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Information card for entry 4519251
Preview
| Coordinates | 4519251.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H31 N O4 S |
|---|---|
| Calculated formula | C28 H31 N O4 S |
| Title of publication | Cp*RhIII/Chiral Disulfonate/CuOAc Catalyst System for the Enantioselective Intramolecular Oxyamination of Alkenes |
| Authors of publication | Hirose, Jumpei; Wakikawa, Takumi; Satake, Shun; Kojima, Masahiro; Hatano, Manabu; Ishihara, Kazuaki; Yoshino, Tatsuhiko; Matsunaga, Shigeki |
| Journal of publication | ACS Catalysis |
| Year of publication | 2021 |
| Journal volume | 11 |
| Journal issue | 24 |
| Pages of publication | 15187 - 15193 |
| a | 11.2477 ± 0.0007 Å |
| b | 11.2911 ± 0.0007 Å |
| c | 11.5245 ± 0.0007 Å |
| α | 85.163 ± 0.004° |
| β | 69.406 ± 0.003° |
| γ | 65.577 ± 0.003° |
| Cell volume | 1244.26 ± 0.14 Å3 |
| Cell temperature | 233 ± 2 K |
| Ambient diffraction temperature | 233 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.0396 |
| Residual factor for significantly intense reflections | 0.0377 |
| Weighted residual factors for significantly intense reflections | 0.1048 |
| Weighted residual factors for all reflections included in the refinement | 0.1062 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
| Diffraction radiation wavelength | 1.5418 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 271746 (current) | 2022-01-03 | cif/ Adding structures of 4519251 via cif-deposit CGI script. |
4519251.cif |
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Users of the data should acknowledge the original authors of the
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