12 29.45 1.69 -2 2 -13 15.33 1.66 -2 2 -13 13.20 1.29 -2 -2 -13 13.59 1.76 2 2 13 13.24 1.98 2 -2 13 15.55 2.13 -2 -2 -13 16.37 1.19 -2 -2 -13 14.38 1.39 -2 2 -14 24.15 1.70 -2 -2 -14 18.57 1.64 2 2 14 21.50 2.53 -2 2 -14 22.86 2.02 -2 2 -15 16.22 1.53 2 -3 -15 2.66 1.02 2 3 -14 2.32 0.75 2 -3 -14 1.68 0.90 2 -3 -14 1.75 0.93 2 3 -13 6.94 1.16 -2 3 13 9.57 1.61 2 3 -13 6.37 0.91 2 -3 -13 8.46 1.43 2 3 -13 9.55 1.10 2 3 -13 8.02 1.01 2 -3 -13 8.35 1.15 2 -3 -13 6.63 1.11 2 -3 -12 10.63 1.42 -2 3 12 10.00 1.52 2 3 -12 10.96 1.11 2 -3 -12 7.69 1.11 2 -3 -12 11.17 1.27 2 3 -12 12.01 1.05 2 3 -12 9.96 1.17 2 3 -12 11.25 1.08 2 3 -12 10.96 1.03 2 3 -11 4.02 0.80 -2 3 11 3.10 1.08 2 -3 -11 2.65 0.80 2 3 -11 4.84 0.76 2 -3 -11 4.69 0.91 2 3 -11 6.28 0.82 2 3 -11 4.38 0.70 2 -3 -11 4.75 0.54 2 -3 -11 4.99 1.14 2 3 -11 4.87 0.95 2 3 -11 4.26 0.77 2 3 -11 5.35 1.10 2 -3 -10 9.61 0.65 2 3 -10 9.63 0.99 2 3 -10 8.60 0.83 2 3 -10 9.82 1.21 2 -3 -10 7.99 0.68 2 3 -10 9.25 0.91 -2 3 10 7.12 1.26 2 3 -10 10.07 1.07 2 3 -10 9.03 0.90 2 -3 -10 9.39 1.20 2 3 -10 9.27 0.87 2 3 -10 8.47 0.84 2 -3 -10 8.73 1.04 2 -3 -10 12.19 1.16 2 3 -10 7.14 0.91 2 -3 -9 136.47 4.58 2 3 -9 137.03 4.13 2 -3 -9 140.21 3.61 2 3 -9 135.91 4.04 2 -3 -9 137.85 4.32 2 3 -9 145.36 3.98 2 3 -9 145.51 4.02 2 -3 -9 134.65 3.46 -2 3 9 138.67 4.44 2 3 -9 138.95 3.90 2 3 -9 137.28 4.17 2 3 -9 138.08 4.50 2 3 -9 143.16 4.04 -2 3 9 140.62 4.75 2 3 -9 140.07 4.19 2 -3 -9 139.52 4.46 2 -3 -8 105.14 3.40 2 3 -8 112.10 3.73 2 3 -8 105.81 3.29 2 3 -8 109.93 3.21 2 -3 -8 107.76 3.53 2 3 -8 102.88 3.24 2 -3 -8 105.74 2.70 -2 3 8 105.21 3.62 2 -3 -8 116.26 3.80 -2 3 8 110.72 3.65 2 3 -8 108.11 3.09 2 3 -8 110.39 3.25 2 -3 -8 111.21 2.83 2 -3 -8 106.06 3.56 2 -3 -8 105.03 3.62 -2 3 8 109.45 3.83 2 3 -8 110.92 3.38 2 -3 -7 45.12 1.97 2 3 -7 43.55 1.72 2 3 -7 46.83 2.10 2 -3 -7 42.64 1.93 2 3 -7 41.11 1.49 -2 3 7 44.19 2.00 2 3 -7 43.04 1.64 2 -3 -7 42.71 1.20 2 -3 -7 43.93 1.89 2 3 -7 40.90 1.65 -2 -3 7 42.57 1.62 2 -3 -7 43.10 1.80 -2 -3 7 46.45 1.74 2 3 -7 41.43 1.62 2 -3 -7 43.49 2.02 2 3 -7 44.22 1.68 -2 3 7 42.29 2.05 2 -3 -7 42.73 1.27 2 -3 -6 183.78 4.76 2 3 -6 175.91 4.61 -2 3 6 174.82 4.98 2 -3 -6 174.22 3.93 2 -3 -6 168.39 4.81 2 3 -6 177.37 4.48 2 -3 -6 178.13 3.98 -2 -3 6 180.33 4.67 2 3 -6 178.18 4.53 2 3 -6 167.60 4.29 2 3 -6 188.94 5.17 2 3 -6 178.37 4.56 -2 3 6 176.17 5.06 2 3 -6 176.50 4.51 2 -3 -6 178.74 4.90 2 -3 -6 171.66 4.87 -2 -3 6 183.07 4.50 2 -3 -6 183.90 5.03 -2 -3 5 107.03 2.83 2 3 -5 106.39 2.89 2 -3 -5 104.32 3.20 2 3 -5 101.08 2.97 2 3 -5 100.95 2.74 2 -3 -5 101.30 3.12 2 -3 -5 110.78 3.10 -2 3 5 103.43 3.24 -2 -3 5 104.02 2.96 2 -3 -5 108.02 3.29 2 3 -5 100.84 2.61 2 3 -5 105.52 2.83 -2 3 5 107.14 3.31 2 -3 -5 107.63 3.20 2 3 -5 106.18 2.81 -2 -3 4 1653.22 36.17 2 -3 -4 1590.28 36.37 2 -3 -4 1699.85 36.43 2 3 -4 1682.13 35.71 2 3 -4 1668.03 36.09 2 -3 -4 1680.33 36.31 -2 -3 4 1636.82 36.16 2 -3 -4 1740.29 36.53 2 3 -4 1656.55 36.24 2 3 -4 1683.80 35.84 2 3 -4 1661.20 35.83 2 3 -4 1686.72 35.98 2 -3 -4 1619.68 36.36 -2 -3 4 1669.03 35.99 -2 3 4 1617.83 36.43 -2 3 4 1644.90 36.48 2 -3 -3 560.08 13.10 -2 -3 3 581.08 12.47 2 -3 -3 541.62 13.01 2 3 -3 577.91 12.47 -2 -3 3 579.13 12.92 2 3 -3 570.02 12.67 2 3 -3 593.37 12.82 2 3 -3 567.99 12.98 2 -3 -3 592.35 12.98 -2 -3 3 572.36 12.71 2 -3 -3 575.65 13.04 2 -3 -3 581.80 13.16 -2 3 3 579.25 13.14 -2 3 3 569.64 13.11 2 -3 -2 144.48 3.68 -2 -3 2 135.31 3.62 -2 3 2 138.99 3.76 2 -3 -2 143.30 3.71 -2 3 2 142.56 3.27 -2 3 2 136.64 3.73 2 3 -2 146.08 3.37 2 3 -2 137.09 3.69 -2 3 2 143.17 3.40 2 3 -2 145.06 3.52 -2 -3 2 143.75 3.42 2 -3 -2 143.50 3.76 -2 -3 1 978.74 20.79 2 -3 -1 910.04 21.20 2 3 -1 963.70 21.08 2 3 -1 979.11 20.93 -2 -3 1 964.83 20.96 -2 3 1 954.13 21.21 -2 -3 1 946.68 21.11 -2 3 1 986.43 21.30 2 -3 -1 987.29 21.23 2 3 -1 947.95 21.34 2 -3 -1 945.28 21.27 -2 -3 1 983.40 20.86 -2 3 1 972.32 21.30 2 3 -1 973.27 20.90 2 3 0 1137.83 24.49 2 -3 0 1144.60 24.74 -2 3 0 1099.40 24.71 -2 3 0 1044.09 24.93 2 3 0 1144.87 24.58 2 -3 0 1087.80 24.97 -2 -3 0 1115.65 24.61 -2 -3 0 1097.02 24.51 2 -3 0 1155.16 24.49 -2 3 0 1170.43 24.52 -2 3 0 1150.14 24.78 -2 -3 0 1150.51 24.90 2 3 0 1133.71 24.65 2 3 0 1129.23 24.98 2 -3 0 1178.45 24.76 -2 -3 0 1145.45 24.61 2 -3 1 3037.26 65.69 -2 3 -1 3084.91 65.37 2 3 1 2979.80 66.06 2 3 1 3083.72 65.87 -2 -3 -1 3125.08 65.83 -2 3 -1 2956.23 65.71 -2 3 -1 2970.64 65.79 2 3 1 3052.30 65.56 2 3 1 3080.28 65.60 -2 3 -1 3021.86 65.65 2 -3 1 3150.69 65.77 2 -3 1 2952.23 66.22 2 -3 1 3095.75 65.34 -2 -3 -1 3084.59 65.61 -2 -3 -1 3059.32 65.99 -2 3 -2 283.43 6.98 2 -3 2 292.82 6.95 2 -3 2 295.86 6.38 2 3 2 299.99 6.81 -2 -3 -2 297.59 6.80 -2 3 -2 286.99 6.79 -2 3 -2 291.37 6.90 -2 3 -2 297.01 6.43 2 3 2 278.99 7.17 2 3 2 276.50 7.29 2 -3 2 290.89 7.52 2 -3 2 300.53 6.73 -2 -3 -2 287.68 7.22 -2 3 -3 61.29 2.07 2 3 3 61.12 2.32 2 3 3 62.62 1.94 2 3 3 62.95 1.90 -2 -3 -3 61.30 1.93 2 -3 3 64.84 1.83 -2 -3 -3 59.44 1.87 -2 3 -3 66.29 1.88 2 -3 3 63.27 2.05 2 -3 3 67.69 2.64 -2 -3 -3 65.71 2.29 -2 3 -3 64.51 2.48 -2 3 -4 69.02 2.75 2 -3 4 71.09 2.04 -2 -3 -4 71.39 2.55 -2 3 -4 72.23 2.10 -2 -3 -4 70.55 2.11 2 3 4 72.20 2.16 -2 -3 -4 71.33 2.22 -2 3 -4 70.77 1.63 -2 3 -4 71.82 2.38 2 3 4 70.04 2.70 2 3 4 70.74 2.22 2 -3 4 68.60 2.90 2 3 5 119.69 4.03 2 3 5 119.05 4.05 -2 -3 -5 122.86 3.83 -2 3 -5 118.70 3.59 2 3 5 121.19 3.36 -2 3 -5 124.66 2.78 -2 3 -5 120.10 3.26 -2 -3 -5 118.38 3.43 2 3 5 116.21 3.40 -2 -3 -5 125.91 3.97 -2 -3 -5 118.93 3.29 2 -3 5 120.75 3.22 -2 3 -5 121.02 4.07 -2 3 -6 177.82 4.60 -2 -3 -6 182.69 5.42 -2 3 -6 168.08 5.30 2 -3 6 174.26 4.55 2 3 6 171.27 4.68 -2 -3 -6 172.04 4.60 -2 3 -6 163.76 5.41 2 3 6 173.90 5.55 2 3 6 174.27 5.48 -2 3 -6 173.99 4.98 -2 -3 -6 178.93 5.24 -2 3 -6 179.72 4.10 -2 -3 -6 175.70 4.81 2 -3 7 91.06 2.87 -2 3 -7 94.86 3.60 -2 -3 -7 96.63 2.94 -2 3 -7 99.96 3.34 -2 -3 -7 100.31 3.16 -2 3 -7 91.81 2.88 -2 3 -7 97.24 2.45 2 -3 7 99.21 4.10 -2 3 -7 109.68 2.59 -2 -3 -7 98.91 3.54 2 3 7 95.71 3.83 -2 -3 -7 98.77 3.57 -2 3 -7 94.99 3.71 2 3 7 94.08 3.77 2 3 7 97.52 3.02 -2 -3 -7 96.61 3.64 -2 -3 -8 2.76 0.89 -2 3 -8 1.54 0.48 -2 -3 -8 2.45 0.90 -2 3 -8 1.71 0.30 2 -3 8 2.28 1.10 2 -3 8 0.97 0.51 -2 -3 -8 1.34 0.44 -2 -3 -8 2.58 0.68 2 3 8 2.47 0.60 -2 3 -8 1.77 0.40 -2 3 -8 1.72 0.68 2 3 8 2.65 0.93 -2 -3 -9 7.97 1.25 2 3 9 7.23 1.35 2 3 9 6.59 0.83 -2 3 -9 8.96 0.56 -2 -3 -9 8.39 0.91 -2 3 -9 8.32 0.83 2 -3 9 6.95 1.41 -2 -3 -9 8.34 0.82 -2 3 -9 8.05 1.05 -2 3 -9 9.03 0.68 -2 -3 -9 8.83 1.21 -2 3 -10 33.85 1.32 -2 -3 -10 27.37 2.06 2 3 10 30.50 2.32 -2 3 -10 30.82 1.90 -2 -3 -10 29.97 1.52 -2 3 -10 32.39 1.59 -2 3 -10 30.52 1.16 2 -3 10 29.90 2.48 -2 -3 -10 28.00 1.69 2 3 10 34.88 2.55 2 3 11 27.75 2.34 2 -3 11 27.15 2.47 -2 3 -11 29.81 1.17 -2 -3 -11 30.39 1.77 -2 3 -11 26.39 1.54 -2 -3 -11 28.46 1.55 -2 3 -11 26.47 1.89 -2 -3 -11 23.88 1.98 -2 3 -12 46.93 2.62 -2 -3 -12 49.85 2.16 -2 -3 -12 57.51 3.04 -2 3 -12 55.25 2.78 2 3 12 53.65 3.22 -2 -3 -12 50.59 2.46 -2 3 -12 51.73 2.28 2 -3 12 51.67 3.36 -2 -3 -13 3.34 0.79 -2 3 -13 0.80 0.96 -2 3 -13 3.75 0.88 -2 -3 -13 3.66 0.96 2 3 13 4.33 1.52 -2 -3 -13 3.40 1.21 -2 3 -14 2.59 1.23 -2 3 -14 3.74 0.95 2 3 14 2.06 1.59 -2 4 14 31.77 2.60 2 -4 -14 27.68 1.93 2 -4 -14 31.23 2.07 2 4 -13 16.11 1.22 -2 4 13 13.44 1.79 2 4 -13 14.18 1.26 2 4 -13 13.63 1.25 2 -4 -13 12.67 1.39 2 -4 -13 12.08 1.34 2 4 -13 15.85 1.32 2 4 -12 3.29 0.76 2 -4 -12 2.60 0.89 2 4 -12 2.91 0.69 2 4 -12 3.30 0.85 2 4 -12 3.28 0.74 2 4 -12 2.44 0.73 2 -4 -12 3.20 1.10 2 -4 -12 3.81 0.93 -2 4 12 4.46 1.31 2 -4 -11 16.32 1.37 2 4 -11 13.88 1.29 2 -4 -11 15.80 1.63 -2 4 11 15.48 1.72 2 -4 -11 17.58 1.45 2 4 -11 18.25 1.28 2 4 -11 18.07 1.34 2 4 -11 16.88 1.10 2 4 -11 14.84 1.51 2 4 -11 14.44 1.10 2 4 -11 16.97 1.24 2 4 -11 16.33 1.21 2 4 -10 12.11 1.15 2 -4 -10 12.20 1.17 -2 4 10 10.96 1.44 2 -4 -10 11.27 0.64 2 4 -10 11.73 0.90 2 4 -10 12.21 1.05 2 -4 -10 11.52 1.17 2 4 -10 10.04 0.93 2 -4 -10 12.06 1.38 2 4 -10 11.60 0.91 2 4 -10 11.68 1.38 2 -4 -10 11.06 0.70 2 4 -10 11.80 1.04 2 4 -10 9.39 0.87 2 4 -10 11.39 1.02 -2 4 9 81.90 3.37 -2 4 9 76.50 3.05 2 -4 -9 74.54 3.16 2 4 -9 84.69 2.55 2 -4 -9 72.50 2.87 2 4 -9 75.08 2.72 2 4 -9 76.47 2.74 2 4 -9 79.02 2.55 2 4 -9 84.67 3.27 2 4 -9 75.96 2.67 2 4 -9 78.13 2.50 2 4 -9 76.41 2.56 2 -4 -9 76.42 2.15 2 -4 -9 75.75 3.04 2 4 -9 76.66 2.75 2 -4 -8 17.96 1.41 2 4 -8 16.04 1.09 2 4 -8 17.55 0.95 -2 4 8 15.80 1.34 2 4 -8 14.29 1.34 2 4 -8 16.22 0.99 2 4 -8 15.57 0.90 2 -4 -8 16.38 1.20 2 4 -8 15.10 0.95 2 4 -8 16.22 1.13 2 -4 -8 15.18 0.69 -2 4 8 17.69 1.45 2 4 -8 16.77 1.04 2 -4 -8 18.47 1.37 2 4 -7 25.75 1.68 -2 -4 7 28.02 1.29 2 4 -7 26.16 1.27 2 4 -7 26.53 1.34 2 -4 -7 23.41 1.37 -2 4 7 24.96 1.54 2 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4 76.38 2.39 2 -4 -4 80.20 2.57 2 4 -4 77.18 2.24 -2 -4 4 77.39 2.08 -2 4 4 80.78 2.68 -2 4 4 77.99 2.58 2 4 -3 44.60 1.45 -2 -4 3 45.83 1.63 -2 -4 3 43.12 1.30 -2 -4 3 45.20 1.14 -2 -4 3 45.25 1.51 -2 4 3 45.74 1.18 -2 4 3 44.55 1.29 2 -4 -3 48.44 1.82 -2 4 3 46.75 1.78 2 -4 -3 46.41 1.72 2 4 -3 43.70 1.18 2 -4 -3 45.03 1.69 -2 4 3 42.81 1.68 2 4 -3 43.57 1.64 2 4 -3 44.84 1.27 2 4 -2 121.98 3.15 -2 4 2 127.65 3.20 -2 4 2 122.70 2.98 -2 4 2 128.20 3.50 2 4 -2 127.42 2.94 -2 -4 2 123.03 2.99 -2 -4 2 123.54 2.85 2 4 -2 120.72 3.42 2 -4 -2 123.50 3.45 2 -4 -2 129.48 3.42 -2 4 2 123.87 3.42 2 4 -2 122.33 2.91 2 4 -1 716.56 16.16 2 4 -1 741.84 15.96 2 -4 -1 728.83 16.25 2 -4 -1 747.32 16.40 2 -4 -1 717.40 16.16 -2 4 1 733.95 16.12 -2 4 1 716.96 16.44 -2 -4 1 731.84 16.00 2 -4 -1 734.85 16.43 -2 4 1 770.93 16.45 -2 4 1 749.25 16.40 2 4 -1 729.55 16.52 -2 -4 1 739.93 16.01 2 4 -1 736.34 16.07 2 -4 0 1255.35 26.83 2 -4 0 1236.72 27.07 -2 -4 0 1260.04 26.78 2 4 0 1237.58 26.90 2 4 0 1238.56 26.75 -2 -4 0 1229.89 26.93 2 -4 0 1203.82 26.93 2 -4 0 1295.09 26.81 -2 4 0 1144.45 27.33 -2 -4 0 1235.48 27.23 2 -4 0 1264.30 27.11 -2 4 0 1258.20 27.12 -2 4 0 1227.70 27.16 2 -4 0 1203.14 27.33 2 4 0 1210.17 27.30 -2 4 0 1265.15 27.04 -2 -4 0 1263.33 26.94 2 4 0 1182.46 26.99 -2 4 -1 467.23 10.46 -2 -4 -1 438.63 10.34 2 -4 1 470.88 10.18 2 4 1 462.44 10.33 2 -4 1 442.44 11.01 2 4 1 444.10 10.67 2 -4 1 469.28 10.13 -2 4 -1 464.65 10.56 -2 -4 -1 469.43 10.44 2 4 1 464.35 10.89 2 -4 1 455.40 10.59 -2 4 -1 464.54 10.67 -2 -4 -1 478.37 10.80 2 4 1 477.04 10.42 2 -4 1 458.10 10.36 -2 -4 -1 457.95 10.61 -2 -4 -2 393.95 9.06 -2 4 -2 388.12 9.13 2 -4 2 398.86 8.92 2 -4 2 389.84 8.59 2 4 2 406.68 9.04 2 -4 2 401.68 8.56 2 -4 2 386.49 9.82 2 4 2 398.44 9.49 2 -4 2 411.04 9.24 -2 4 -2 379.77 9.26 -2 4 -2 393.16 9.00 -2 -4 -2 388.99 9.43 -2 -4 -2 401.60 9.41 -2 -4 -3 42.43 1.52 2 4 3 45.06 1.56 -2 4 -3 45.41 1.59 2 -4 3 45.42 1.41 2 4 3 44.99 1.95 -2 4 -3 46.13 1.48 2 -4 3 45.22 2.19 -2 4 -3 46.32 1.74 -2 4 -3 43.62 2.07 -2 -4 -3 47.89 1.90 2 -4 4 311.55 8.48 2 4 4 313.79 7.49 2 4 4 312.27 8.12 -2 4 -4 317.41 7.30 2 4 4 312.84 7.44 2 -4 4 314.06 7.20 -2 -4 -4 307.16 7.39 -2 -4 -4 315.61 7.88 -2 4 -4 311.16 7.67 -2 4 -4 311.42 8.23 2 4 4 298.24 8.06 2 4 5 21.57 1.47 -2 -4 -5 19.77 1.32 2 4 5 15.37 1.37 2 4 5 20.73 1.08 -2 4 -5 20.90 1.57 -2 -4 -5 20.67 1.10 -2 4 -5 21.35 1.22 -2 4 -5 19.57 0.93 2 4 5 19.47 1.09 2 -4 5 20.05 0.91 -2 -4 -5 18.41 0.99 -2 -4 -6 233.25 6.42 2 -4 6 240.01 5.71 2 4 6 236.60 5.97 -2 -4 -6 232.87 6.50 -2 4 -6 234.69 5.74 -2 -4 -6 238.23 6.62 -2 -4 -6 226.02 6.02 -2 -4 -6 230.04 5.86 -2 4 -6 218.46 6.72 -2 4 -6 236.52 5.10 -2 4 -6 228.52 5.13 2 4 6 230.79 6.72 2 4 6 228.80 6.00 -2 4 -6 240.09 6.25 2 4 6 241.18 6.87 -2 -4 -7 13.37 1.29 -2 4 -7 14.06 0.88 2 -4 7 13.33 0.88 2 4 7 16.56 1.07 -2 -4 -7 14.83 1.07 -2 4 -7 14.26 0.51 -2 -4 -7 14.39 0.95 2 4 7 14.50 1.42 -2 -4 -7 14.19 1.41 2 4 7 14.40 1.51 -2 4 -7 14.43 0.55 -2 -4 -7 13.78 1.11 -2 4 -7 13.81 1.13 -2 4 -7 13.29 1.45 -2 -4 -7 13.56 1.25 -2 4 -7 14.74 1.39 2 -4 7 14.10 1.61 -2 -4 -8 17.47 1.53 -2 4 -8 19.39 1.07 -2 4 -8 18.54 0.67 2 -4 8 17.87 1.07 -2 -4 -8 17.30 1.22 2 4 8 17.72 1.18 -2 -4 -8 17.72 1.13 -2 -4 -8 17.14 1.43 -2 4 -8 17.85 1.33 -2 4 -8 16.80 0.68 2 -4 8 14.45 1.73 2 4 8 17.08 1.63 2 4 8 16.81 1.67 -2 4 -9 43.07 1.35 -2 -4 -9 46.98 2.15 -2 4 -9 49.42 2.31 -2 -4 -9 43.66 2.46 -2 4 -9 47.90 1.42 -2 4 -9 45.95 1.86 2 4 9 43.97 2.61 -2 -4 -9 47.20 2.35 -2 -4 -9 45.95 1.94 2 -4 9 46.09 2.98 -2 4 -10 9.66 0.57 -2 -4 -10 12.38 1.48 -2 -4 -10 12.55 1.01 2 4 10 13.09 1.67 -2 -4 -10 11.57 1.18 -2 4 -10 12.24 1.00 -2 4 -10 11.82 1.27 2 -4 10 11.63 1.77 -2 4 -11 90.22 3.06 2 4 11 88.27 4.28 -2 -4 -11 83.64 3.81 -2 -4 -11 87.19 3.09 2 4 11 90.85 4.12 -2 4 -11 87.04 3.52 2 -4 11 91.98 4.55 -2 -4 -11 84.25 3.30 -2 -4 -12 26.53 1.59 -2 -4 -12 24.35 1.71 -2 4 -12 23.66 1.86 2 4 12 25.23 2.27 -2 4 -12 28.99 1.60 2 4 13 1.41 1.40 -2 -4 -13 2.46 0.80 -2 -4 -13 1.89 0.94 -2 4 -13 1.73 0.80 -2 4 -13 1.98 1.03 -2 -4 -13 2.20 1.27 2 4 14 6.06 1.74 -2 4 -14 5.01 1.08 -2 4 -14 6.51 1.41 -2 5 14 7.16 1.72 2 -5 -14 6.43 1.18 2 -5 -14 5.76 1.16 2 5 -13 1.18 0.82 2 -5 -13 0.96 0.94 2 -5 -13 -0.67 0.82 -2 5 13 1.03 1.29 -2 5 12 4.18 1.38 2 -5 -12 0.69 1.09 2 5 -12 2.93 0.84 2 -5 -12 2.56 0.91 2 5 -12 2.45 0.83 2 -5 -12 3.16 0.96 2 5 -12 3.59 0.76 2 5 -12 3.47 0.67 2 5 -12 2.39 0.78 2 5 -11 29.31 1.41 -2 5 11 26.47 2.20 2 5 -11 30.56 1.64 2 5 -11 29.89 1.68 2 -5 -11 27.08 1.76 2 -5 -11 28.91 2.07 2 -5 -11 29.45 1.87 2 5 -11 28.27 1.48 2 5 -11 28.24 1.67 2 -5 -10 65.81 2.83 2 5 -10 71.10 2.32 2 5 -10 70.89 2.66 2 5 -10 68.07 2.52 2 -5 -10 63.01 1.93 2 5 -10 72.26 2.75 2 5 -10 66.50 2.56 2 -5 -10 66.70 2.80 2 5 -10 67.27 3.13 -2 5 10 67.49 3.27 2 -5 -10 70.89 3.18 2 5 -10 72.13 2.44 2 5 -10 72.84 2.43 2 5 -10 68.54 2.33 -2 5 9 32.99 1.97 2 -5 -9 34.09 2.11 2 5 -9 33.71 1.47 2 5 -9 35.36 1.43 2 -5 -9 32.88 1.81 2 5 -9 32.19 1.55 2 5 -9 34.76 1.48 2 5 -9 34.06 1.75 2 -5 -9 36.05 1.15 -2 5 9 36.53 2.25 2 5 -9 34.62 2.16 2 5 -9 36.34 1.53 2 5 -9 34.67 1.69 2 5 -8 2.81 0.47 2 5 -8 4.56 1.00 2 5 -8 3.28 0.54 -2 5 8 4.60 1.02 2 5 -8 3.95 0.58 2 -5 -8 5.04 0.78 -2 5 8 4.48 0.39 -2 5 8 3.90 0.90 2 -5 -8 3.23 0.89 -2 -5 8 5.70 0.67 2 5 -8 3.66 0.69 2 5 -8 5.09 0.74 2 5 -8 3.95 0.49 2 -5 -8 4.22 0.36 2 5 -8 4.68 0.60 2 -5 -8 4.04 0.88 2 -5 -7 244.87 6.77 2 5 -7 257.48 6.31 -2 5 7 249.88 6.85 2 5 -7 258.79 7.26 2 -5 -7 248.02 6.64 2 5 -7 253.30 6.12 2 -5 -7 243.82 5.61 2 5 -7 251.18 6.05 -2 -5 7 261.04 6.37 -2 5 7 246.92 5.63 2 5 -7 244.85 6.00 -2 5 7 253.10 7.09 2 5 -7 250.83 6.03 2 -5 -7 242.37 6.87 2 -5 -7 249.64 6.47 2 -5 -7 257.77 6.75 2 5 -7 244.22 6.50 2 5 -7 255.33 5.97 -2 5 6 61.26 2.58 2 5 -6 64.70 2.33 -2 5 6 62.80 1.60 2 -5 -6 62.96 1.58 2 -5 -6 65.75 2.57 2 5 -6 63.08 2.00 2 -5 -6 59.82 2.33 -2 -5 6 64.77 2.12 2 5 -6 64.82 1.86 2 -5 -6 65.41 2.29 2 5 -6 62.03 1.88 2 5 -6 61.80 1.87 -2 5 6 63.16 2.46 2 5 -6 62.80 2.07 2 -5 -6 62.34 2.44 2 -5 -6 64.46 2.49 2 5 -5 162.95 3.86 2 -5 -5 167.24 4.80 -2 -5 5 164.27 4.46 2 -5 -5 160.14 4.56 -2 5 5 163.89 4.66 2 -5 -5 168.53 3.74 -2 -5 5 163.84 4.28 2 5 -5 167.15 4.56 -2 -5 5 170.40 3.95 -2 5 5 160.48 3.79 2 5 -5 159.79 4.15 2 5 -5 168.97 3.97 2 5 -5 167.12 3.99 2 -5 -5 161.04 4.61 2 5 -5 168.55 4.18 2 -5 -5 156.75 4.64 -2 5 5 160.80 4.83 -2 -5 4 356.47 7.91 -2 5 4 356.32 8.80 -2 -5 4 347.60 8.50 2 5 -4 360.51 8.21 -2 5 4 342.96 8.67 -2 5 4 344.96 8.80 -2 -5 4 366.12 8.33 2 -5 -4 356.17 7.84 2 5 -4 356.61 7.90 2 -5 -4 352.38 8.78 2 5 -4 360.91 8.63 2 5 -4 359.47 7.97 2 -5 -4 358.80 8.69 -2 -5 4 355.20 7.92 -2 5 4 350.06 7.90 -2 5 3 297.65 7.12 2 -5 -3 289.37 7.27 -2 -5 3 289.28 7.10 2 5 -3 291.42 6.81 2 5 -3 286.90 6.47 2 5 -3 294.53 7.22 -2 5 3 295.79 6.81 -2 5 3 294.83 6.60 -2 -5 3 292.74 6.51 -2 5 3 294.29 7.31 -2 -5 3 288.46 6.53 2 -5 -3 295.55 7.22 2 5 -3 292.42 6.59 -2 5 3 290.45 7.22 -2 -5 3 299.07 6.90 -2 -5 2 124.34 3.04 2 5 -2 124.67 3.25 -2 5 2 134.26 3.48 -2 5 2 137.20 3.48 -2 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12 -2 32.57 1.74 -2 -12 2 31.52 1.11 2 -12 -1 28.41 1.64 -2 12 1 28.38 1.49 -2 -12 1 27.72 1.18 -2 12 1 28.35 1.46 -2 -12 1 28.49 1.07 -2 -12 1 26.95 1.39 -2 -12 1 28.32 1.00 -2 12 1 29.44 1.74 2 -12 -1 27.48 1.37 -2 12 1 29.75 1.67 2 12 -1 27.58 1.42 2 -12 -1 28.65 1.42 -2 -12 1 30.63 1.56 -2 12 1 31.94 2.15 -2 12 1 31.98 2.04 2 12 -1 28.95 1.72 -2 -12 0 120.44 3.63 -2 12 0 123.79 3.56 -2 12 0 115.12 3.90 2 -12 0 114.99 3.34 -2 12 0 120.68 3.97 -2 12 0 129.23 4.63 2 -12 0 121.07 3.42 -2 -12 0 123.77 3.81 -2 12 0 111.44 4.19 -2 -12 0 117.39 3.11 -2 -12 0 118.43 3.43 2 -12 0 116.03 3.75 -2 -12 0 121.47 3.27 2 12 0 107.97 3.98 -2 12 0 124.52 3.58 -2 12 -1 29.74 1.68 -2 12 -1 27.06 1.30 -2 -12 -1 27.49 1.18 2 -12 1 27.58 1.18 -2 -12 -1 29.24 1.49 -2 -12 -1 29.64 1.50 2 -12 1 26.61 1.19 2 -12 1 30.80 1.55 -2 12 -1 30.80 1.76 2 12 1 25.57 1.82 -2 -12 -1 28.30 1.64 -2 12 -1 27.74 1.87 -2 12 -1 27.93 1.33 2 12 1 28.89 1.83 -2 -12 -1 26.48 1.29 -2 -12 -2 75.94 2.60 -2 12 -2 78.50 2.88 -2 -12 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30.41 2.16 -2 -13 7 33.79 1.47 2 13 -7 29.48 1.67 -2 13 6 41.23 1.93 2 -13 -6 36.76 2.03 2 13 -6 37.78 2.38 -2 13 6 41.58 2.25 2 -13 -6 36.17 2.31 -2 -13 6 40.19 1.65 2 13 -6 40.70 1.62 2 13 -6 37.69 1.89 -2 -13 6 38.71 1.70 2 -13 -5 7.03 1.26 -2 13 5 6.08 1.32 -2 13 5 7.34 1.07 -2 13 5 7.28 0.91 2 -13 -5 7.03 0.97 2 -13 -5 9.00 0.89 2 13 -5 7.66 0.75 -2 -13 5 7.96 0.83 -2 -13 5 7.34 0.77 2 13 -5 5.71 1.19 2 13 -5 6.40 0.96 2 -13 -4 95.90 3.78 2 -13 -4 104.25 3.52 -2 13 4 104.32 3.90 2 -13 -4 100.66 3.28 2 13 -4 105.17 3.13 -2 -13 4 105.20 3.22 2 13 -4 100.55 4.03 -2 -13 4 105.43 3.21 -2 13 4 102.76 3.52 -2 13 4 102.80 3.64 2 13 -4 104.91 3.54 -2 13 4 101.60 4.27 -2 13 3 55.02 2.32 -2 -13 3 51.39 2.01 -2 -13 3 50.25 2.00 2 -13 -3 47.67 2.08 2 13 -3 46.77 1.89 2 -13 -3 45.66 2.03 2 13 -3 48.54 2.61 -2 13 3 51.05 2.25 2 -13 -3 48.77 2.40 -2 13 3 46.94 2.43 2 13 -3 50.36 2.27 -2 13 3 50.45 2.77 -2 -13 2 31.02 1.12 -2 -13 2 31.49 1.53 -2 13 2 32.77 1.94 2 -13 -2 30.93 1.53 -2 13 2 30.49 1.73 -2 -13 2 29.58 0.79 2 -13 -2 34.81 1.65 -2 13 2 30.12 1.62 -2 -13 2 32.16 1.59 -2 -13 2 26.83 0.76 2 13 -2 31.50 2.09 2 -13 -2 32.99 1.86 -2 13 2 31.10 2.19 2 13 -2 30.95 1.80 -2 13 1 52.34 2.10 -2 13 1 51.75 2.39 2 -13 -1 47.01 1.90 -2 -13 1 49.68 1.49 -2 13 1 50.99 2.35 2 -13 -1 48.92 2.25 2 -13 -1 50.54 2.00 -2 -13 1 51.96 2.07 -2 13 1 50.01 2.06 -2 -13 1 50.27 2.15 -2 -13 1 49.66 1.74 -2 -13 1 50.00 1.58 -2 13 1 49.30 2.69 2 13 -1 51.88 2.42 -2 13 0 140.51 4.07 -2 -13 0 139.19 3.63 -2 -13 0 142.85 4.21 -2 13 0 143.51 4.52 -2 13 0 147.35 4.14 -2 -13 0 137.64 3.77 2 -13 0 138.19 3.92 -2 13 0 150.39 4.64 2 -13 0 145.84 3.97 2 -13 0 147.07 4.39 2 13 0 138.14 4.90 -2 -13 0 154.71 4.46 -2 -13 0 139.52 3.97 -2 13 0 135.65 4.88 2 13 0 145.74 4.76 -2 -13 -1 121.81 3.66 -2 13 -1 116.88 3.45 -2 -13 -1 112.74 3.22 2 -13 1 117.70 3.28 -2 -13 -1 115.06 3.66 -2 13 -1 120.05 4.12 -2 13 -1 119.16 3.90 2 -13 1 118.64 3.26 2 13 1 112.74 4.32 -2 13 -1 113.36 4.29 -2 -13 -1 118.27 3.40 2 -13 1 120.22 3.73 2 13 1 117.58 4.26 -2 13 -1 116.96 3.43 2 -13 2 32.16 1.61 -2 13 -2 34.04 1.99 -2 13 -2 31.83 1.38 2 -13 2 30.05 1.19 -2 -13 -2 29.86 1.36 2 13 2 29.59 2.08 2 -13 2 31.10 1.22 -2 -13 -2 31.75 1.65 -2 -13 -2 29.16 1.67 -2 13 -2 33.91 1.81 -2 13 -2 26.56 1.93 -2 13 -2 29.54 1.33 -2 -13 -2 28.88 1.47 2 13 2 31.10 2.06 2 13 3 0.26 0.91 -2 13 -3 0.83 0.44 -2 -13 -3 0.55 0.64 -2 -13 -3 0.31 0.56 2 13 3 1.02 0.88 -2 13 -3 0.20 0.41 -2 -13 -3 1.34 0.78 2 -13 3 0.43 0.32 2 -13 3 0.64 0.29 -2 13 -3 0.32 0.73 -2 -13 -3 0.11 0.47 -2 13 -3 1.23 0.78 -2 13 -3 1.16 0.86 2 13 4 30.62 2.12 -2 -13 -4 27.66 1.47 -2 13 -4 26.69 1.89 2 -13 4 27.52 0.98 -2 -13 -4 28.80 1.84 2 13 4 31.07 2.22 2 -13 4 28.10 0.95 -2 13 -4 27.64 1.94 -2 13 -4 27.11 1.62 -2 13 -4 29.11 1.18 -2 13 -5 59.72 2.45 -2 -13 -5 65.34 2.92 2 13 5 59.48 3.24 2 13 5 61.79 3.08 2 -13 5 58.70 1.62 -2 -13 -5 62.63 2.42 -2 13 -5 57.88 2.85 -2 13 -5 61.67 1.86 -2 -13 -6 10.66 1.04 2 13 6 9.55 1.60 2 -13 6 9.08 0.45 -2 -13 -6 8.51 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1.40 -2 -14 1 23.14 0.96 -2 14 1 24.20 1.42 -2 14 1 23.09 1.92 2 14 -1 22.67 1.71 2 -14 0 45.69 2.13 -2 -14 0 44.25 1.80 -2 14 0 49.15 2.35 -2 -14 0 44.57 2.00 -2 14 0 43.01 1.87 -2 14 0 43.86 1.93 -2 -14 0 44.83 1.52 2 -14 0 44.87 1.78 -2 14 0 46.29 2.35 2 -14 0 46.95 1.78 2 14 0 48.90 2.64 -2 -14 0 45.74 1.67 -2 14 0 44.11 2.57 2 14 0 46.41 2.46 2 -14 1 27.98 1.60 -2 -14 -1 29.15 1.57 -2 14 -1 30.45 1.82 -2 14 -1 33.89 1.53 2 14 1 26.93 2.05 -2 -14 -1 29.07 1.28 2 -14 1 31.72 1.36 2 -14 1 32.91 1.33 -2 -14 -1 34.90 1.71 -2 14 -1 29.72 1.91 -2 14 -1 26.60 2.04 -2 -14 -1 29.73 1.43 -2 14 -1 28.13 1.40 2 14 1 31.24 2.08 -2 14 -2 14.50 0.95 2 14 2 15.33 1.62 2 14 2 13.31 1.56 -2 -14 -2 15.46 1.29 -2 14 -2 16.39 1.04 -2 -14 -2 14.37 1.17 2 -14 2 13.96 0.79 -2 -14 -2 14.43 0.94 -2 14 -2 14.19 1.43 -2 14 -2 17.04 1.37 2 -14 2 14.91 1.16 2 -14 2 16.40 0.89 -2 14 -2 16.09 1.60 -2 -14 -2 16.02 1.13 -2 14 -3 5.23 0.59 2 14 3 5.45 1.23 -2 -14 -3 5.23 0.70 -2 -14 -3 5.67 0.87 2 -14 3 4.72 0.44 -2 14 -3 4.43 0.96 -2 -14 -3 4.71 0.95 -2 14 -3 3.83 1.02 2 14 3 4.93 1.26 2 -14 3 5.55 0.51 -2 14 -3 7.41 1.27 -2 -14 -4 1.45 0.84 2 14 4 2.66 1.07 -2 -14 -4 2.28 0.66 -2 -14 -4 1.75 0.68 2 -14 4 1.64 0.29 -2 14 -4 1.72 0.42 2 -14 4 1.53 0.30 -2 14 -4 2.26 0.96 -2 14 -4 1.50 0.81 -2 14 -4 1.26 0.96 2 14 4 0.76 1.08 -2 -14 -5 1.96 0.68 -2 14 -5 2.20 0.85 -2 -14 -5 1.72 0.92 2 -14 5 1.46 0.24 2 14 5 2.29 1.09 -2 14 -5 1.89 1.02 2 14 5 2.95 1.37 -2 -14 -6 20.20 1.78 -2 -14 -6 21.52 1.43 2 14 6 21.77 2.17 2 14 6 17.89 1.86 -2 14 -6 20.21 1.84 -2 -14 -7 23.24 1.59 -2 -14 -7 22.86 1.66 -2 14 -7 22.08 2.01 2 14 7 22.61 2.13 2 14 7 24.55 2.40 -2 14 -7 26.22 2.04 -2 -14 -7 28.74 2.17 -2 14 -8 16.63 1.82 2 14 8 14.53 2.03 -2 -14 -8 14.19 1.39 -2 -14 -8 11.86 1.30 2 14 8 12.97 1.81 -2 14 -8 14.33 1.64 2 14 9 31.49 2.80 2 14 9 30.14 2.45 -2 -14 -9 29.17 1.94 -2 14 -9 32.20 2.47 -2 -14 -9 28.14 1.92 -2 14 -9 32.46 2.30 -2 14 -10 10.65 1.59 2 14 10 6.99 1.61 2 15 -9 33.92 2.48 2 -15 -9 33.08 2.12 2 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3.74 -4 3 -7 160.25 4.55 -4 3 -7 162.55 5.04 4 3 7 160.31 5.79 4 -3 8 18.63 0.77 4 3 8 20.50 1.23 -4 -3 -8 21.23 1.18 -4 -3 -8 20.34 1.40 -4 3 -8 17.87 0.76 -4 3 -8 20.12 1.32 -4 3 -8 21.74 1.63 4 3 8 16.74 1.98 4 3 9 28.39 2.52 -4 -3 -9 27.64 1.41 -4 -3 -9 28.58 1.72 -4 3 -9 26.71 0.97 -4 3 -9 28.94 1.63 4 -3 9 26.08 2.54 -4 -3 -9 25.88 1.95 -4 3 -9 27.14 1.92 -4 -3 -10 6.16 1.30 4 3 10 6.92 1.67 -4 -3 -10 6.37 0.79 -4 -3 -10 3.86 0.91 -4 3 -10 4.34 0.87 -4 -3 -10 5.17 1.25 -4 3 -10 5.17 1.15 4 -3 10 6.11 1.69 4 -3 11 -0.46 1.63 -4 -3 -11 1.64 0.66 -4 -3 -11 1.91 0.88 -4 3 -11 2.15 0.80 4 3 11 2.71 1.54 -4 -3 -11 1.33 0.99 -4 3 -11 1.81 1.09 -4 -3 -12 58.41 2.77 4 -3 12 56.21 3.96 -4 3 -12 53.60 2.59 4 3 12 58.42 3.81 -4 -3 -12 57.43 3.20 -4 3 -12 60.88 3.18 4 3 13 13.40 2.33 -4 3 -13 21.21 1.73 -4 4 14 7.34 1.55 4 4 -14 11.72 1.44 -4 4 13 12.67 1.65 4 4 -13 14.62 1.53 4 -4 -13 13.62 1.56 4 -4 -12 2.94 1.12 -4 4 12 2.91 1.05 4 4 -12 3.03 1.01 -4 4 12 3.51 1.25 4 4 -12 3.85 0.84 4 -4 -12 3.13 0.95 4 4 -11 10.84 0.98 4 -4 -11 10.45 1.44 -4 4 11 14.69 1.56 -4 4 11 11.83 1.42 4 4 -11 11.96 1.28 4 -4 -11 8.56 1.18 4 4 -11 12.09 1.06 -4 4 10 31.84 2.05 -4 4 10 32.22 2.01 4 -4 -10 28.43 1.99 -4 -4 10 29.05 1.56 4 -4 -10 28.08 1.85 4 4 -10 32.95 1.62 4 4 -10 30.55 1.20 4 4 -10 31.31 1.58 4 4 -10 29.12 1.88 4 4 -10 28.26 1.45 4 4 -9 15.29 0.99 -4 4 9 16.56 1.50 4 -4 -9 14.05 1.41 -4 4 9 14.00 1.38 -4 4 9 15.14 1.42 4 -4 -9 14.05 1.30 4 4 -9 13.59 1.36 -4 -4 9 13.40 1.06 4 4 -9 14.29 1.09 -4 -4 9 13.07 1.17 4 4 -9 13.93 0.72 4 4 -9 15.86 1.10 4 4 -9 15.39 0.82 4 -4 -9 14.57 1.24 -4 4 8 27.59 1.75 -4 4 8 27.13 1.75 4 4 -8 27.73 1.24 -4 4 8 27.23 1.80 4 -4 -8 25.45 1.69 -4 -4 8 29.64 1.65 4 -4 -8 29.44 1.83 4 4 -8 30.45 1.53 4 4 -8 28.34 1.41 4 4 -8 29.47 0.95 -4 -4 8 31.48 1.49 4 -4 -8 30.06 1.63 4 4 -8 29.65 1.02 4 4 -8 31.18 1.86 -4 4 7 58.30 2.46 4 4 -7 58.72 1.79 4 -4 -7 63.20 2.56 -4 -4 7 58.38 2.03 4 -4 -7 52.58 2.38 -4 4 7 57.32 2.49 -4 -4 7 61.62 2.34 4 4 -7 56.67 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4 -3 28.00 1.14 -4 -4 3 26.63 1.33 4 -4 -3 28.29 1.29 4 -4 -3 26.41 1.40 4 -4 -3 26.21 1.39 -4 -4 3 27.67 1.23 4 -4 -3 25.91 1.29 -4 4 3 27.94 1.50 -4 4 3 27.31 1.09 -4 4 3 29.30 1.44 4 4 -3 25.43 1.42 4 4 -2 21.51 1.06 4 4 -2 23.18 0.99 -4 4 2 22.47 1.12 -4 -4 2 22.17 1.14 4 -4 -2 22.20 1.08 -4 4 2 20.47 1.09 -4 -4 2 22.20 1.08 -4 -4 2 19.56 1.18 4 -4 -2 22.66 1.24 -4 -4 2 22.27 0.65 -4 -4 2 20.12 0.84 4 -4 -2 20.72 1.12 -4 4 2 20.48 1.25 4 -4 -2 21.87 1.20 -4 4 2 22.45 1.22 -4 -4 2 21.31 0.70 4 4 -2 23.90 1.37 -4 -4 1 382.13 8.74 -4 -4 1 380.71 8.70 4 4 -1 383.96 9.60 -4 -4 1 380.74 9.09 4 4 -1 379.22 8.97 4 4 -1 392.33 8.86 4 -4 -1 371.50 8.89 -4 -4 1 368.94 8.97 -4 4 1 382.37 9.00 -4 4 1 383.68 9.29 -4 -4 1 382.33 8.58 4 -4 -1 384.24 9.47 -4 4 1 387.15 9.34 -4 -4 1 391.52 9.37 4 -4 -1 392.44 9.12 4 -4 -1 393.40 9.23 -4 4 1 396.09 9.29 4 -4 0 300.69 7.35 4 4 0 301.35 7.85 4 4 0 303.03 7.07 -4 -4 0 307.64 7.26 4 -4 0 296.96 6.97 -4 -4 0 296.32 7.18 4 -4 0 309.08 7.89 -4 4 0 306.37 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0.81 -4 4 -3 19.76 1.22 -4 -4 -3 20.96 1.40 -4 -4 -3 23.81 1.53 -4 -4 -4 30.57 1.82 4 4 4 30.10 1.88 4 4 4 30.79 1.42 -4 4 -4 28.73 1.49 4 4 4 30.85 1.35 4 -4 4 31.21 0.92 4 -4 4 30.77 1.33 -4 -4 -4 28.50 1.33 -4 4 -4 29.87 1.45 -4 4 -4 29.78 0.96 4 -4 4 31.23 1.59 4 -4 4 30.10 2.13 -4 4 -4 27.97 1.59 -4 -4 -4 32.83 1.85 -4 4 -5 27.10 1.45 4 4 5 31.79 2.03 -4 -4 -5 26.96 1.78 4 4 5 25.86 1.38 4 -4 5 27.18 0.82 4 4 5 26.97 1.31 4 -4 5 28.38 1.31 -4 -4 -5 27.97 1.32 -4 4 -5 28.38 1.43 -4 4 -5 28.99 0.88 4 -4 5 31.31 1.61 -4 -4 -5 28.47 1.79 -4 4 -5 30.07 1.68 4 -4 5 30.23 2.23 -4 4 -5 27.14 1.95 4 4 6 33.11 2.24 4 -4 6 29.06 0.85 4 4 6 33.17 1.52 4 -4 6 33.37 1.46 -4 -4 -6 34.54 1.50 -4 -4 -6 32.47 1.65 -4 4 -6 30.91 1.55 -4 4 -6 31.89 0.91 4 4 6 33.35 2.30 -4 4 -6 33.10 1.87 4 -4 6 34.56 2.57 4 4 7 24.45 1.36 -4 -4 -7 23.08 1.47 -4 -4 -7 22.70 1.26 -4 4 -7 25.71 1.42 -4 4 -7 24.10 0.74 -4 4 -7 25.87 1.72 4 4 7 26.99 2.19 -4 -4 -8 153.77 4.31 -4 -4 -8 141.65 4.58 -4 4 -8 151.81 4.47 -4 4 -8 137.49 3.39 -4 4 -8 165.21 3.48 -4 4 -8 148.96 4.99 4 4 8 151.67 5.78 -4 -4 -9 3.00 1.12 -4 -4 -9 1.20 0.57 -4 -4 -9 1.32 0.72 -4 4 -9 1.83 0.69 -4 4 -9 0.72 0.88 4 4 9 1.65 1.23 4 -4 9 1.68 1.32 4 4 10 0.78 1.35 -4 -4 -10 0.88 1.01 4 -4 10 3.81 1.54 -4 -4 -10 1.48 0.64 -4 -4 -10 2.44 0.83 -4 4 -10 2.57 0.77 -4 -4 -10 0.14 0.91 -4 4 -10 2.98 1.02 4 4 11 7.45 1.74 -4 -4 -11 8.14 0.93 -4 -4 -11 6.85 1.16 -4 4 -11 8.17 1.07 4 -4 11 9.27 2.07 -4 -4 -11 8.06 1.41 -4 4 -11 7.94 1.39 4 4 12 43.36 3.37 -4 -4 -12 47.95 2.12 -4 4 -12 46.31 2.32 4 -4 12 50.86 3.79 -4 -4 -12 43.13 2.42 -4 4 -12 46.01 2.80 4 4 13 -0.45 1.64 -4 4 -13 0.73 0.82 -4 5 14 3.38 1.37 -4 5 13 2.74 1.35 4 5 -13 1.83 0.92 4 -5 -13 0.90 0.94 4 -5 -12 18.66 1.85 -4 5 12 23.55 2.03 -4 5 12 19.70 1.81 4 5 -12 23.04 1.74 4 -5 -12 22.57 1.78 4 5 -11 3.64 0.72 4 -5 -11 3.36 0.97 -4 5 11 3.05 1.07 -4 5 11 3.85 1.09 4 -5 -11 3.91 1.10 4 5 -11 3.12 0.83 4 -5 -10 3.78 1.09 -4 5 10 5.29 1.13 -4 5 10 4.45 1.05 4 -5 -10 4.26 0.96 4 5 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190.63 6.18 5 -4 3 187.70 6.27 -5 4 -3 186.43 4.62 -5 4 -3 188.65 5.29 -5 4 -3 182.16 5.85 -5 -4 -3 190.20 5.19 5 -4 3 192.69 5.28 -5 4 -3 181.97 5.40 -5 4 -3 195.53 5.32 -5 -4 -3 186.75 5.70 -5 4 -4 154.22 4.72 5 4 4 159.72 4.41 5 -4 4 164.00 3.92 5 -4 4 164.80 4.47 -5 -4 -4 167.54 4.54 5 4 4 163.92 5.73 -5 -4 -4 164.94 5.17 -5 4 -4 165.67 4.03 5 -4 4 158.29 5.80 -5 4 -4 169.53 4.80 -5 -4 -4 161.77 4.78 -5 4 -5 109.18 3.58 5 -4 5 109.04 2.70 5 4 5 107.52 3.27 -5 -4 -5 107.72 3.32 -5 4 -5 109.27 3.55 -5 4 -5 107.79 2.78 5 -4 5 113.73 4.78 -5 -4 -5 105.86 3.69 -5 4 -6 13.70 1.20 5 -4 6 12.21 0.55 5 -4 6 13.75 1.88 -5 -4 -6 14.51 1.03 -5 -4 -6 13.79 1.16 -5 4 -6 13.17 0.61 -5 4 -6 12.09 1.10 -5 -4 -6 13.24 1.26 -5 4 -6 14.31 1.33 5 -4 7 40.64 1.18 -5 -4 -7 47.19 1.92 -5 -4 -7 46.04 2.20 -5 4 -7 46.68 2.13 -5 4 -7 45.67 1.29 -5 -4 -7 45.21 2.36 -5 4 -7 43.13 2.37 5 -4 7 53.27 3.36 5 4 7 49.22 3.09 -5 -4 -8 18.82 1.24 -5 -4 -8 20.20 1.47 -5 4 -8 18.02 1.37 -5 -4 -8 18.19 1.63 5 4 8 20.63 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6.82 1.46 5 11 9 48.92 3.55 -5 -11 -9 55.95 2.75 -5 -11 -9 56.73 2.64 5 11 9 60.74 3.87 -5 11 -9 58.14 3.25 -5 -12 11 18.64 1.58 5 12 -11 12.41 1.69 -5 12 10 25.69 2.41 -5 -12 10 25.72 1.80 5 12 -10 24.55 2.11 -5 12 9 3.73 1.33 -5 12 9 2.79 1.19 5 -12 -9 4.70 1.14 -5 -12 9 2.72 0.90 5 12 -9 1.89 1.10 -5 12 8 5.63 1.48 -5 12 8 9.97 1.46 5 -12 -8 6.53 1.16 -5 -12 8 8.23 1.08 5 12 -8 9.70 1.47 5 12 -7 22.64 1.95 -5 12 7 18.71 2.02 -5 12 7 18.30 1.75 5 -12 -7 17.78 1.60 -5 -12 7 20.84 1.51 -5 12 6 15.65 1.75 5 12 -6 14.42 1.68 5 -12 -6 15.72 1.65 -5 12 6 13.13 1.53 5 -12 -6 13.18 1.38 -5 -12 6 13.41 1.27 -5 12 6 12.85 0.67 5 12 -5 4.33 1.16 -5 12 5 3.65 1.09 -5 -12 5 2.38 0.24 -5 -12 5 3.14 0.27 5 -12 -5 3.28 0.85 -5 -12 5 4.05 0.86 -5 12 5 3.87 0.69 -5 12 5 3.56 0.55 -5 12 5 2.71 1.14 -5 12 4 -0.12 0.85 5 12 -4 1.46 1.03 5 -12 -4 0.09 0.67 -5 -12 4 0.09 0.64 -5 -12 4 0.11 0.24 -5 12 4 0.56 0.48 -5 12 4 0.46 0.68 -5 -12 4 0.55 0.34 -5 12 4 0.15 1.00 -5 12 3 33.43 1.90 5 12 -3 32.32 1.49 5 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13 -2 27.10 2.23 -5 13 2 28.40 1.89 5 -13 -1 33.38 2.02 5 13 -1 31.22 1.80 -5 -13 1 29.89 1.14 5 -13 -1 33.19 1.59 -5 13 1 29.86 1.75 -5 -13 1 30.84 1.83 -5 -13 1 33.48 1.45 -5 -13 1 35.17 1.60 -5 13 1 31.73 1.95 5 13 -1 32.88 2.39 5 -13 0 27.54 1.82 5 13 0 26.61 1.80 -5 -13 0 28.16 1.31 5 13 0 24.11 2.16 5 -13 0 26.67 1.33 -5 13 0 29.07 1.77 -5 -13 0 28.13 1.73 -5 -13 0 25.16 1.34 5 -13 0 28.54 1.33 -5 -13 0 26.97 1.55 -5 13 0 26.74 1.78 5 -13 1 42.30 2.21 5 13 1 42.63 2.36 -5 -13 -1 43.86 1.88 -5 13 -1 43.85 2.28 5 -13 1 41.66 1.59 -5 -13 -1 44.02 1.88 5 -13 1 43.07 1.60 5 13 1 44.12 2.86 -5 13 -1 40.28 2.14 -5 13 -1 42.58 2.62 5 13 2 53.29 2.77 -5 -13 -2 47.21 2.17 -5 13 -2 52.11 2.59 5 -13 2 48.99 1.57 -5 -13 -2 50.07 2.09 -5 13 -2 47.59 2.31 -5 13 -2 53.85 2.94 -5 -13 -3 19.86 1.49 5 13 3 20.96 1.89 5 -13 3 18.34 0.63 -5 -13 -3 20.82 1.54 -5 -13 -3 21.35 1.35 -5 13 -3 19.06 1.69 5 13 3 18.75 2.00 -5 13 -3 20.79 1.50 -5 13 -3 21.74 1.92 5 13 4 16.21 1.88 -5 -13 -4 15.19 1.47 -5 -13 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17.06 1.42 -5 14 5 14.64 1.04 5 -14 -4 42.73 2.15 -5 -14 4 42.81 2.21 -5 14 4 44.42 1.93 5 14 -4 38.84 2.71 -5 14 4 41.00 2.77 -5 14 4 45.63 2.48 5 -14 -3 36.17 2.23 5 -14 -3 34.46 1.84 -5 -14 3 36.51 2.01 -5 14 3 36.80 1.83 5 14 -3 34.50 2.57 -5 14 3 38.69 2.62 -5 14 3 39.20 2.27 5 -14 -2 29.81 2.00 5 -14 -2 28.28 1.59 -5 -14 2 27.85 1.77 -5 14 2 30.30 1.74 -5 -14 2 25.86 1.16 5 14 -2 30.08 2.41 -5 14 2 29.44 1.94 5 -14 -1 2.75 0.96 -5 -14 1 2.30 0.38 5 14 -1 3.35 0.90 5 14 -1 1.71 1.22 5 -14 -1 2.51 0.65 -5 -14 1 3.51 0.83 -5 14 1 3.99 1.01 -5 14 1 2.67 0.90 -5 -14 1 3.08 0.57 -5 14 0 13.70 1.37 5 -14 0 12.60 1.34 -5 -14 0 13.10 0.92 5 14 0 12.97 1.38 5 14 0 13.43 1.78 5 -14 0 12.06 0.94 -5 -14 0 14.38 1.29 -5 -14 0 12.94 0.98 -5 14 0 12.07 1.31 -5 14 0 10.75 1.62 -5 14 -1 9.13 1.14 5 -14 1 11.09 1.27 -5 -14 -1 8.12 0.89 5 14 1 6.99 1.27 5 -14 1 8.60 0.73 -5 -14 -1 9.27 1.15 -5 14 -1 9.36 1.24 -5 -14 -1 8.59 0.89 -5 14 -1 8.97 1.53 -5 -14 -2 8.91 1.05 5 14 2 10.63 1.53 5 -14 2 10.02 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1.99 -8 5 3 23.68 1.68 -8 5 3 22.43 1.45 8 -5 -2 39.95 2.13 -8 -5 2 41.24 1.81 -8 5 2 41.02 2.06 8 5 -2 42.53 2.65 -8 -5 2 38.96 2.15 -8 5 2 39.09 2.02 -8 -5 2 39.68 2.16 8 -5 -2 42.79 2.48 -8 5 2 38.36 2.36 -8 -5 2 37.13 1.33 -8 5 2 38.99 2.14 -8 -5 2 40.37 1.45 -8 -5 1 114.34 3.47 -8 -5 1 119.54 3.69 8 5 -1 125.31 4.96 -8 -5 1 117.41 4.14 -8 5 1 121.94 3.92 -8 -5 1 121.01 4.16 8 -5 -1 121.99 4.73 -8 5 1 118.89 4.46 -8 -5 1 115.58 3.31 -8 5 1 122.58 4.19 -8 -5 0 149.15 4.44 -8 -5 0 152.16 4.46 8 5 0 150.17 5.77 -8 -5 0 151.22 4.85 -8 5 0 156.67 4.59 -8 -5 0 149.48 4.89 8 -5 0 146.35 5.66 -8 5 0 152.12 5.23 -8 -5 0 148.87 4.21 -8 5 0 149.94 4.95 8 5 1 10.17 1.70 -8 -5 -1 12.62 1.17 -8 -5 -1 12.20 1.21 8 -5 1 12.76 1.81 -8 -5 -1 10.46 1.17 -8 5 -1 11.49 1.03 -8 -5 -1 10.17 1.20 -8 -5 -1 9.27 0.95 -8 5 -1 11.80 1.43 -8 5 -1 10.79 1.30 8 5 2 1.74 1.31 8 -5 2 0.38 1.27 8 -5 2 0.19 0.44 -8 -5 -2 0.09 0.69 -8 5 -2 -0.14 0.56 -8 -5 -2 -0.43 0.77 -8 -5 -2 0.15 0.62 -8 5 -2 0.12 0.89 -8 5 -2 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1.84 -8 6 6 5.31 1.08 8 -6 -6 4.64 1.03 8 -6 -6 5.65 1.24 8 6 -6 3.38 1.12 -8 -6 6 6.42 1.05 8 -6 -5 17.27 1.53 -8 6 5 15.80 0.81 8 -6 -5 16.15 1.56 -8 -6 5 18.91 1.60 8 6 -5 11.60 1.59 -8 -6 5 15.84 1.42 -8 6 5 16.29 1.82 -8 6 5 14.41 1.43 8 -6 -4 35.01 2.10 -8 -6 4 40.09 1.61 8 -6 -4 35.64 2.15 8 6 -4 34.20 2.39 -8 -6 4 40.50 2.26 -8 -6 4 41.76 2.19 -8 6 4 38.47 2.42 -8 6 4 36.32 2.15 8 -6 -3 13.45 1.34 -8 -6 3 15.05 1.06 8 -6 -3 14.98 1.50 8 -6 -3 14.66 1.39 -8 6 3 14.37 1.19 -8 -6 3 15.34 1.45 8 6 -3 14.42 1.72 -8 -6 3 16.63 1.45 -8 6 3 12.75 1.55 -8 6 3 13.09 1.41 8 -6 -2 49.02 2.66 8 -6 -2 45.33 2.30 -8 -6 2 45.79 1.88 -8 6 2 44.62 2.16 8 6 -2 42.93 2.75 -8 -6 2 50.50 2.46 -8 -6 2 50.57 2.38 -8 6 2 43.61 2.57 -8 -6 2 41.61 1.36 -8 6 2 42.14 2.32 -8 -6 2 43.10 1.42 -8 -6 1 11.47 0.90 -8 -6 1 13.28 1.07 -8 -6 1 13.85 1.34 -8 6 1 12.86 1.17 8 -6 -1 14.42 1.75 -8 -6 1 12.09 0.82 -8 -6 1 11.79 1.28 8 6 -1 12.15 1.75 -8 6 1 13.55 1.52 -8 6 1 11.49 1.37 -8 -6 0 68.95 2.56 8 6 0 74.62 3.80 -8 -6 0 74.69 3.07 -8 -6 0 72.27 3.00 -8 6 0 73.33 2.69 -8 -6 0 67.44 2.37 -8 6 0 65.38 3.17 -8 6 0 74.88 3.21 8 -6 0 72.22 3.69 -8 -6 0 70.81 2.59 -8 -6 -1 28.90 1.69 -8 -6 -1 29.06 1.60 -8 -6 -1 26.87 1.79 8 -6 1 29.10 2.50 -8 -6 -1 26.69 1.79 -8 6 -1 31.25 1.58 -8 -6 -1 30.26 1.53 -8 6 -1 29.46 2.07 -8 6 -1 27.76 1.96 8 6 1 24.92 2.41 8 6 2 1.96 1.33 8 -6 2 1.61 0.46 8 -6 2 2.54 1.39 -8 -6 -2 0.59 0.72 -8 6 -2 1.55 0.57 -8 -6 -2 1.81 0.90 -8 -6 -2 1.20 0.68 -8 6 -2 -0.38 0.99 -8 6 -2 1.35 0.97 8 6 3 14.93 2.12 -8 -6 -3 12.08 1.25 8 -6 3 13.69 2.07 -8 -6 -3 12.99 1.36 -8 -6 -3 11.72 1.19 -8 6 -3 12.25 1.46 -8 6 -3 15.91 1.61 8 6 4 3.73 1.59 -8 -6 -4 3.55 0.89 8 -6 4 2.47 1.63 -8 -6 -4 3.31 0.97 -8 -6 -4 4.56 0.97 -8 6 -4 3.13 1.06 -8 6 -4 3.85 1.16 8 6 5 1.85 1.53 -8 -6 -5 0.96 0.77 -8 -6 -5 2.83 0.97 8 -6 5 1.91 1.64 -8 -6 -5 2.94 0.95 -8 6 -5 2.64 1.07 -8 6 -5 0.97 1.04 8 6 6 4.37 1.74 -8 -6 -6 4.89 0.99 -8 -6 -6 3.68 1.11 -8 -6 -6 5.31 1.18 -8 6 -6 4.46 1.13 8 -6 6 6.31 1.86 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7 2 1.98 1.00 -8 -7 1 7.61 0.89 8 -7 -1 10.08 1.16 8 -7 -1 10.25 1.63 -8 -7 1 7.45 1.14 -8 -7 1 8.40 1.13 8 7 -1 6.37 1.50 -8 -7 1 8.97 0.69 -8 7 1 7.93 1.31 -8 7 1 10.56 1.39 -8 -7 0 142.06 4.17 8 -7 0 155.06 5.72 8 -7 0 143.80 4.46 8 7 0 147.61 5.74 -8 -7 0 140.52 4.76 -8 -7 0 147.04 4.74 -8 -7 0 136.86 3.96 -8 7 0 143.01 5.10 -8 7 0 152.93 5.06 -8 -7 -1 7.84 0.97 -8 -7 -1 8.32 1.07 8 -7 1 5.94 0.87 -8 -7 -1 6.80 1.09 -8 -7 -1 8.96 1.23 -8 -7 -1 9.10 0.90 -8 7 -1 7.45 1.28 -8 7 -1 6.79 1.23 8 7 1 8.91 1.81 8 -7 1 9.80 1.79 8 -7 2 23.02 1.34 -8 -7 -2 23.99 1.71 -8 -7 -2 25.22 1.77 -8 -7 -2 24.64 1.47 -8 7 -2 22.77 1.85 -8 7 -2 28.69 2.07 8 -7 2 22.08 2.43 8 7 2 21.20 2.31 8 7 3 2.74 1.48 8 -7 3 3.46 0.63 -8 -7 -3 3.72 0.92 -8 -7 -3 2.64 0.93 -8 -7 -3 4.67 0.94 -8 7 -3 3.42 1.13 -8 7 -3 4.95 1.19 8 -7 3 1.94 1.52 8 7 4 21.13 2.54 -8 -7 -4 21.46 1.62 -8 -7 -4 23.36 1.76 -8 -7 -4 21.07 1.57 -8 7 -4 20.63 1.82 -8 7 -4 24.87 2.04 8 -7 4 25.28 2.76 8 -7 5 25.60 2.88 8 7 5 21.29 2.51 -8 -7 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-0.34 0.85 8 8 -2 -0.68 1.16 -8 -8 2 1.44 0.83 -8 8 2 0.55 0.96 -8 8 2 0.75 0.93 -8 -8 1 43.67 1.80 8 -8 -1 49.81 2.26 8 8 -1 40.76 2.82 -8 -8 1 41.29 2.32 -8 -8 1 46.79 2.29 8 -8 -1 45.59 2.77 -8 -8 1 43.50 1.54 -8 8 1 44.18 2.59 -8 8 1 46.44 2.59 -8 -8 0 45.28 1.92 8 -8 0 43.67 2.07 8 8 0 45.52 3.05 -8 -8 0 43.05 2.35 8 -8 0 51.24 3.11 -8 -8 0 47.30 2.33 -8 -8 0 42.96 1.72 -8 8 0 42.09 2.54 -8 8 0 43.26 2.55 -8 -8 -1 3.56 0.77 8 -8 1 4.24 0.82 -8 -8 -1 3.51 0.92 8 -8 1 6.23 1.67 -8 -8 -1 4.61 1.02 -8 -8 -1 3.93 0.71 -8 8 -1 4.44 1.11 8 8 1 3.70 1.47 -8 8 -1 3.87 1.21 8 -8 2 7.82 0.83 8 -8 2 6.57 1.77 -8 -8 -2 9.04 1.18 -8 -8 -2 7.93 1.17 -8 -8 -2 6.55 0.93 -8 8 -2 6.09 1.27 -8 8 -2 6.98 1.35 8 8 2 10.63 1.87 8 -8 3 11.50 0.86 8 -8 3 16.36 2.36 -8 -8 -3 14.13 1.40 -8 -8 -3 11.97 1.38 -8 -8 -3 12.55 1.23 -8 8 -3 13.30 1.53 -8 8 -3 14.17 1.68 8 8 3 15.64 2.10 8 8 4 13.96 2.26 -8 -8 -4 20.73 1.61 8 -8 4 21.44 2.62 -8 -8 -4 22.36 1.75 -8 -8 -4 20.67 1.54 -8 8 -4 20.96 1.82 -8 8 -4 17.57 1.85 8 8 5 -0.47 1.52 -8 -8 -5 0.11 0.79 8 -8 5 1.25 1.80 -8 -8 -5 1.06 0.88 -8 -8 -5 -0.75 0.89 -8 8 -5 0.26 0.99 -8 8 -5 -0.15 1.09 -8 -8 -6 0.64 0.82 -8 -8 -6 1.11 0.92 -8 -8 -6 1.53 0.99 8 -8 6 1.84 1.71 -8 8 -6 0.13 1.05 -8 -8 -7 0.21 0.89 -8 -8 -7 0.51 1.01 -8 8 -7 -0.26 1.06 -8 9 9 1.46 1.20 -8 9 8 1.59 1.14 -8 9 7 1.97 1.25 -8 9 7 0.63 1.13 8 -9 -7 2.03 1.06 8 9 -7 -0.61 1.07 -8 -9 7 1.14 1.01 -8 9 6 23.76 2.10 8 9 -6 29.44 2.31 8 -9 -6 28.13 2.04 -8 -9 6 24.93 1.89 -8 -9 6 26.49 1.62 -8 9 6 27.69 2.20 -8 9 5 10.84 1.60 8 -9 -5 16.37 1.58 8 9 -5 16.79 1.88 -8 -9 5 14.95 1.57 -8 -9 5 14.50 1.33 -8 9 5 14.38 1.64 8 -9 -4 -0.34 0.81 8 9 -4 -0.66 1.12 -8 -9 4 -0.54 0.76 -8 9 4 -0.40 1.06 -8 9 4 -0.73 1.12 -8 9 3 19.01 1.20 8 -9 -3 15.39 1.44 8 9 -3 14.47 1.88 -8 -9 3 20.54 1.64 -8 -9 3 17.20 1.45 -8 9 3 17.92 1.78 -8 9 3 15.95 1.72 -8 -9 2 7.72 0.76 8 -9 -2 7.05 1.08 -8 9 2 8.35 0.98 -8 -9 2 8.80 1.16 8 9 -2 6.53 1.51 -8 -9 2 6.89 1.06 -8 9 2 9.14 1.42 -8 9 2 6.60 1.38 8 -9 -1 8.01 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10 -1 3 1.44 1.65 -10 -1 -3 3.44 0.97 -10 -1 -3 2.79 1.04 -10 1 -3 1.32 1.01 10 1 3 2.64 1.62 -10 -1 -4 5.72 1.22 -10 1 -4 3.57 1.19 -10 -1 -5 5.73 1.31 -10 1 -5 5.52 1.45 -10 -2 7 1.85 1.18 -10 -2 6 1.56 1.18 -10 -2 5 61.19 3.05 -10 2 5 55.96 2.95 -10 -2 5 57.22 3.08 -10 2 5 58.06 3.24 -10 -2 4 4.44 1.19 -10 2 4 3.06 1.11 -10 -2 4 2.81 1.24 -10 2 4 5.35 1.47 10 2 -3 19.86 2.08 -10 -2 3 21.25 1.84 -10 2 3 21.23 1.83 -10 -2 3 22.40 1.99 -10 2 3 21.29 1.53 -10 2 3 21.48 2.00 10 -2 -2 14.54 1.91 10 2 -2 12.19 1.85 -10 -2 2 15.62 1.56 -10 2 2 15.37 1.58 -10 -2 2 14.60 1.66 -10 2 2 14.25 1.73 -10 2 2 14.38 1.34 10 -2 -1 13.87 2.01 10 2 -1 14.14 2.03 -10 -2 1 14.68 1.51 -10 2 1 16.67 1.58 -10 -2 1 14.94 1.77 -10 2 1 15.20 1.45 10 -2 0 16.81 2.26 -10 -2 0 21.09 1.70 10 2 0 18.36 2.28 -10 2 0 18.81 1.58 -10 -2 0 14.96 1.71 -10 -2 0 15.28 1.31 -10 2 0 17.27 1.56 10 -2 1 2.75 1.63 -10 -2 -1 2.10 0.89 -10 2 -1 3.06 1.01 10 2 1 5.61 1.77 -10 -2 -1 2.71 1.18 -10 2 -1 1.22 1.11 -10 -2 -1 2.68 0.87 -10 2 -1 3.00 1.11 10 -2 2 3.16 1.77 -10 -2 -2 4.28 0.98 -10 2 -2 4.27 1.04 10 2 2 4.11 1.76 -10 -2 -2 5.04 1.29 -10 -2 -2 4.15 1.07 -10 2 -2 6.04 1.31 -10 -2 -3 9.38 1.27 10 -2 3 6.93 1.92 -10 -2 -3 7.94 1.23 10 2 3 6.52 1.94 -10 2 -3 6.62 1.31 -10 -2 -4 1.11 0.82 -10 -2 -4 1.51 0.95 -10 2 -4 1.98 1.19 -10 -2 -5 8.19 1.37 -10 -3 8 -0.41 1.24 -10 -3 7 3.32 1.25 -10 -3 6 1.66 1.24 -10 3 5 30.50 2.14 -10 -3 5 29.76 2.23 -10 -3 4 0.53 1.00 -10 3 4 0.87 0.98 -10 -3 4 0.55 1.14 -10 3 4 2.82 1.28 10 3 -3 20.94 2.27 -10 -3 3 18.05 1.68 -10 3 3 16.50 1.65 -10 -3 3 13.04 1.63 -10 3 3 16.49 1.90 -10 3 3 15.79 1.47 10 3 -2 8.31 1.71 -10 -3 2 5.82 1.18 -10 3 2 9.62 1.37 -10 -3 2 8.13 1.41 -10 3 2 6.78 1.14 10 3 -1 6.07 1.74 -10 -3 1 5.64 1.19 -10 3 1 3.93 1.08 10 -3 -1 3.07 1.52 -10 -3 1 4.56 1.25 -10 3 1 4.48 1.11 10 3 0 20.17 2.49 -10 -3 0 21.26 1.71 -10 3 0 20.98 1.66 10 -3 0 18.64 2.38 -10 -3 0 21.93 1.91 -10 3 0 18.09 1.95 -10 3 0 21.21 1.76 10 3 1 33.47 2.93 -10 -3 -1 36.03 2.14 -10 3 -1 33.98 2.02 -10 -3 -1 34.81 2.36 10 -3 1 32.65 2.99 -10 -3 -1 30.60 1.81 -10 3 -1 32.42 2.16 -10 3 -1 27.91 2.26 -10 -3 -2 2.65 0.99 10 3 2 0.23 1.60 -10 -3 -2 0.28 1.08 -10 -3 -2 2.65 0.90 10 -3 2 1.35 1.60 -10 3 -2 1.12 1.06 -10 -3 -3 1.29 0.84 10 3 3 -0.24 1.74 -10 -3 -3 1.87 0.92 -10 3 -3 0.39 1.20 10 -3 3 0.24 1.66 -10 -3 -4 4.91 1.05 -10 -3 -4 5.18 1.16 -10 3 -4 3.69 1.22 -10 -3 -5 3.03 1.16 -10 -4 8 1.46 1.23 -10 -4 7 2.82 1.27 -10 -4 6 3.78 1.19 -10 -4 5 6.47 1.35 10 4 -4 9.82 1.73 -10 -4 4 7.77 1.29 -10 4 4 10.27 1.35 10 4 -3 4.26 1.52 -10 -4 3 5.46 1.20 -10 4 3 6.52 1.22 -10 -4 3 5.11 1.31 -10 4 3 8.08 1.27 10 4 -2 1.90 1.47 -10 -4 2 2.79 1.06 -10 4 2 2.27 1.01 -10 -4 2 2.99 1.22 -10 4 2 1.73 1.19 -10 4 2 3.30 1.06 10 -4 -1 14.71 2.15 10 4 -1 12.21 2.05 -10 -4 1 11.83 1.46 -10 4 1 16.48 1.52 -10 -4 1 15.21 1.66 -10 4 1 13.82 1.80 -10 4 1 14.27 1.53 10 -4 0 -0.20 1.39 10 4 0 2.33 1.64 -10 -4 0 -0.12 0.96 -10 4 0 -0.31 0.89 -10 -4 0 0.14 1.04 -10 4 0 1.10 1.18 -10 4 0 2.01 1.09 10 -4 1 10.78 2.02 10 4 1 6.26 1.92 -10 -4 -1 8.96 1.30 -10 4 -1 9.08 1.16 -10 -4 -1 7.48 1.40 -10 4 -1 8.82 1.43 10 -4 2 12.87 2.14 10 4 2 16.68 2.45 -10 -4 -2 15.09 1.50 -10 -4 -2 15.01 1.40 -10 4 -2 18.34 1.77 10 -4 3 -0.24 1.83 -10 -4 -3 2.55 0.99 -10 -4 -3 1.51 0.91 -10 4 -3 3.40 1.24 -10 -4 -4 1.41 0.85 -10 -4 -4 0.55 0.98 -10 4 -4 2.98 1.34 -10 -4 -5 43.85 2.34 -10 -4 -5 38.91 2.39 -10 -5 8 4.58 1.29 -10 -5 7 2.72 1.21 -10 -5 6 6.81 1.49 10 -5 -5 5.87 1.39 -10 -5 5 5.52 1.26 10 5 -4 5.50 1.48 -10 -5 4 2.51 1.26 -10 5 4 4.67 1.18 10 5 -3 9.10 1.84 -10 -5 3 6.90 1.30 -10 5 3 7.26 1.27 -10 -5 3 6.75 1.39 -10 5 3 7.65 1.33 10 5 -2 4.45 1.58 -10 -5 2 1.95 1.03 -10 5 2 1.00 0.92 -10 -5 2 2.13 1.13 -10 5 2 2.18 1.10 10 5 -1 9.39 1.99 -10 -5 1 11.00 1.42 -10 5 1 14.79 1.44 -10 -5 1 11.12 1.55 -10 5 1 12.18 1.50 10 5 0 9.49 1.98 10 -5 0 5.49 1.79 -10 -5 0 4.68 1.15 -10 5 0 4.44 1.05 -10 -5 0 5.67 1.34 -10 5 0 5.01 1.31 10 -5 1 17.85 2.39 -10 -5 -1 16.43 1.62 -10 -5 -1 15.72 1.77 -10 5 -1 20.61 1.88 10 5 2 -1.90 1.78 10 -5 2 0.68 1.75 -10 -5 -2 0.12 0.90 -10 5 -2 1.09 1.26 10 -5 3 2.92 1.83 -10 -5 -3 2.76 0.93 -10 -5 -3 2.35 0.95 -10 5 -3 2.41 1.21 -10 -5 -4 0.57 0.94 -10 -5 -4 0.11 0.96 -10 -5 -5 0.23 0.98 -10 -6 7 1.99 1.15 -10 -6 6 6.72 1.35 10 -6 -5 0.56 1.04 -10 -6 5 1.67 1.11 10 -6 -4 12.34 1.53 -10 -6 4 14.84 1.66 -10 6 4 13.51 1.60 10 6 -4 13.00 1.92 10 6 -3 4.30 1.51 10 -6 -3 2.89 1.18 -10 -6 3 5.19 1.23 -10 6 3 3.47 1.20 10 6 -2 0.79 1.47 10 -6 -2 1.18 0.96 -10 -6 2 -0.26 1.15 -10 6 2 1.48 1.03 10 6 -1 4.38 1.68 -10 -6 1 6.07 1.19 -10 -6 1 3.16 1.13 -10 6 1 6.00 1.32 10 6 0 0.44 1.57 -10 -6 0 1.77 1.01 10 -6 0 0.79 1.57 -10 -6 0 1.20 1.05 -10 6 0 -0.13 1.09 10 6 1 18.96 2.53 -10 -6 -1 19.04 1.75 10 -6 1 18.22 2.44 -10 -6 -1 19.31 1.82 -10 6 -1 19.44 1.94 -10 -6 -2 3.28 1.05 10 -6 2 2.54 1.80 -10 6 -2 5.60 1.42 10 -6 3 7.85 2.02 -10 -6 -4 0.84 0.95 -10 -6 -5 11.67 1.49 -10 -7 6 9.27 1.45 -10 -7 5 26.08 2.06 10 -7 -4 8.84 1.48 -10 -7 4 8.69 1.41 10 7 -4 5.73 1.62 -10 7 4 6.71 1.36 10 -7 -3 5.23 1.22 -10 -7 3 3.05 1.24 -10 7 3 3.34 1.22 10 7 -3 3.30 1.52 10 -7 -2 0.70 0.94 -10 -7 2 1.68 1.10 -10 7 2 0.79 1.05 10 7 -2 1.42 1.44 10 7 -1 2.12 1.47 10 -7 -1 3.68 1.06 -10 -7 1 1.56 1.12 -10 7 1 3.66 1.29 10 7 0 14.89 2.22 10 -7 0 11.91 1.38 -10 -7 0 13.30 1.68 -10 7 0 12.21 1.70 10 -7 1 17.67 2.40 -10 7 -1 13.40 1.78 10 -7 2 1.63 1.74 -10 -8 5 0.60 1.11 -10 8 5 0.80 1.14 10 -8 -4 3.53 1.17 10 8 -4 2.10 1.51 -10 -8 4 1.35 1.13 -10 8 4 2.16 1.23 10 -8 -3 3.55 1.22 -10 -8 3 1.00 1.07 10 8 -3 1.80 1.45 -10 8 3 1.65 1.21 10 -8 -2 7.65 1.25 -10 -8 2 6.85 1.40 -10 8 2 7.99 1.51 10 8 -2 9.00 2.01 10 -8 -1 4.72 1.09 -10 -8 1 4.73 1.24 -10 8 1 5.62 1.43 -10 -8 0 31.94 2.28 -10 8 0 40.24 2.69 10 -8 2 8.19 2.07 -10 9 5 8.45 1.55 -10 -9 4 8.18 1.42 -10 9 4 7.78 1.58 10 -9 -3 -0.24 0.98 -10 -9 3 0.36 1.00 -10 9 3 0.73 1.24 10 -9 -2 9.70 1.33 -10 -9 2 9.33 1.47 -10 9 2 9.52 1.73 -10 -9 1 6.92 1.34 -10 9 1 7.33 1.65 -10 -9 0 5.26 1.32 10 -9 2 2.82 1.86 10 -10 -3 6.25 1.22 -10 -10 2 5.10 1.29 -10 -10 1 0.87 1.08 -10 -11 1 7.03 1.34 -11 0 1 1.62 1.03 11 0 0 30.36 2.90 -11 0 0 30.01 2.02 -11 0 -1 14.16 1.54 -11 0 -3 4.63 1.19 -11 1 1 3.11 1.21 11 1 -1 2.87 1.77 11 -1 0 4.54 1.74 -11 -1 0 4.98 1.17 -11 1 0 4.99 1.19 11 1 0 2.85 1.75 11 -1 1 7.85 2.08 -11 -1 -1 7.73 1.32 -11 -1 -2 1.36 1.02 -11 1 -2 0.72 1.02 -11 1 -3 0.89 1.11 -11 2 2 4.44 1.27 -11 2 1 12.37 1.52 11 2 -1 9.83 2.01 11 -2 0 10.70 2.20 -11 2 0 15.10 1.61 11 2 0 17.54 2.45 11 -2 1 8.68 2.21 -11 2 -1 8.94 1.51 -11 2 -2 11.14 1.54 -11 3 2 8.53 1.35 11 3 -1 12.16 2.23 -11 3 1 15.05 1.63 11 -3 1 1.59 1.69 -11 3 -1 1.00 1.09 -11 3 -2 0.52 1.14 11 4 -2 2.89 1.61 -11 4 2 1.97 1.06 11 4 -1 2.61 1.57 -11 4 0 0.74 1.08 11 -4 1 6.12 1.81 -11 4 -1 4.47 1.35 11 5 -2 0.84 1.49 -11 5 2 0.12 0.97 -11 5 0 5.26 1.42 11 -6 -1 13.37 1.50 -11 6 1 14.10 1.76 0 0 0 0.00 0.00 TITL MX8954 in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 0.71073 7.999036 14.943058 11.032412 90.0000 95.8287 90.0000 ZERR 25.00 0.000163 0.000271 0.000212 0.0000 0.0020 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 25.00 25.00 25.00 25.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 62610 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.716 _oxdiff_exptl_absorpt_empirical_full_min 0.664 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.40466(17) 0.41227(9) 0.62993(10) 0.0396(3) Uani 1 1 d . . . . . O2 O 0.61351(13) 0.45930(7) 0.36789(9) 0.0246(2) Uani 1 1 d . . . . . O3 O 0.79563(15) 0.54713(7) 0.21157(10) 0.0335(2) Uani 1 1 d . . . . . O4 O 0.71088(13) 0.44931(8) 0.06301(9) 0.0316(2) Uani 1 1 d . . . . . N1 N 0.55834(19) 0.53076(10) 0.57976(13) 0.0357(3) Uani 1 1 d . . . . . H1A H 0.541898 0.559435 0.645089 0.043 Uiso 1 1 calc R U . . . H1B H 0.618096 0.554305 0.527571 0.043 Uiso 1 1 calc R U . . . C1 C 0.49178(19) 0.45053(11) 0.55956(13) 0.0272(3) Uani 1 1 d . . . . . C2 C 0.52546(18) 0.40217(10) 0.44379(13) 0.0245(3) Uani 1 1 d . . . . . H2 H 0.417297 0.386133 0.399328 0.029 Uiso 1 1 calc R U . . . C3 C 0.6237(2) 0.31676(11) 0.47399(15) 0.0346(3) Uani 1 1 d . . . . . H3A H 0.561954 0.278768 0.525131 0.042 Uiso 1 1 calc R U . . . H3B H 0.731142 0.331139 0.518517 0.042 Uiso 1 1 calc R U . . . C4 C 0.6516(2) 0.26757(11) 0.35735(17) 0.0382(4) Uani 1 1 d . . . . . H4A H 0.545103 0.245607 0.318835 0.046 Uiso 1 1 calc R U . . . H4B H 0.724771 0.216594 0.376152 0.046 Uiso 1 1 calc R U . . . C5 C 0.7309(2) 0.33021(10) 0.27071(15) 0.0314(3) Uani 1 1 d . . . . . H5A H 0.734231 0.301105 0.192403 0.038 Uiso 1 1 calc R U . . . H5B H 0.845453 0.343664 0.303086 0.038 Uiso 1 1 calc R U . . . C6 C 0.63034(18) 0.41704(10) 0.25394(13) 0.0239(3) Uani 1 1 d . . . . . H6 H 0.518559 0.404050 0.212850 0.029 Uiso 1 1 calc R U . . . C7 C 0.72101(18) 0.48080(10) 0.17690(13) 0.0242(3) Uani 1 1 d . . . . . C8 C 0.8198(2) 0.48814(11) -0.02118(14) 0.0327(3) Uani 1 1 d . . . . . H8A H 0.896775 0.530568 0.021145 0.039 Uiso 1 1 calc R U . . . H8B H 0.753128 0.519352 -0.086360 0.039 Uiso 1 1 calc R U . . . C9 C 0.91580(17) 0.41303(10) -0.07220(13) 0.0247(3) Uani 1 1 d . . . . . C10 C 0.90150(19) 0.39602(11) -0.19667(13) 0.0284(3) Uani 1 1 d . . . . . H10 H 0.830891 0.431010 -0.249473 0.034 Uiso 1 1 calc R U . . . C11 C 0.9926(2) 0.32679(12) -0.24223(14) 0.0328(3) Uani 1 1 d . . . . . H11 H 0.984643 0.316420 -0.325736 0.039 Uiso 1 1 calc R U . . . C12 C 1.0945(2) 0.27348(11) -0.16463(15) 0.0333(3) Uani 1 1 d . . . . . H12 H 1.154117 0.226733 -0.195516 0.040 Uiso 1 1 calc R U . . . C13 C 1.1081(2) 0.28951(12) -0.04030(15) 0.0330(3) Uani 1 1 d . . . . . H13 H 1.176431 0.253272 0.012353 0.040 Uiso 1 1 calc R U . . . C14 C 1.02008(19) 0.35940(11) 0.00553(14) 0.0306(3) Uani 1 1 d . . . . . H14 H 1.030827 0.370527 0.088894 0.037 Uiso 1 1 calc R U . . . O5 O 0.48577(18) 0.60123(8) 0.81203(11) 0.0414(3) Uani 1 1 d . . . . . O6 O 0.31140(13) 0.55487(7) 1.08511(9) 0.0243(2) Uani 1 1 d . . . . . O7 O 0.18654(14) 0.45362(7) 1.25916(10) 0.0312(2) Uani 1 1 d . . . . . O8 O 0.14316(14) 0.57687(7) 1.36816(10) 0.0316(2) Uani 1 1 d . . . . . N2 N 0.34697(17) 0.48024(9) 0.87149(11) 0.0303(3) Uani 1 1 d . . . . . H2A H 0.369986 0.449056 0.809807 0.036 Uiso 1 1 calc R U . . . H2B H 0.288471 0.457223 0.924842 0.036 Uiso 1 1 calc R U . . . C15 C 0.40164(18) 0.56375(10) 0.88433(13) 0.0269(3) Uani 1 1 d . . . . . C16 C 0.35235(18) 0.61634(10) 0.99324(13) 0.0250(3) Uani 1 1 d . . . . . H16 H 0.250757 0.650581 0.966531 0.030 Uiso 1 1 calc R U . . . C17 C 0.48736(19) 0.68205(10) 1.04055(14) 0.0281(3) Uani 1 1 d . . . . . H17A H 0.506828 0.724508 0.976976 0.034 Uiso 1 1 calc R U . . . H17B H 0.591534 0.650281 1.063463 0.034 Uiso 1 1 calc R U . . . C18 C 0.4335(2) 0.73179(11) 1.15057(16) 0.0340(3) Uani 1 1 d . . . . . H18A H 0.525918 0.768092 1.186836 0.041 Uiso 1 1 calc R U . . . H18B H 0.340227 0.771239 1.124982 0.041 Uiso 1 1 calc R U . . . C19 C 0.3809(2) 0.66541(11) 1.24419(15) 0.0308(3) Uani 1 1 d . . . . . H19A H 0.478205 0.631949 1.278745 0.037 Uiso 1 1 calc R U . . . H19B H 0.334796 0.697401 1.309697 0.037 Uiso 1 1 calc R U . . . C20 C 0.24981(18) 0.60133(10) 1.18428(13) 0.0251(3) Uani 1 1 d . . . . . H20 H 0.151967 0.636611 1.152034 0.030 Uiso 1 1 calc R U . . . C21 C 0.19171(17) 0.53320(10) 1.27225(13) 0.0246(3) Uani 1 1 d . . . . . C22 C 0.0609(2) 0.52547(10) 1.45668(14) 0.0287(3) Uani 1 1 d . . . . . H22A H 0.141389 0.487683 1.504349 0.034 Uiso 1 1 calc R U . . . H22B H -0.026628 0.487932 1.416217 0.034 Uiso 1 1 calc R U . . . C23 C -0.01266(17) 0.59305(10) 1.53658(13) 0.0240(3) Uani 1 1 d . . . . . C24 C 0.0178(2) 0.58889(11) 1.66238(14) 0.0298(3) Uani 1 1 d . . . . . H24 H 0.085191 0.543629 1.698677 0.036 Uiso 1 1 calc R U . . . C25 C -0.0521(2) 0.65204(13) 1.73420(14) 0.0376(4) Uani 1 1 d . . . . . H25 H -0.033638 0.647851 1.818606 0.045 Uiso 1 1 calc R U . . . C26 C -0.1482(2) 0.72073(12) 1.68213(17) 0.0389(4) Uani 1 1 d . . . . . H26 H -0.193560 0.763245 1.730918 0.047 Uiso 1 1 calc R U . . . C27 C -0.1770(2) 0.72626(12) 1.55661(17) 0.0378(4) Uani 1 1 d . . . . . H27 H -0.240323 0.773211 1.520679 0.045 Uiso 1 1 calc R U . . . C28 C -0.1118(2) 0.66196(11) 1.48457(14) 0.0310(3) Uani 1 1 d . . . . . H28 H -0.134617 0.664914 1.400307 0.037 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0512(7) 0.0426(7) 0.0271(5) -0.0003(5) 0.0145(5) -0.0136(6) O2 0.0305(5) 0.0243(5) 0.0199(4) -0.0002(4) 0.0071(4) 0.0006(4) O3 0.0445(6) 0.0281(5) 0.0284(5) -0.0018(4) 0.0071(5) -0.0038(5) O4 0.0317(5) 0.0407(6) 0.0244(5) -0.0059(5) 0.0119(4) -0.0037(5) N1 0.0465(8) 0.0361(7) 0.0271(6) -0.0049(6) 0.0161(6) -0.0092(6) C1 0.0289(7) 0.0322(7) 0.0204(6) 0.0018(6) 0.0028(5) 0.0007(6) C2 0.0260(7) 0.0260(7) 0.0216(6) 0.0037(5) 0.0032(5) 0.0009(5) C3 0.0399(9) 0.0316(8) 0.0318(8) 0.0096(7) 0.0013(7) 0.0069(7) C4 0.0466(9) 0.0235(7) 0.0453(10) 0.0031(7) 0.0089(8) 0.0105(7) C5 0.0339(8) 0.0250(7) 0.0360(8) -0.0022(6) 0.0076(6) 0.0074(6) C6 0.0249(6) 0.0250(6) 0.0222(6) -0.0020(5) 0.0038(5) 0.0036(5) C7 0.0244(6) 0.0258(6) 0.0227(6) -0.0013(5) 0.0037(5) 0.0063(5) C8 0.0383(8) 0.0332(7) 0.0290(7) -0.0002(6) 0.0157(6) 0.0024(7) C9 0.0237(6) 0.0287(7) 0.0227(6) -0.0016(5) 0.0072(5) -0.0026(5) C10 0.0287(7) 0.0337(7) 0.0229(7) 0.0014(6) 0.0041(6) 0.0001(6) C11 0.0361(8) 0.0406(8) 0.0222(7) -0.0080(6) 0.0054(6) -0.0010(7) C12 0.0312(7) 0.0327(8) 0.0370(8) -0.0066(7) 0.0087(6) 0.0013(6) C13 0.0283(7) 0.0386(8) 0.0323(8) 0.0041(7) 0.0039(6) 0.0043(6) C14 0.0293(7) 0.0415(8) 0.0212(6) -0.0023(6) 0.0036(6) 0.0007(6) O5 0.0587(8) 0.0380(6) 0.0305(6) -0.0007(5) 0.0196(6) -0.0105(6) O6 0.0298(5) 0.0242(5) 0.0199(4) -0.0021(4) 0.0076(4) 0.0000(4) O7 0.0398(6) 0.0273(5) 0.0273(5) -0.0018(4) 0.0065(4) 0.0029(5) O8 0.0387(6) 0.0300(5) 0.0290(5) -0.0067(4) 0.0178(5) -0.0054(5) N2 0.0362(7) 0.0333(7) 0.0227(6) -0.0037(5) 0.0093(5) -0.0050(5) C15 0.0280(7) 0.0317(7) 0.0210(6) 0.0025(6) 0.0029(5) 0.0012(6) C16 0.0248(6) 0.0269(7) 0.0235(6) 0.0022(5) 0.0037(5) 0.0022(5) C17 0.0283(7) 0.0246(7) 0.0323(7) 0.0000(6) 0.0074(6) -0.0012(5) C18 0.0370(8) 0.0251(7) 0.0414(9) -0.0079(7) 0.0121(7) -0.0035(6) C19 0.0335(7) 0.0300(7) 0.0299(7) -0.0100(6) 0.0078(6) -0.0038(6) C20 0.0250(6) 0.0261(7) 0.0250(7) -0.0043(6) 0.0066(5) 0.0024(5) C21 0.0216(6) 0.0301(7) 0.0223(6) -0.0037(5) 0.0027(5) 0.0025(5) C22 0.0329(7) 0.0272(7) 0.0276(7) 0.0006(6) 0.0105(6) 0.0003(6) C23 0.0233(6) 0.0261(7) 0.0233(6) -0.0004(5) 0.0065(5) -0.0036(5) C24 0.0288(7) 0.0361(8) 0.0245(7) 0.0038(6) 0.0028(5) -0.0039(6) C25 0.0398(9) 0.0525(10) 0.0213(7) -0.0067(7) 0.0068(6) -0.0111(8) C26 0.0385(8) 0.0404(9) 0.0405(9) -0.0149(8) 0.0166(7) -0.0057(7) C27 0.0378(8) 0.0327(8) 0.0445(9) 0.0020(7) 0.0122(7) 0.0068(7) C28 0.0346(8) 0.0349(8) 0.0244(7) 0.0032(6) 0.0074(6) 0.0034(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 O2 C2 110.38(11) . . ? C7 O4 C8 118.43(12) . . ? H1A N1 H1B 120.0 . . ? C1 N1 H1A 120.0 . . ? C1 N1 H1B 120.0 . . ? O1 C1 N1 123.88(14) . . ? O1 C1 C2 117.98(14) . . ? N1 C1 C2 118.15(13) . . ? O2 C2 C1 110.44(12) . . ? O2 C2 H2 108.4 . . ? O2 C2 C3 110.83(12) . . ? C1 C2 H2 108.4 . . ? C1 C2 C3 110.39(12) . . ? C3 C2 H2 108.4 . . ? C2 C3 H3A 109.7 . . ? C2 C3 H3B 109.7 . . ? C2 C3 C4 109.80(13) . . ? H3A C3 H3B 108.2 . . ? C4 C3 H3A 109.7 . . ? C4 C3 H3B 109.7 . . ? C3 C4 H4A 109.7 . . ? C3 C4 H4B 109.7 . . ? C3 C4 C5 109.96(14) . . ? H4A C4 H4B 108.2 . . ? C5 C4 H4A 109.7 . . ? C5 C4 H4B 109.7 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 C6 110.52(13) . . ? H5A C5 H5B 108.1 . . ? C6 C5 H5A 109.5 . . ? C6 C5 H5B 109.5 . . ? O2 C6 C5 111.42(12) . . ? O2 C6 H6 109.4 . . ? O2 C6 C7 108.09(11) . . ? C5 C6 H6 109.4 . . ? C7 C6 C5 109.08(12) . . ? C7 C6 H6 109.4 . . ? O3 C7 O4 124.86(14) . . ? O3 C7 C6 126.41(13) . . ? O4 C7 C6 108.68(12) . . ? O4 C8 H8A 110.2 . . ? O4 C8 H8B 110.2 . . ? O4 C8 C9 107.64(13) . . ? H8A C8 H8B 108.5 . . ? C9 C8 H8A 110.2 . . ? C9 C8 H8B 110.2 . . ? C10 C9 C8 120.88(14) . . ? C14 C9 C8 119.87(13) . . ? C14 C9 C10 119.25(14) . . ? C9 C10 H10 120.0 . . ? C11 C10 C9 120.02(15) . . ? C11 C10 H10 120.0 . . ? C10 C11 H11 119.8 . . ? C12 C11 C10 120.39(14) . . ? C12 C11 H11 119.8 . . ? C11 C12 H12 120.1 . . ? C11 C12 C13 119.90(15) . . ? C13 C12 H12 120.1 . . ? C12 C13 H13 120.0 . . ? C14 C13 C12 120.02(15) . . ? C14 C13 H13 120.0 . . ? C9 C14 H14 119.8 . . ? C13 C14 C9 120.40(14) . . ? C13 C14 H14 119.8 . . ? C20 O6 C16 110.68(11) . . ? C21 O8 C22 117.59(12) . . ? H2A N2 H2B 120.0 . . ? C15 N2 H2A 120.0 . . ? C15 N2 H2B 120.0 . . ? O5 C15 N2 123.78(14) . . ? O5 C15 C16 118.69(14) . . ? N2 C15 C16 117.51(13) . . ? O6 C16 C15 108.94(11) . . ? O6 C16 H16 107.8 . . ? O6 C16 C17 112.28(12) . . ? C15 C16 H16 107.8 . . ? C17 C16 C15 112.01(12) . . ? C17 C16 H16 107.8 . . ? C16 C17 H17A 109.7 . . ? C16 C17 H17B 109.7 . . ? C16 C17 C18 110.00(12) . . ? H17A C17 H17B 108.2 . . ? C18 C17 H17A 109.7 . . ? C18 C17 H17B 109.7 . . ? C17 C18 H18A 109.6 . . ? C17 C18 H18B 109.6 . . ? H18A C18 H18B 108.2 . . ? C19 C18 C17 110.06(12) . . ? C19 C18 H18A 109.6 . . ? C19 C18 H18B 109.6 . . ? C18 C19 H19A 109.7 . . ? C18 C19 H19B 109.7 . . ? H19A C19 H19B 108.2 . . ? C20 C19 C18 109.96(13) . . ? C20 C19 H19A 109.7 . . ? C20 C19 H19B 109.7 . . ? O6 C20 C19 111.32(12) . . ? O6 C20 H20 108.0 . . ? O6 C20 C21 108.51(12) . . ? C19 C20 H20 108.0 . . ? C21 C20 C19 112.85(12) . . ? C21 C20 H20 108.0 . . ? O7 C21 O8 124.88(14) . . ? O7 C21 C20 126.87(13) . . ? O8 C21 C20 108.24(12) . . ? O8 C22 H22A 110.6 . . ? O8 C22 H22B 110.6 . . ? O8 C22 C23 105.72(12) . . ? H22A C22 H22B 108.7 . . ? C23 C22 H22A 110.6 . . ? C23 C22 H22B 110.6 . . ? C24 C23 C22 121.27(14) . . ? C24 C23 C28 118.83(14) . . ? C28 C23 C22 119.90(13) . . ? C23 C24 H24 119.9 . . ? C25 C24 C23 120.14(15) . . ? C25 C24 H24 119.9 . . ? C24 C25 H25 119.6 . . ? C26 C25 C24 120.73(15) . . ? C26 C25 H25 119.6 . . ? C25 C26 H26 120.2 . . ? C25 C26 C27 119.55(16) . . ? C27 C26 H26 120.2 . . ? C26 C27 H27 120.0 . . ? C28 C27 C26 119.98(16) . . ? C28 C27 H27 120.0 . . ? C23 C28 H28 119.6 . . ? C27 C28 C23 120.74(15) . . ? C27 C28 H28 119.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.2350(18) . ? O2 C2 1.4304(17) . ? O2 C6 1.4253(16) . ? O3 C7 1.1994(19) . ? O4 C7 1.3364(17) . ? O4 C8 1.4568(18) . ? N1 H1A 0.8600 . ? N1 H1B 0.8600 . ? N1 C1 1.322(2) . ? C1 C2 1.515(2) . ? C2 H2 0.9800 . ? C2 C3 1.518(2) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C4 1.518(2) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C4 C5 1.522(2) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C5 C6 1.528(2) . ? C6 H6 0.9800 . ? C6 C7 1.510(2) . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 C9 1.502(2) . ? C9 C10 1.390(2) . ? C9 C14 1.389(2) . ? C10 H10 0.9300 . ? C10 C11 1.389(2) . ? C11 H11 0.9300 . ? C11 C12 1.375(2) . ? C12 H12 0.9300 . ? C12 C13 1.386(2) . ? C13 H13 0.9300 . ? C13 C14 1.384(2) . ? C14 H14 0.9300 . ? O5 C15 1.2296(19) . ? O6 C16 1.4302(17) . ? O6 C20 1.4251(16) . ? O7 C21 1.1981(19) . ? O8 C21 1.3340(17) . ? O8 C22 1.4515(18) . ? N2 H2A 0.8600 . ? N2 H2B 0.8600 . ? N2 C15 1.325(2) . ? C15 C16 1.521(2) . ? C16 H16 0.9800 . ? C16 C17 1.513(2) . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 C18 1.522(2) . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 C19 1.522(2) . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 C20 1.521(2) . ? C20 H20 0.9800 . ? C20 C21 1.512(2) . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 C23 1.500(2) . ? C23 C24 1.386(2) . ? C23 C28 1.388(2) . ? C24 H24 0.9300 . ? C24 C25 1.386(2) . ? C25 H25 0.9300 . ? C25 C26 1.373(3) . ? C26 H26 0.9300 . ? C26 C27 1.383(3) . ? C27 H27 0.9300 . ? C27 C28 1.383(2) . ? C28 H28 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 O2 174.27(13) . . . . ? O1 C1 C2 C3 -62.82(18) . . . . ? O2 C2 C3 C4 -59.11(17) . . . . ? O2 C6 C7 O3 13.7(2) . . . . ? O2 C6 C7 O4 -168.89(11) . . . . ? O4 C8 C9 C10 119.84(15) . . . . ? O4 C8 C9 C14 -59.94(19) . . . . ? N1 C1 C2 O2 -6.26(18) . . . . ? N1 C1 C2 C3 116.66(16) . . . . ? C1 C2 C3 C4 178.21(13) . . . . ? C2 O2 C6 C5 -61.21(15) . . . . ? C2 O2 C6 C7 178.96(11) . . . . ? C2 C3 C4 C5 53.08(18) . . . . ? C3 C4 C5 C6 -51.39(19) . . . . ? C4 C5 C6 O2 55.63(17) . . . . ? C4 C5 C6 C7 174.88(13) . . . . ? C5 C6 C7 O3 -107.62(17) . . . . ? C5 C6 C7 O4 69.81(15) . . . . ? C6 O2 C2 C1 -174.21(11) . . . . ? C6 O2 C2 C3 63.13(15) . . . . ? C7 O4 C8 C9 125.53(14) . . . . ? C8 O4 C7 O3 11.0(2) . . . . ? C8 O4 C7 C6 -166.45(12) . . . . ? C8 C9 C10 C11 179.37(15) . . . . ? C8 C9 C14 C13 179.45(14) . . . . ? C9 C10 C11 C12 1.4(2) . . . . ? C10 C9 C14 C13 -0.3(2) . . . . ? C10 C11 C12 C13 -0.8(2) . . . . ? C11 C12 C13 C14 -0.4(2) . . . . ? C12 C13 C14 C9 1.0(2) . . . . ? C14 C9 C10 C11 -0.8(2) . . . . ? O5 C15 C16 O6 -159.31(13) . . . . ? O5 C15 C16 C17 -34.49(19) . . . . ? O6 C16 C17 C18 -56.10(16) . . . . ? O6 C20 C21 O7 -4.6(2) . . . . ? O6 C20 C21 O8 176.51(11) . . . . ? O8 C22 C23 C24 -128.43(14) . . . . ? O8 C22 C23 C28 50.85(18) . . . . ? N2 C15 C16 O6 22.40(18) . . . . ? N2 C15 C16 C17 147.22(14) . . . . ? C15 C16 C17 C18 -179.05(12) . . . . ? C16 O6 C20 C19 -61.04(16) . . . . ? C16 O6 C20 C21 174.20(11) . . . . ? C16 C17 C18 C19 52.03(18) . . . . ? C17 C18 C19 C20 -52.90(17) . . . . ? C18 C19 C20 O6 57.65(16) . . . . ? C18 C19 C20 C21 179.95(12) . . . . ? C19 C20 C21 O7 -128.43(16) . . . . ? C19 C20 C21 O8 52.66(16) . . . . ? C20 O6 C16 C15 -174.71(11) . . . . ? C20 O6 C16 C17 60.63(15) . . . . ? C21 O8 C22 C23 -167.66(12) . . . . ? C22 O8 C21 O7 -7.2(2) . . . . ? C22 O8 C21 C20 171.77(12) . . . . ? C22 C23 C24 C25 -179.84(14) . . . . ? C22 C23 C28 C27 -178.26(15) . . . . ? C23 C24 C25 C26 -1.8(2) . . . . ? C24 C23 C28 C27 1.0(2) . . . . ? C24 C25 C26 C27 0.7(3) . . . . ? C25 C26 C27 C28 1.2(3) . . . . ? C26 C27 C28 C23 -2.1(3) . . . . ? C28 C23 C24 C25 0.9(2) . . . . ?