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Information card for entry 4519167
Preview
| Coordinates | 4519167.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C48 H57 O P |
|---|---|
| Calculated formula | C48 H57 O P |
| Title of publication | Enantioselective Cobalt-Catalyzed Reductive Cross-Coupling for the Synthesis of Axially Chiral Phosphine–Olefin Ligands |
| Authors of publication | Zhang, Xi; Wang, Juan; Yang, Shang-Dong |
| Journal of publication | ACS Catalysis |
| Year of publication | 2021 |
| Journal volume | 11 |
| Journal issue | 22 |
| Pages of publication | 14008 - 14015 |
| a | 10.2524 ± 0.0001 Å |
| b | 10.0212 ± 0.0001 Å |
| c | 19.2295 ± 0.0002 Å |
| α | 90° |
| β | 90.56 ± 0.001° |
| γ | 90° |
| Cell volume | 1975.57 ± 0.03 Å3 |
| Cell temperature | 149.99 ± 0.1 K |
| Ambient diffraction temperature | 149.99 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0473 |
| Residual factor for significantly intense reflections | 0.0428 |
| Weighted residual factors for significantly intense reflections | 0.1019 |
| Weighted residual factors for all reflections included in the refinement | 0.1034 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.116 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 271033 (current) | 2021-12-03 | cif/ Adding structures of 4519167 via cif-deposit CGI script. |
4519167.cif |
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Users of the data should acknowledge the original authors of the
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